CAS: 897-15-4; (Z)-3-(Dibenzo[b,E]Thiepin-11(6H)-Ylidene)-N,N-Dimethylpropan-1-Amine Hydrochloride
- 英文名称(Z)-3-(Dibenzo[b,E]Thiepin-11(6H)-Ylidene)-N,N-Dimethylpropan-1-Amine Hydrochloride
- 中文名称盐酸度硫平杂质
- IUPAC名称(Z)-3-(dibenzo[b,e]thiepin-11(6H)-ylidene)-N,N-dimethylpropan-1-amine hydrochloride
- 其它别名Dothiepin Hydrochloride; 11-[3-(Dimethylamino)Propylidene]-6,E]Thiepine Hydrochloride; 1-Propanamine,E]Thiepin-11(6H)-Ylidene-N,N-Dimethyl-, Hydrochloride; Dosulepin Hydrochloride [jan]; Dothiepin Hydrochloride; Dosulepin
- CAS编号897-15-4
- MFCD编号:MFCD00941484
- EINECS号:212-978-8
- 分子式:C19H22ClNS分子量:331.91
- 产品CID: 1918930
- 产品分类分析化学 → 标准品 → 药典标准品和杂质标准品
物理性质
MSDS等安全信息
欧盟法规
ECHA物质C&L通报REACH预注册上下游产品
CAS号113-53-1 度硫平 | CAS号1154-09-2 去甲度硫平合成工艺路线路线简述
📜度琉平置于盐酸体系中,用 乙醚,乙醇 作为反应溶剂,化学反应生成 盐酸度硫平杂质
参考文献:Wo2007/136743
标题:Wo2007/136743
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主要参考文献
1. Lancaster SG, Gonzalez JP. Dothiepin. A review of its pharmacodynamic and pharmacokinetic properties, and therapeutic efficacy in depressive illness. Drugs. 1989 Jul;38(1):123-47. doi: 10.2165/00003495-198938010-00005.180:179-84. doi: 10.1016/j.jad.2015.03.021. Epub 2015 Mar 31. 18(7):1143-62. doi: 10.1016/0278-5846(94)90117-1.
合成参考文献
参考文献:10.1007/s10812-012-9670-7
摘要:Abdulrahman SAM, Basavaiah K, Cijo MX, Vinay KB. Validation of UV spectrophotometric methods for the determination of dothiepin hydrochloride in pharmaceutical dosage form and stress degradation studies. Journal of Applied Spectroscopy. 2012 Nov 23;79(5):780–7. doi: 10.1007/s10812-012-9670-7.
参考文献:10.1007/s00216-003-2040-9
摘要:Taha EA. Kinetic spectrophotometric methods for the determination of dothiepin hydrochloride in bulk and in drug formulation. Analytical and Bioanalytical Chemistry. 2003 Aug 01;376(7):1131–6. doi: 10.1007/s00216-003-2040-9.
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