CAS: 27519-02-4; Muscalure

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CAS号17049-50-2 癸基溴化镁 | CAS号93662-70-5 1-iodotridec-4-ene | CAS号100566-56-1 (Z)-d°Cos-13-en... | CAS号75-16-1 甲基溴化镁 | CAS号39487-08-6 9-TRICOSYNE | CAS号125043-73-4 (Z)-tricos-14-e... | CAS号124-19-6 正壬醛 | CAS号124-25-4 十四烷醛

油醇置于li2Cucl3,三苯基膦,Lithium Iodide,偶氮二甲酸二乙酯体系中,用 四氢呋喃,乙醚 用作溶剂,化学反应 6.0H,反应生成诱虫烯
参考文献:New Simple Synthesis Of The Housefly Sex Attractant
标题:New Simple Synthesis Of The Housefly Sex Attractant
摘要:
Doi:10.1080/00304949709355226

专利信息

专利号:US-3798273-A
优先权日:1972-11-29
标 题:Intermediate for synthesis of housefly sex attractant
发明人：CARGILL R
权利人:RESEARCH CORP
摘要:THE INVENTION RELATES TO COMPOUNDS OF THE FORMULA CH3-(CH2)7-CH=CH-(CH2)X-CO-(CH2)Y-CH3 (CIS) WHEREIN X IS AN INTEGER FROM 7 TO 11, INCLUSIVE, AND Y IS AN INTEGER FROM 0 TO 4 INCLUSIVE, SAID KETONE CONTAINING 23 CARBON ATOMS WHICH ARE USEFUL IN THE SYNTHESIS OF THE HOUSEFLY SEX ATTRACTANT OF THE FORMULA CH3-(CH3)7-CH=CH-(CH2)12-CH3 (CIS)

专利号:US-4922049-A
优先权日:1989-01-13
标 题:Synthesis of cis-olefins
发明人：BYERS JIM D
权利人:PHILLIPS PETROLEUM CO
摘要:A process for the synthesis of cis-olefins from cis-olefinic alcohols consisting essentially of the following steps: n (a) reacting a cis-olefinic alcohol with a source of an alkali metal ion selected from the group consisting of lithium and sodium ions to form a first reaction product, n (b) then contacting said thus formed first reaction product with a sulfonyl halide compound to form a second reaction product, n (c) then containing said thus formed second reaction product with an alkyl magnesium compound and a cuprous salt to form a third reaction product comprising a cis-olefin wherein said steps are carried out in a suitable organic solvent.

专利号:WO-2025056767-A1
优先权日:2023-09-15
标题 :Process for the preparation of enantiomerically enriched aliphatic amines
发明人：BOU HAMDAN FARHAN; GODINEAU EDOUARD; SMEJKAL TOMAS; DUMEUNIER RAPHAEL; BOUSSEMGHOUNE MOHAMED ABDELOUAHAB; BLUM MATHIAS
权利人:SYNGENTA CROP PROTECTION AG
摘要:The present invention relates to a process for the preparation of enantiomerically enriched cyclobutylamines of formula (I) from α-tertiary cyclobutanones and reacting said enantiomerically enriched cyclobutylamines to enantiomerically enriched cyclobutylamides. Such compounds are useful intermediates in the synthesis of microbiocidal thiazole compounds.

专利号:US-4749818-A
优先权日:1987-09-30
标 题:Synthesis of cis-9-tricosene
发明人：BYERS JIM D; DRAKE CHARLES A
权利人:PHILLIPS PETROLEUM CO
摘要:A process for the preparation of cis-9-tricosene is disclosed. Cis-1,9-octadecadiene, which may be obtained by the dehydration of oleyl alcohol, is metallated with an organomagnesium halide, producing cis-9-octadecenylmagnesium halide, which in turn is alkylated with n-pentyl halide to form the desired cis-9-tricosene.

专利号:US-4006065-A
优先权日:1972-06-26
标题 :Process for the synthesis of pure isomers of long chain alkenes
发明人：MERESZ OTTO; MOZSGAI CECILIA
权利人:MERESZ OTTO; MOZSGAI CECILIA
摘要:Long chain alkenes are produced by electrolyzing an organic solution containing a mixture of short chain carboxylic acid and a larger chain carboxylic acid, one of which is unsaturated. Many of the products so formed are useful as insect attractants.

专利号:US-5481040-A
优先权日:1994-03-31
标 题:Process for the preparation of phosphonium salts
发明人：FUKUMOTO TAKEHIKO; HIROKAWA KAZUSHI; OKADA KURAO
权利人:SHINETSU CHEMICAL CO
摘要:A process for the preparation of phosphonium salts by the use of chlorides, which is useful in the course of synthesis of olefin compounds by the Wittig reaction, and which comprises reacting a phosphine compound of the general formula R13P wherein R1 is a phenyl group or a straight-chain alkyl group having 2 to 8 carbon atoms, with a primary or secondary chloride of the general formula wherein R2 and R3 are hydrocarbon radicals, in a solvent selected from the group consisting of N,N-dimethylformamide, N,N-dimethylacetamide and N,N-1,3-dimethyl-2-imidazolidinone, and in the presence of an alkali metal salt of the general formula MBr or MI.