- 英文名称(3,4-Dimethylhexane-3,4-Diyl)Dibenzene
- 中文名称(3,4-二甲基己烷-3,4-二基)二苯
- IUPAC名称(3,4-dimethyl-4-phenylhexan-3-yl)benzene
- 其它别名3,4-Dimethyl-3,4-diphenylhexane; 1,1'-(1,2-diethyl-1,2-dimethyl-1,2-ethanediyl)bis-benzen; Benzene,1,1'-(1,2-diethyl-1,2-dimethyl-1,2-ethanediyl)bis-
- CAS编号10192-93-5
- MFCD编号:MFCD00230177
- EINECS号:233-474-4
- 分子式:C20H26分子量:266.42
- 产品CID: 40520
- 产品分类有机原料→分子砌块→芳环类化合物→苯类化合物
欧盟法规
ECHA物质ECHA物质C&L通报REACH预注册上下游产品
CAS号75-16-1 甲基溴化镁 | CAS号93-55-0 苯丙酮 | CAS号1565-75-9 2-苯基-2-丁醇 | CAS号98-86-2 苯乙酮 | CAS号925-90-6 乙基溴化镁 | CAS号917-54-4 甲基锂 | CAS号100-39-0 溴化苄合成工艺路线路线简述
- 合成目标产物 3,4-Dimethyl-3,4-Diphenylhexane 主要起始原料 Methylmagnesium Bromide And Benzyl Bromide And Propiophenone
- (文献来源)合成步骤主要原料 Methylmagnesium Bromide 和 Benzyl Bromide 和 Propiophenone
📜仲丁基苯置于二叔丁基过氧化物,Sodium Acetate体系中,化学反应 10.0H,以82%的收率获得3,4-二甲基-3,4-二苯基己烷
参考文献:还原性氧化石墨烯负载的ptpd @ Pt多孔纳米球催化的非偶合基团sp3 C-h活化,通过均相偶合合成联苄.
标题:还原性氧化石墨烯负载的ptpd @ Pt多孔纳米球催化的非偶合基团sp3 C-h活化,通过均相偶合合成联苄.
摘要:很少探索使用非均相双金属钯基纳米催化剂指导失活的sp 3 C-H偶联.这项工作报道了通过使用还原性氧化石墨烯负载的ptpd @ Pt多孔纳米球催化的灭活的sp 3 C-H键形成对称的c-C键.Sp 3 C H活化反应在温和条件下进行,没有任何溶剂,配体或指导基团.在合成具有各种官能团(例如芳基,烷基,甲氧基,卤素,酯和吡啶基)的联苄中,开发多相催化剂是一种更高的原子,步骤和成本效益策略.
Doi:10.1002/adsc.201701389
专利信息
专利号:US-2003068317-A1
优先权日:2001-04-20
标题:High capacity methods for separation, purification, concentration, immobilization and synthesis of compounds and applications based thereupon
发明人:LEE WILLIAM; SAITO KYOICHI
摘要:Compositions are provided herein comprising a base material having engrafted polymer brushes. The polymer brushes further comprise one or more functional groups immobilized along the surface of the brushes in a plurality of layers, which confer functional properties to the base material compositions. Methods of using these compositions include deoxygenation of a sample solution, hydrolysis of denaturing agents in a sample solution, resolution of racemic mixtures in a sample solution, and purification, and concentration of target compounds.
专利号:US-2008070274-A1
优先权日:2001-12-10
标 题 :High capacity, methods for separation, purification, concentration, immobilization and synthesis of compounds and applications based thereupon
发明人:LEE WILLIAM; SAITO KYOICHI
权利人:LEE WILLIAM; SAITO KYOICHI
摘要:Compositions are provided herein comprising a base material having engrafted polymer brushes. The polymer brushes further comprise one or more functional groups immobilized along the surface of the brushes in a plurality of layers, which confer functional properties to the base material compositions. Methods of using these compositions include deoxygenation of a sample solution, hydrolysis of denaturing agents in a sample solution, resolution of racemic mixtures in a sample solution, and purification, and concentration of target compounds.
专利号:EP-1572363-A4
优先权日:2001-04-20
标题:HIGHLY EFFICIENT METHODS OF SEPARATION, PURIFICATION, CONCENTRATION, IMMOBILIZATION AND SYNTHESIS OF COMPOUNDS AND APPLICATIONS BASED ON SAID METHODS
专利号:JP-2005502321-A
优先权日:2001-04-20
标 题 :High volume methods for the separation, purification, concentration, immobilization and synthesis of compounds and applications based on them
专利号:JP-2009148276-A
优先权日:2001-04-20
标题 :High volume methods for the separation, purification, concentration, immobilization and synthesis of compounds and applications based on them
专利号:CN-107827693-A
优先权日:2017-11-09
标 题:Graphene-supported palladium/platinum catalyzed sp3C-H bond coupling method for synthesis of 1,2-diphenylethane derivatives