CAS: 127604-16-4; Sodium (S)-3-Hydroxybutanoate

该化合物是三氢丁酸的一种钠盐衍生物,是一种短链脂肪酸,其特征是它在各种生化过程中的作用,特别是在能源新陈代谢和作为潜在治疗剂的作用,通常在水中溶解,适合生物和制药环境中的各种应用.(S)配置表明其具体的立体化学,这对生物活动至关重要.这种化合物可能具有诸如能源来源,影响代谢途径和可能成为合成其他生物分子的前体等特性.此外,它可能对临床研究产生影响,特别是在与代谢障碍和...

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13613-65-5 150-83-4 1219804-68-8

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CAS号53562-86-0 (S)-(+)3-羟基丁酸甲酯 | CAS号127604-17-5 benzyl (3S)-3-h...

合成工艺路线路线简述

    📜(S)-3-羟基丁酸甲酯置于sodium Hydroxide体系中,化学反应生成(S)-(+)-3-羟基丁酸钠盐
    参考文献:Tai,Akira; Morimoto,Naotake; Yoshikawa,Masato,Agricultural And Biological Chemistry,1990,Vol. 54,# 7,P. 1753-1762
    标题:Tai,Akira; Morimoto,Naotake; Yoshikawa,Masato,Agricultural And Biological Chemistry,1990,Vol. 54,# 7,P. 1753-1762

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    参考标题:Sythesis Of 1,3-Dioxin-4-Ones And Their Use In Synthesis. Xviii. Synthesis Of Azetidin-2-Ones From 1,3-Dioxin-4-Ones Via 3-Hydroxycarboxamides.
    作者:Jun-Ichi Sakaki,Satoshi Kobayashi,Masayuki Sato,Chikasra Kaneko
    摘要:A General Method For The Synthesis Of Azetidin-2-Ones From 1, 3-Dioxin-4-Ones Is Described. The Method Consists Of 1) The Formatin Of β-Ketocarboxamides, 2) Their Reduction To 3-Hydroxycarboxamides, 3) Mesylationg, And 4) Base-Mediated Cyclization Of 3-Mesyloxycarboxamides To The Final Azetidinones. Stereochemical Demand In The Cyclizatino Step Has Been Clarified By Using 5, 6-Tri- And -Tetramethylene Derivatives Of 2, 2-Dimethyl-1, 3-Dioxin-4-One. Microbiological Reduction Of The Acetoacetamides By Baker'S Yeast Gave (S)-3-Hydroxybutanamides Of >=98% Optical Purity, Whose Cyclization Afforded (R)-4-Methylazetidin-2-Ones.
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