CAS: 53866-34-5; (8R,9S,13S,14S)-2,4,16,16-Tetradeuterio-3-Hydroxy-13-Methyl-6,7,8,9,11,12,14,15-Octahydrocyclopenta[a]Phenanthren-17-One
- 英文名称(8R,9S,13S,14S)-2,4,16,16-Tetradeuterio-3-Hydroxy-13-Methyl-6,7,8,9,11,12,14,15-Octahydrocyclopenta[a]Phenanthren-17-One
- 中文名称雌酮-2,4,16,16-d4
- IUPAC名称(8R,9S,13S,14S)-2,4,16,16-tetradeuterio-3-hydroxy-13-methyl-6,7,8,9,11,12,14,15-octahydrocyclopenta[a]phenanthren-17-one
- 其它别名Estrone-2,4,16,16-d4
- CAS编号53866-34-5
- MFCD编号:MFCD01074157
- EINECS号:685-780-6
- 分子式:C18H18D4O2分子量:274.39
- 产品CID: 2504696
- 产品分类化学试剂 → 氘代试剂
物理性质
MSDS等安全信息
欧盟法规
C&L通报上下游产品
CAS号53-16-7 雌酚酮 | CAS号56588-58-0 雌酚酮-D2 | CAS号221093-45-4 17β-雌二醇-2,4,16,...合成工艺路线路线简述
- 合成目标产物 Estrone-2,4,16,16-D4 主要起始原料 Estrone
- (文献来源)合成步骤主要原料 Estrone
📜雌酚酮置于氘代三氟乙酸,乙醇体系中,化学反应 0.17H,以95%的收率获得产物雌酮-2,4,16,16-D4
参考文献:Expedient Microwave Deuteration Of Estrone In Cf3Cood
标题:Expedient Microwave Deuteration Of Estrone In Cf3Cood
摘要:A Rapid And Efficient Deuteration Procedure Was Developed For Estrone. Irradiation Of Estrone In Cf3Cood In A Microwave Oven Gave [2,4,16,16-H-2(4)]-Estrone In 95% Yield. Ultrasound And Cf3Cood Reflux Deuterations Of Estrone Were Also Studied. (C) 2002 Published By Elsevier Science Ltd.
DOI:10.1016/s0040-4039(02)00509-9
海关参考信息
- 2902600000-乙苯
2902700000-异丙基苯
2912110000-甲醛
2912120000-乙醛 - 💡 提示：海关信息按照顺序优先匹配，如需确认的海关信息，请参考相关资料。
- 详情请参考：📖 海关编码查询和海关进出口税则
供应商参考报价(招募中)
品牌试剂参考报价(招募中)
📌 第三方产品分析报告
合成参考文献
参考文献:10.1007/s00216-018-1069-8
摘要:Gusmaroli L, Insa S, Petrovic M. Development of an online SPE-UHPLC-MS/MS method for the multiresidue analysis of the 17 compounds from the EU “Watch list”. Analytical and Bioanalytical Chemistry. 2018 Apr 24;410(17):4165–76. doi: 10.1007/s00216-018-1069-8.
参考文献:10.1186/1752-153x-7-74
摘要:Segura PA, Kaplan P, Yargeau V. Identification and structural elucidation of ozonation transformation products of estrone. Chemistry Central Journal. 2013 Apr 23;7(1). doi: 10.1186/1752-153x-7-74.
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