📜甲基碘化镁置于cadmium(II) Chloride体系中,化学反应生成 高纯二甲基镉 参考文献:Investigation Of An Abnormal Organocadmium Reaction1 标题:Investigation Of An Abnormal Organocadmium Reaction1 摘要: DOI:10.1021/ja01525A044
专利信息
专利号:US-7615169-B2 优先权日:2004-09-20 标题 :Method for synthesis of colloidal nanoparticles 发明人:STROUSE GEOFFREY FIELDING; GERBEC JEFFREY A; MAGANA DONNY 权利人:UNIV CALIFORNIA 摘要:A method for synthesis of high quality colloidal nanoparticles using comprises a high heating rate process. Irradiation of single mode, high power, microwave is a particularly well suited technique to realize high quality semiconductor nanoparticles. The use of microwave radiation effectively automates the synthesis, and more importantly, permits the use of a continuous flow microwave reactor for commercial preparation of the high quality colloidal nanoparticles.
专利号:US-7927516-B2 优先权日:2004-09-20 标题 :Method for synthesis of colloidal nanoparticles 发明人:STROUSE GEOFFREY F; GERBEC JEFFREY A; MAGANA DONNY 权利人:UNIV CALIFORNIA 摘要:A method for synthesis of high quality colloidal nanoparticles using comprises a high heating rate process. Irradiation of single mode, high power, microwave is a particularly well suited technique to realize high quality semiconductor nanoparticles. The use of microwave radiation effectively automates the synthesis, and more importantly, permits the use of a continuous flow microwave reactor for commercial preparation of the high quality colloidal nanoparticles.
专利号:US-7998271-B2 优先权日:2003-11-19 标题 :Solvents and new method for the synthesis of CdSe semiconductor nanocrystals 发明人:ALKHAWALDEH AMMAR S; PASQUALI MATTEO; WONG MICHAEL S 权利人:William Marsh Rice Universtiy 摘要:New methods for the synthesis of nanocrystals/quantum dots are disclosed. The methods comprise use of reasonably-priced and commercially available heat transfer fluids (such as Dowtherm® A) as solvents to synthesize CdSe nanocrystals. Separation of nucleation and growth is achieved by quenching the reaction solution with relatively cold (room temperature) solvent to lower the solution temperature. Quenching may be followed by raising the solution temperature, to allow controlled growth to take place.
专利号:US-2018076373-A1 优先权日:2016-09-13 标题 :SOLUTION PHASE SYNTHESIS OF HIGHLY PROCESSIBLE NANOCRYSTALLINE LiZnP AND SIMILAR TERNARY SEMICONDUCTORS 发明人:Vela-Becerra Javier; White Miles Arthur Burris; THOMPSON MICHELLE JOANN; MILLER GORDON J 权利人:VELA BECERRA JAVIER; White Miles Arthur Burris; THOMPSON MICHELLE JOANN; MILLER GORDON J; UNIV IOWA STATE RES FOUND INC 摘要:Nowotny-Juza phases offer a wide range of potential applications including solar cell and thermoelectric device fabrication. The disclosure presents a solution phase synthesis of the Nowotny-Juza semiconductors LiZnP, LiCdP, and LiZnSb. These samples are phase pure, crystalline, and exhibit particle sizes of around 20 nm.
专利号:US-2005036938-A1 优先权日:2003-08-13 标 题 :Method for synthesizing nanoparticles of metal sulfides 发明人:HYEON TAEGWHAN 摘要:A synthetic method of fabricating highly crystalline and uniform nanoparticles of metal sulfides, doped metal sulfides, and multi-metallic sulfides disclosed, using no-toxic and inexpensive reagents. A typical synthetic method comprises the steps of, synthesis of metal-surfactant complexes from the reaction of metal precursors and surfactant, addition of sulfur reagent to the solution containing said metal-surfactant complexes followed by heating to high temperature, aging at that temperature to produce metal sulfide nanoparticles and completing the formation of synthesis of nanoparticles metal sulfides and multi-metallic sulfides by adding a poor solvent followed by centrifuging.
专利号:US-7482059-B2 优先权日:2004-05-10 标 题:Semiconductor nanocrystal complexes comprising a metal coating and methods of making same 发明人:PENG ADAM; LIU WEI 权利人:EVIDENT TECHNOLOGIES 摘要:A semiconductor nanocrystal complex including a metal layer formed on the outer surface of a semiconductor nanocrystal core after synthesis of the semiconductor nanocrystal core and a method for preparing a nanocrystal complex comprising forming a metal layer on a semiconductor nanocrystal core after synthesis of the semiconductor nanocrystal core. The metal layer may passivate the surface of the semiconductor nanocrystal core and protect the semiconductor nanocrystal core from the effects of oxidation. Also provided is a semiconductor nanocrystal complex with a shell grown onto the metal layer formed on the semiconductor nanocrystal core. In this embodiment, the metal layer may prevent lattice mismatch between the semiconductor shell and the semiconductor nanocrystal core.
摘要:O'Brien, P.; Malik, M. A., Science of Synthesis, (2004) 3, 100. 摘要:O'Brien, P.; Malik, M. A., Science of Synthesis, (2004) 3, 104. 摘要:O'Brien, P.; Malik, M. A., Science of Synthesis, (2004) 3, 102. 摘要:O'Brien, P.; Malik, M. A., Science of Synthesis, (2004) 3, 99. 摘要:O'Brien, P.; Malik, M. A., Science of Synthesis, (2004) 3, 97.