正癸基二甲基硅烷置于四氯化碳,Palladium Dichloride体系中,化学反应 2.0H,以82.8%的收率获得癸基二甲基氯硅烷 参考文献:Trialkylsilylethynyl-Substituted Triphenylenes And Hexabenzocoronenes: Highly Soluble Liquid Crystalline Materials And Their Hole Transport Abilities 标题:Trialkylsilylethynyl-Substituted Triphenylenes And Hexabenzocoronenes: Highly Soluble Liquid Crystalline Materials And Their Hole Transport Abilities 摘要:Four Triphenylene (Tp) And Four Hexa-Peri-Hexabenzocoronene (Hbc) Derivatives With Trialkylsilylethynyl Groups Were Prepared And Characterized By Differential Scanning Calorimetry,Polarizing Optical Microscopy,And X-Ray Diffraction Measurements. All Compounds Were Highly Soluble In Less-Polar Organic Solvents And Exhibited A Columnar Phase,Col(H) Or Col(R) For The Tps,And Col(H) For The Hbcs. The Hole Transport Ability In The Hbcs' Columnar Phase,0.4-1.5X10(-3) Cm(2) V-1 S(-1) At 40-180 Degrees C,And Its Temperature Dependence Were Determined By The Time-Of-Flight Method Using A Solution Technique. (C) 2015 Elsevier Ltd. All Rights Reserved. Doi:10.1016/j.Tet.2015.05.071
专利号:US-11033507-B2 优先权日:2013-12-19 标 题 :Method of synthesis of silica vesicles and use thereof 发明人:YU CHENGZHONG; MITTER NEENA; ZHANG JUN 权利人:UNIV QUEENSLAND 摘要:The invention relates, in part, to a method of producing silica vesicles including under controlled conditions to thereby heavily influence the morphology and characteristics of the vesicles. The vesicles are shown to be effective as delivery agents for chemical and biological agents. They are also shown to be useful in methods of treatment and as components of an immunogenic composition.
专利号:US-2022355262-A1 优先权日:2019-07-22 标题 :System and method for manufacturing water-based hydrophobic aerogels and aerogel composites 发明人:SACHITHANADAM MAHESH; KHORASGANI SOGHRATI ELMIRA; NATARAJAN GAYATHRI 权利人:KROSSLINKER PTE LTD 摘要:Embodiments of the present invention provide users with a system and method for manufacturing water-based hydrophobic aerogels and aerogel composites. The system and method can be carried out in a manner which is more rapid than typical ways and can be readily scalable. The method of manufacture is useful for producing water based hydrophobic aerogels and aerogel composites on a large scale with good homogeneity and consistency. Advantageously, the method of manufacture also has the benefit of a shorter processing time due to the vacuum homogenizing and mixing processes, the use of microwave assisted vacuum freeze drying for ease of synthesis of water-based hydrophobic aerogels.
专利号:US-2018193278-A1 优先权日:2013-12-19 标题 :Method of synthesis of silica vesicles and use thereof
专利号:US-9416147-B2 优先权日:2014-04-03 标题 :Preparation of silazane compound 发明人:TONOMURA YOICHI; KUBOTA TOHRU 权利人:SHINETSU CHEMICAL CO 摘要:A silazane compound useful as synthesis intermediates for paint additives, polymer modifiers, pharmaceuticals and agricultural chemicals is efficiently prepared by reaction of a halosilane compound with an amino-containing compound in a solvent which is the same silazane compound as the target product.
专利号:CN-105980447-A 优先权日:2013-12-19 标题:Synthesis method and application of silica vesicle