CAS: 61652-81-1; Decane-1-Sulfonyl Chloride

该化合物是有机化合物,其特征是:含有一个附于一个十烷链的全氟辛烷磺酸功能组;该化合物一般是淡黄色液体的无色,有刺眼味;在二氯甲烷和乙醚等有机溶剂中溶解,但由于其盐分碳基链,一般在水中无法溶解;1-Decanesulfonyl 氯化物因其活性而闻名,特别是在核糖类替代反应中,可用作磺酰胺和其他衍生物;在与该化合物合作时,必须谨慎处理,因为它具有腐蚀性,可能会对皮肤,眼睛和呼吸系统造成刺激;适当的安全防范措施,包括使用个人防护设备,并在通风良好的地区工作.

结构式图片

欧盟法规

ECHA物质C&L通报

上下游产品

1-bromo dodecane 1-thi°Cyanatodecane didecyl disulfide perfluorodecane sulfonylfluoride decane-1-sulfonanilide Aethyl-4-decansulfonamidobenzoat N'-(decylsulfonyloxy)-4-nitrobenzimidamide

合成工艺路线路线简述

  • 合成目标产物 1-Decanesulfonyl Chloride 主要起始原料 Didecyl Disulfide
  • (文献来源)合成步骤主要原料 Didecyl Disulfide
📜癸基溴置于水,Sodium Sulfite体系中,化学反应生成 1-癸烷磺酰氯
参考文献:Burdon Et Al.,Journal Of The Chemical Society,1957,P. 2574,2576
标题:Burdon Et Al.,Journal Of The Chemical Society,1957,P. 2574,2576

海关参考信息

专利信息


专利号:US-2003153783-A1
优先权日:1999-06-30
标题:Synthesis of (R) and (S)-aminocarnitine, (R) and (S)-4-phosphonium-3-amino-butanoate, (R) and (S) 3,4-diaminobutanoic acid, and their derivatives starting from D- and L-aspartic acid
发明人:GIANNESSI FABIO; DELL UOMO NATALINA; TINTI MARIA ORNELLA; DE ANGELIS FRANCESCO
权利人:SIGMA TAU IND FARMACEUTI
摘要:A process is described for the preparation of R or S aminocarnitine, R or S phosphonium aminocarnitine and R and S 3,4 diaminobutanoic acid, and their derivatives with the following formula: n n n where Y is as described in the attached description, starting from aspartic acid with the same configuration as the desired compounds. This process is advantageous from the industrial point of view in terms of the type of reactants used, the reduced volumes of solvents and the possibility of avoiding purification of the intermediate products.

专利号:US-6228988-B1
优先权日:1995-02-24
标题:Synthesis of hydroxamic acid derivatives
发明人:FLOYD CHRISTOPHER DAVID; LEWIS CHRISTOPHER NORMAN
权利人:BRITISH BIOTECH PHARM
摘要:The present invention describes processes for preparing desired synthetic products that comprise a covalently bonded hydroxamic acid group -CONHOH by forming a mixture of a liquid reaction medium and a solid phase reaction product that carries a plurality of moieties of formula (A1) or (B1):where X is a residual, non-hydroxamate partial structure of the desired synthetic product, P1 is hydrogen or an amino-protecting group, P2 is hydrogen or a hydroxyl protecting group, and the bond designated (a) covalently links the moieties (A1) or (B1) to the residue of a solid substrate; by cleaving the bond designated (a) in the resultant mixture; and by separating the resultant liquid reaction phase from the resultant reaction solids to recover the desired synthetic product.

专利号:US-6822115-B2
优先权日:1999-06-30
标 题:Synthesis of (R) and (S)-aminocarnitine, (R) and (S)-4-phosphonium-3-amino-butanoate, (R) and (S) 3,4-diaminobutanoic acid, and their derivatives starting from D- and L-aspartic acid
发明人:GIANNESSI FABIO; DELL UOMO NATALINA; TINTI MARIA ORNELLA; DE ANGELIS FRANCESCO
权利人:SIGMA TAU IND FARMACEUTI
摘要:R or S aminocarnitine, R or S phosphonium aminocarnitine and R and S 3,4 diaminobutanoic acid, and their derivatives are prepared using n starting from aspartic acid with the same configuration as the desired compounds. This process is advantageous from the industrial point of view in terms of the type of reactants used, the reduced volumes of solvents and the possibility of avoiding purification of the intermediate products.

专利号:US-6528684-B1
优先权日:1999-06-30
标题 :Synthesis of (R) and (S) -aminocarnitine and their derivatives starting from D- and L-aspartic acid
发明人:GIANNESSI FABIO; DELL UOMO NATALINA; TINTI MARIA ORNELLA; DE ANGELIS FRANCESCO
权利人:SIGMA TAU IND FARMACEUTI
摘要:R or S aminocarnitine and their derivatives with formula (I)where Y is as described in the description, starting with aspartic acid with the same configuration as the aminocarnitine desired. This process has advantage in the type of reactants used, reduced volumes of solvents and the possibility of avoiding purification of intermediate products.

专利号:US-2003153784-A1
优先权日:1999-06-30
标题 :Synthesis of (R) and (S)-aminocarnitine, (R) and (S)-4-phosphonium-3-amino-butanoate, (R) and (S) 3,4-diaminobutanoic acid, and their derivatives starting from D- and L-aspartic acid

专利号:US-6093798-A
优先权日:1995-02-24
标题 :Synthesis of hydroxamic acid derivatives

供应商参考报价(招募中)

品牌试剂参考报价(招募中)

📌 第三方产品分析报告

✅ COA系统入驻 | 共享模式

合成参考文献

参考DOI号:10.1016/j.tet.2014.02.013
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