CAS: 4151-97-7; 1-Chloro-3-Methoxypropan-2-Ol

该化合物是一种多用途氯氢醚化合物,可应用于有机合成和专门化工制造,其双功能结构以丙醇骨干上的氯和甲氧基为主,使它成为生产药品,农用化学品和精美化学物的宝贵中间体.该化合物在核生殖替代和醚化反应中表现出良好的回动性,允许有选择地修改.它在普通有机溶剂中的平衡极性和溶性促进了合成工艺的处理.这两个反应场所的存在都允许连续功能化,在多步合成中提供了灵活性.由于具有卤化性质,需要适当的处理,但在标准条件下的稳定性确保了受控制环境中的可靠性能.

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上下游产品

CAS号107-05-1 氯丙烯 | CAS号67-56-1 甲醇 | CAS号106-89-8 环氧氯丙烷 | CAS号1634-04-4 甲基叔丁基醚 | CAS号623-39-2 3-甲氧基-1,2-丙二醇 | CAS号1072-61-3 1,3-Dioxolane,4... | CAS号930-37-0 (甲氧基甲基)环氧乙烷 | CAS号1000801-77-3 1-甲氧基-3-(4-(4,4... | CAS号168431-71-8 1-azido-3-metho... | CAS号13635-03-5 3-hydroxy-4-met... | CAS号86027-01-2 1H-Imidazole-1-... | CAS号53171-80-5 1-chloro-3-(1-c... | CAS号62312-90-7 1-(dimethylamin... | CAS号62042-94-8 1-methoxy-3-pro... | CAS号62042-97-1 1-butylsulfanyl...

合成工艺路线路线简述

    📜3-甲氧基-1,2-丙二醇置于盐酸体系中,化学反应生成 1-氯-3-甲氧基-2-丙醇
    参考文献:Malinowskii; Wwedenskii,Ukrainskij Khimicheskij Zhurnal,1957,Vol. 23,P. 626
    标题:Malinowskii; Wwedenskii,Ukrainskij Khimicheskij Zhurnal,1957,Vol. 23,P. 626

    海关参考信息

    专利信息


    专利号:US-10968308-B2
    优先权日:2017-11-07
    标 题 :Preparation method of epoxy compound having alkoxysilyl group, epoxy compound having alkoxysilyl group, composition comprising the same, and use thereof
    发明人：CHUN HYUN AEE; KIM YUN JU; PARK SOOK YEON; PARK SU JIN
    权利人:KOREA INST IND TECH
    摘要:Provided are a preparation method of an epoxy compound having an alkoxysilyl group in which an increase in the epoxy equivalent weight (EEW) of the epoxy compound is minimized because alkoxysilylation occurs through a simple one-step reaction using a hydroxyl group formed during the synthesis of the epoxy compound, an epoxy compound having an alkoxysilyl group prepared by the method, a composition comprising the same, and a use thereof. The method includes the reaction of an epoxy compound having a hydroxyl group with an isocyanate alkoxysilane in the presence of amine-based base catalyst, wherein the epoxy compound having an alkoxysilyl group has a mole ratio of [epoxide group]:[alkoxysilyl group] of n:1 ranging from 2:1 to 10:1, and an EEW increase of the epoxy compound having an alkoxysilyl group is less than 260/n. The epoxy compound has good physical properties when being cured.

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    合成参考文献


    参考文献:10.1007/s13233-013-1074-x
    摘要:Cho B, Noh S. Synthesis and thermal properties of ferrocene-modified poly(epichlorohydrin-co-2-(methoxymethyl)oxirane). Macromolecular Research. 2012 Nov 28;21(2):221–7. doi: 10.1007/s13233-013-1074-x.
    参考文献:10.1134/s1070427209110160
    摘要:Danov SM, Sulimov AV, Sulimova AV. Influence of synthesis conditions of titanium-containing zeolite on its catalytic activity in epoxidation of allyl chloride with hydrogen peroxide in methanol medium. Russian Journal of Applied Chemistry. 2009 Nov;82(11):1991. doi: 10.1134/s1070427209110160.
    参考文献:10.1007/s00003-022-01368-y
    摘要:Korte R, Goldbeck C, Bernsmann B, Schmissas D. Release of chloropropanols 3-MCPD and 1,3-DCP from kid’s toy products made of paper and cardboard. Journal of Consumer Protection and Food Safety. 2022 Feb 26;17(2):155–61. doi: 10.1007/s00003-022-01368-y.
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