CAS: 1664-40-0; N-Phenylethylenediamine

该化合物是一种二胺化合物,具有芳香和脂态的两种功能.其结构包括一个苯基组和一个灵活的乙烯联系器,使其在有机合成中成为多功能中间体,特别是用于制备镀层,结壳,药品和特殊聚合物.该化合物的双重矿物质组可以有选择的再活性,有利于催化和协调化学的应用.在标准条件下和与普通溶剂兼容性下,其稳定性提高了其在实验室和工业环境中的效用.N1-苯乙烷-12-二二甲胺因其在合成复杂的分子结构中所起的作用而得到精确的估价.

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合成工艺路线路线简述

    N,N-Dibenzyl-N'-Phenyl-Ethylenediamine置于钯,溶剂黄146体系中,化学反应生成N-苯基乙二胺
    参考文献:De550762
    标题:De550762

    海关参考信息

    专利信息


    专利号:WO-0140193-A1
    优先权日:1999-12-03
    标题:Method for the synthesis of pyrazolines
    发明人:BOLDI ARMEN M
    权利人:CHEMRX ADVANCED TECHNOLOGIES I; BOLDI ARMEN M
    摘要:The present invention provides a method for the synthesis of compounds of Formula (I). Also claimed are novel intermediates and their methods of synthesis.

    专利号:US-2002103381-A1
    优先权日:2000-11-30
    标 题 :Method for the synthesis of pyrazolines
    发明人:BOLDI ARMEN M
    摘要:The present invention provides a method for the synthesis of compounds of Formula I: n n n Also claimed are novel intermediates and their methods of synthesis.

    专利号:US-2013102730-A1
    优先权日:2010-04-02
    标 题:Polyamine-containing polymers and methods of synthesis and use
    发明人:JOST ROBERT W; ULUDAG HASAN; BOLUK MEHMET YAMAN
    权利人:JOST ROBERT W; ULUDAG HASAN; BOLUK MEHMET YAMAN; ALBERTA INNOVATES TECHNOLOGY FUTURES
    摘要:The present invention relates to polyamine-containing polymers and methods of their synthesis and use. The polymer may be hydroxyethylcellulose, dextran, poly(vinyl alcohol) or poly(methyl acrylate).

    专利号:US-2024279231-A1
    优先权日:2021-05-20
    标题:Map4k4 inhibitors and methods of synthesis and use thereof
    发明人:AWASTHI VIBHUDUTTA; EEDA VENKATESWARARAO
    权利人:UNIV OKLAHOMA
    摘要:The compound DMX-5804, IUPAC name 5-(4-(2-methoxyethoxy)phenyl)-7-phenyl-3,4a,7,7a-tetrahydro-4H-pyrrolo[2,3-d]pyrimidin-4-one, is a potent and selective inhibitor of mitogen-activated protein kinase kinase kinase kinase-4 (MAP4K4). The present disclosure describes a scalable and practical synthesis process for making DMX-5804. The process (1) doesn't rely on transition metals, (2) has reduced duration of reactions, (3) is streamlined with significantly improved yields using low cost raw materials, (4) includes no microwave-assisted reactions, (5) does not require column purification, and (6) generally results in crystalized products having over a 95% purity in each step. The present disclosure also describes DMX-5804 analogs and derivatives for use in inhibiting MAP4K4, and scalable and practical processes for making such DMX-5804 analogs.

    专利号:US-7968075-B2
    优先权日:2009-03-04
    标 题:Multi-element metal chalcogenide and method for preparing the same
    发明人:CHUNG JUN-WEN
    权利人:HELIOHAWK OPTOELECTRONICS CORP
    摘要:A multi-element metal chalcogenide and a method for preparing the same are provided. The multi-element metal chalcogenide includes multiple metal elements. A multi-element metal chalcogenide powder is prepared, and all of the multiple metal elements of the multi-element metal chalcogenide are derived from at least one of simple substance powders of the metal elements and one or more alloy powders mixed in accordance with a mole ratio. A solution phase synthesis of the powder of the multi-element metal chalcogenide is then conducted under normal pressure to prepare the multi-element metal chalcogenide. The multi-element metal chalcogenide can be coated to obtain a film or used to make a target and then bombard the target for sputtering a film. In such a way, a selenization process which is conventional in fabricating the semiconductor solar cell is eliminated, thus improving production yield and efficiency.

    专利号:US-8003785-B2
    优先权日:2008-06-18
    标 题 :Halo-substituted pyrimidodiazepines
    发明人:CAI JIANPING; CHEN SHAOQING; CHU XIN-JIE; LUK KIN-CHUN; MISCHKE STEVEN GREGORY; SUN HONGMAO; WOVKULICH PETER MICHAEL
    权利人:TAKEDA PHARMACEUTICAL
    摘要:The present invention provides PLK1 inhibitor compounds of formula I: n nuseful in the treatment or control of cell proliferative disorders, particularly oncological disorders. These compounds and formulations containing such compounds may be useful in the treatment or control of solid tumors, such as, for example, breast, colon, lung and prostate tumors and other oncological diseases such as non-Hodgkin's lymphomas. Also provided are intermediate compounds useful in the synthesis of compounds of formula I.
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    合成参考文献


    摘要:A. E. Frost and A. A. Carlson. J. Org. Chem. 24, 1581 (1959).
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