专利号:US-4100262-A 优先权日:1977-08-15 标 题:Synthesis of zeolite ZSM-5 发明人:PELRINE BRUCE PATRICK 权利人:MOBIL OIL CORP 摘要:As synthesized by conventional technique, zeolite ZSM-5 crystals are cubic with some twinning and measure in size over the range of from about 3 × 3 microns to about 8 × 8 microns. By synthesizing crystalline aluminosilicate zeolite ZSM-5 according to the present method, i.e. in the presence of a tetraureacobalt (II) complex and with a specifically defined reaction mixture composition, the crystalline product will consist of highly twinned rectangular prismatic crystals exhibiting extreme uniformity in size of from about 5 × 10 microns to about 10 × 20 microns, depending on the ratio of said tetraureacobalt (II) complex to silica in the zeolite synthesis reaction mixture. Synthesis of ZSM-5 in accordance hereto will provide a zeolite with enhanced catalytic activity for certain chemical reactions.
专利号:WO-0140193-A1 优先权日:1999-12-03 标题:Method for the synthesis of pyrazolines 发明人:BOLDI ARMEN M 权利人:CHEMRX ADVANCED TECHNOLOGIES I; BOLDI ARMEN M 摘要:The present invention provides a method for the synthesis of compounds of Formula (I). Also claimed are novel intermediates and their methods of synthesis.
专利号:US-2003162992-A1 优先权日:2001-12-14 标 题 :Preparation of intermediates useful in the synthesis of antiviral nucleosides 发明人:WATANABE KYOICHI A; DU JINFA 摘要:The present invention is an efficient process for the manufacture of α-acyloxyacetaldehyde, a key intermediate in the synthesis of 1,3-oxathiolane and 1,3-dioxolane nucleosides.
专利号:US-5475177-A 优先权日:1989-05-26 标 题:Process for the synthesis of alkylated aromatic hydrocarbons 发明人:GANHY JEAN-PIERRE 权利人:SOLVAY INTEROX 摘要:PCT No. PCT/EP92/02026 Sec. 371 Date May 19, 1994 Sec. 102(e) Date May 19, 1994 PCT Filed Sep. 2, 1992 PCT Pub. No. WO93/05001 PCT Pub. Date Mar. 18, 1993.Process for the synthesis of alkylated aromatic hydrocarbons containing a saturated alkyl chain comprising at least four carbon atoms, according to which an aromatic hydrocarbon substituted by a saturated short-chain alkyl group comprising one to three carbon atoms is reacted with an olefin in the presence of a catalyst which comprises at least one alkali metal or one alkali metal hydride impregnated on an alumina support and the catalyst is prepared in the reaction medium in the presence of the aromatic hydrocarbon containing a short alkyl chain by mixing anhydrous alumina with the alkali metal hydride or with the alkali metal, the ratio by weight of the alkali metal or of the alkali metal hydride to the alumina support being between 0.6 and 1.8. Use of the process for the synthesis of tert-amylbenzene by alkylation of cumene with ethylene.
专利号:US-2002103381-A1 优先权日:2000-11-30 标 题 :Method for the synthesis of pyrazolines 发明人:BOLDI ARMEN M 摘要:The present invention provides a method for the synthesis of compounds of Formula I: n n n Also claimed are novel intermediates and their methods of synthesis.
专利号:US-2025154014-A1 优先权日:2022-02-15 标 题 :Continuous flow synthesis of mesoporous silica particles 发明人:KULKARNI AMOL ARVINDRAO; JUNDALE RAJASHRI BABURAO; BARI ATUL HARISHCHANDRA 权利人:COUNCIL SCIENT IND RES 摘要:The present invention discloses a continuous flow synthesis of mesoporous silica particles by using a reactor at shorter reaction times. The particle size of mesoporous silica particles are in the range of 400 nm-1.5 microns. and is monodispersed. surface area >700 m2/g and pore size in the range of 2-4 nm.