CAS: 50816-19-8; 8-Bromooctan-1-Ol

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17696-11-6 29823-21-0 26825-92-3

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8-溴辛酸置于indium(Iii) Bromide,1,1,3,3-四甲基二硅氧烷,1,2,3-三甲氧基丙烷体系中,化学反应 24.0H,以95%的收率获得产物8-溴-1-辛醇
参考文献:1,2,3-三甲氧基丙烷,基于甘油 溶剂 毒性低:新的用途可减少 腈,硝基的,酯以及带有tmds和金属催化剂的酸官能团
标题:1,2,3-三甲氧基丙烷,基于甘油 溶剂 毒性低:新的用途可减少 腈,硝基的,酯以及带有tmds和金属催化剂的酸官能团
摘要:1,2,3-三甲氧基丙烷 (1,2,3-Tmp)由 甘油通过相转移催化,一步一步即可获得非常好的收率和选择性.根据oecd指南,对该化合物进行了毒性研究.结果表明,1,2,3-Tmp在水生环境中具有低急性毒性,无皮肤致敏性,无诱变性和无生态毒性.该化合物还用作溶剂 用于减少有机功能 氢化铝 或者 1,1,3,3-四甲基二硅氧烷 (tmds)为良性 氢化物资源.尤其是减少排放量的新方法.腈 到 胺类 使用tmds与 三氟甲磺酸铜(cu(otf)2).
DOI:10.1039/c3Gc41082J

专利信息

专利号:US-7556743-B2
优先权日:2006-03-06
标 题 :Nanocomposites and methods for synthesis and use thereof
发明人：FURMAN BENJAMIN R; WELLINGHOFF STEPHEN T; THOMPSON PAUL M; RAWLS H RALPH
权利人:SOUTHWEST RES INST; UNIV TEXAS
摘要:Nanocomposite compositions and methods of synthesis of the compositions are described. In particular, liquid crystal-functionalized nanoparticles, liquid crystal-templated nanoparticles, nanocomposite compositions including the nanoparticles, and composite compositions including the nanocomposites are detailed.

专利号:US-4912253-A
优先权日:1988-06-06
标题 :Method for the preparation of an unsaturated alcohol or ester thereof
发明人：FUKUMOTO TAKEHIKO; YAMAMOTO AKIRA
权利人:SHINETSU CHEMICAL CO
摘要:An efficient method is proposed for the synthesis of an unsaturated alcohol of the general formula R--CHâ•?CH(CH 2 ) n+1 OH, in which R is a hydrogen atom or a monovalent hydrocarbon group having 1 to 10 carbon atoms and the subscript n is an integer in the range from 3 to 10, in which an acetate of the formula R--CHâ•?CHCH 2 OCOCH 3 is subjected to a coupling reaction with a Grignard reagent of the formula X 1 Mg(CH 2 ) n OMgX 2 , in which X 1 and X 2 are each a halogen atom, and then the reaction product is hydrolyzed. When the reaction product of the coupling reaction is reacted with acetic anhydride instead of hydrolysis, the corresponding acetate can readily be obtained. These unsaturated alcohols and acetates form a class of important biologically active compounds or intermediates thereof including sex pheromone compounds of insects.

专利号:WO-2010115869-A1
优先权日:2009-04-03
标 题 :Propofol phosphonyl derivatives, synthesis, and use in long acting formulations
发明人：GONNISSEN YVES RENE JOHANNA PAUL
权利人:SEPS PHARMA N V; GONNISSEN YVES RENE JOHANNA PAUL
摘要:This invention relates to compounds represented by the structural formula (I), and the salts and stereoisomers thereof, wherein: - L is a linker selected from the group consisting of -(CH 2 ) P -O-, a single bond, formula (IA), -(CH 2 ) 1-8 -O-X(O)-, and - p is an integer from 1 to 8, - each R 3 and each R 4 is independently selected from the group consisting of C 1-20 alkyl, C 3-12 alkyl, C 3-12 cycloalkyl-C 1-4 alkyl, saturated heterocyclyl and saturated heterocyclyl-C 1-4 alkyl, and - X and Y are each independently C or S(O), - Z is selected from the group consisting of O, S(O) and NR 5 , - W is selected from the group consisting of halogen, OH, S(O)H and O - M + wherein M + is a monovalent cation; and - R 5 is selected from the group consisting of hydrogen and C 1-10 alkyl. These compounds are useful pharmaceutical agents with improved oral bioavailability.

专利号:US-5968736-A
优先权日:1992-10-01
标 题 :Methods for recording the reaction history of a solid support
发明人：STILL W CLARK; WIGLER MICHAEL H; OHLMEYER MICHAEL H J; DILLARD LAWRENCE W; READER JOHN C
权利人:COLD SPRING HARBOR LAB; UNIV COLUMBIA
摘要:Encoded combinatorial chemistry is provided, where sequential synthetic schemes are recorded using organic molecules, which define choice of reactant, and stage, as the same or different bit of information. Various products can be produced in the multi-stage synthesis, such as oligomers and synthetic non-repetitive organic molecules. Conveniently, nested families of compounds can be employed as identifiers, where number and/or position of a substituent define the choice. Alternatively, detectable functionalities may be employed, such as radioisotopes, fluorescers, halogens, and the like, where presence and ratios of two different groups can be used to define stage or choice. Particularly, pluralities of identifiers may be used to provide a binary or higher code, so as to define a plurality of choices with only a few detachable tags. The particles may be screened for a characteristic of interest, particularly binding affinity, where the products may be detached from the particle or retained on the particle. The reaction history of the particles which are positive for the characteristic can be determined by the release of the tags and analysis to define the reaction history of the particle.

专利号:WO-2024230844-A1
优先权日:2023-05-11
标 题:Cationic lipids and preparation method thereof
发明人：MASHIACH ROI
权利人:RIBOX THERAPEUTICS HK LTD
摘要:The present invention provides cationic lipids and lipid nanoparticle formulations comprising these lipids, alone or in combination with other lipids. These lipid nanoparticles may be formulated with nucleic acids to facilitate their intracellular delivery both in vitro and for therapeutic applications. The present invention also provides methods of chemical synthesis of these lipids.

专利号:CN-117756720-A
优先权日:2023-12-18
标 题 :Polymerizable quaternary ammonium salt antibacterial agent and its preparation and application in the synthesis of antibacterial polyester