CAS: 1829-28-3; Ethyl 2-Iodobenzoate

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📜苯甲酸乙酯置于(2,2,6,6-Tetramethylpiperidido)2Ag(Cn)Li2,碘体系中,用 四氢呋喃 用作溶剂,化学反应 5.0H,以93%的收率获得2-碘苯甲酸乙酯,
参考文献:Lipshutz型双(酰胺)银盐用于定向邻苯二甲酸酯化
标题:Lipshutz型双(酰胺)银盐用于定向邻苯二甲酸酯化
摘要:双(酰胺基)银盐(tmp)2 Ag(cn)li 2(3,Tmp-Ag-酸盐; Tmp = 2,2,6,6-四甲基哌啶子基)被设计为通过空前的定向原位化学键进行化学选择性芳族官能化的工具(d O Ag).X射线晶体学分析表明3具有与相应的lipshutz铜酸盐类似的结构.D ø具有这种tmp-Ag-酸酯的ag在具有高化学选择性和与各种官能团相容性的工艺中,以高收率提供了多官能芳烃.这些包括对有机金属和过渡金属敏感的取代基,例如甲酯,醛,乙烯基,碘,(三氟甲磺酰基)氧基和硝基.白蚁类药物与各种亲电试剂显示出非常好的反应性.硫属元素(s,Se和te)的安装和偶氮偶合反应也有效进行.
Doi:10.1039/c9Sc06060J

专利信息

专利号:US-7122694-B2
优先权日:1998-11-06
标 题 :Hydroboronation process
发明人：MARCUCCIO SEBASTIAN MARIO; RODOPOULOS MARY; WEIGOLD HELMUT
权利人:BORON MOLECULAR PTY LTD
摘要:The invention relates to processes for the synthesis of aryl or alkene borates which comprises reacting: (i) an olefinic compound having a halogen or halogen-like substituent in a vinylic substitution position, or (ii) an aromatic ring having a halogen or halogen-like substituent in a ring substitution position, with a disubstituted monohydroborane in the presence of a Group 8-11 metal catalyst. The invention also relates to the use of these borates in coupling reactions. The invention further relates to certain disubstituted monohydroboranes and aryl or alkene borates.

专利号:CN-118359493-A
优先权日:2024-04-18
标题:Synthesis method of 9,10-anthraquinone and synthesis method of 9,10-diethoxyanthracene