CAS: 929-77-1; Methyl Docosanoate

该化合物是一种该化合物是一种白色,蜡状的固体,其特点是熔点和稳定性高;该化合物因其定义明确的保留特性,被广泛用作气体色谱学的参考标准;它还作为表面活性剂,润滑剂和热剂合成的中间体;甲基乙酸具有低挥发性,氧化性稳定极佳,适合高温应用;其生物兼容性和无毒性进一步支持其在化妆和制药配方中的使用.

结构式图片

物理性质

MSDS等安全信息

欧盟法规

ECHA物质C&L通报REACH预注册

上下游产品

diazomethane n-d°Cosanoic acid methanol 13-d°Cosenoic acid methyl ester22-tritetracontanone 1,1-Diphenyl-1-d°Cosen n-d°Cosanoic acid 1-d°Cosanol

合成工艺路线路线简述

  • 合成目标产物 Behenic Acid Methyl Ester 主要起始原料 Docosanoic Acid And Dimethyl Carbonate
  • 112-85-6 = 929-77-1
    反应条件:1.1 Reagents: Hydrochloric Acid Solvents: Water; 3 H,Reflux
    标题:Polyamide Compositions With Improved Thermo-Oxidative,Anti-Bacterial,Light- Or Energy Active Properties And Method For Producing Same
    参考文献:World Intellectual Property Organization]

    1120-34-9 = 929-77-1
    反应条件:1.1 Reagents: Hydrogen Catalysts: Palladium Chloride,2-(2-Methoxyethoxy)-N,N-Bis[2-(2-Methoxyethoxy)Ethyl]Ethanamine Solvents: Dichloromethane
    标题:Hydrogenation Catalyzed By Palladium Or Rhodium Chlorides In The Presence Of Tda-1
    作者:Villemin,Didier; Letulle,Marguerite
    参考文献:Synthetic Communications 日期:1989 卷标:19(16) 页码:2833-9]

    112-85-6 = 929-77-1
    反应条件:1.1 Catalysts: Zinc Oxide (Zno),Selenium; 3 H,65 °C
    标题:Role Of Oxygen Defects In Basicity Of Se Doped Zno Nanocatalyst For Enhanced Triglyceride Transesterification In Biodiesel Production
    作者:Rao,A. V. R. Krishna; Dudhe,Premansh; Chelvam,Venkatesh
    参考文献:Catalysis Communications 日期:2021 卷标:149]

    112-85-6 = 929-77-1
    反应条件:1.1 Catalysts: P-Toluenesulfonic Acid Solvents: Methanol; 24 H,Reflux
    标题:Long-Chain Syn-1-Phenylalkane-1,3-Diyl Diacetates,Related Phenylalkane Derivatives,And Sec-Alcohols,All Possessing Dominantly Iso-Branched Chain Termini,And 2/3-Methyl-Branched Fatty Acids From Primula Veris L. (Primulaceae) Wax
    作者:Radulovic,Niko S.; Zivkovic Stosic,Milena Z.
    参考文献:Phytochemistry (Elsevier) 日期:2021 卷标:186]

    112-85-6 = 929-77-1 [标题:Reaction Conditions
    标题:Improved Protocol Toward 1,3,4-Oxadiazole-2(3H)-Thiones And Scale-Up Synthesis In The Presence Of Sds As A Micelle Promoted Catalyst
    作者:Yildirim,Ayhan
    参考文献:Acta Chimica Slovenica 日期:2015 卷标:62(2) 页码:473-478]

    112-85-6 = 929-77-1
    反应条件:1.1 Catalysts: 1H-Imidazolium,1-Hexadecyl-3-(3-Sulfopropyl)-,Tetracosa-μ-Oxododecaoxo[μ12-[ph...; 3 H,90 °C
    标题:Method For Preparing Fatty Acid Alkyl Ester Using Long Chain Alkyl Sulfonic Acid Functionalized Heteropoly Acid Salt As Catalyst
    参考文献:China]

    112-85-6 = 929-77-1
    反应条件:1.1 Reagents: Boron Trifluoride
    标题:Novel Long-Chain Anteiso-Alkanes And Anteiso-Alkanoic Acids In Antarctic Rocks Colonized By Living And Fossil Cryptoendolithic Microorganisms
    作者:Matsumoto,Genki I.; Friedmann,E. Imre; Watanuki,Kunihiko; Ocampo-Friedmann,Roseli
    参考文献:Journal Of Chromatography 日期:1992 卷标:598(2) 页码:266-76]

    112-85-6 = 929-77-1 [标题:Reaction Conditions
    标题:Capillary Gas Chromatography-Mass Spectrometry Of Unusual And Very Long-Chain Fatty Acids From Soil Oligotrophic Bacteria
    作者:Rezanka,T.; Zlatkin,I. V.; Viden,I.; Slabova,O. I.; Nikitin,D. I.
    参考文献:Journal Of Chromatography 日期:1991 卷标:558(1) 页码:215-21]

    112-85-6 = 929-77-1
    反应条件:1.1 Reagents: Hydrochloric Acid Solvents: Methanol
    标题:Determination Of Very-Long-Chain Fatty Acids In Plasma By A Simplified Gas Chromatographic-Mass Spectrometric Procedure
    作者:Caruso,U.; Fowler,B.; Erceg,M.; Romano,C.
    参考文献:Journal Of Chromatography 日期:1991 卷标:562(1-2) 页码:147-52]

    112-85-6 = 929-77-1
    反应条件:1.1 Reagents: Boron Trifluoride Solvents: Methanol
    标题:Occurrence Of Cis-6-Hexadecenoic Acid And Other Unusual Monounsaturated Fatty Acids In The Lipids Of Oceanic Particulate Matter
    作者:Nichols,Peter D.; Volkman,John K.; Everitt,David A.
    参考文献:Oceanologica Acta 日期:1989 卷标:12(4) 页码:393-403]

    112-85-6 = 929-77-1
    反应条件:1.1 Catalysts: Boron Trifluoride Solvents: Methanol; 4 Min,Rt -> 150 °C; 10 Min,20 Bar,150 °C; 10 Min,150 °C -> 50 °C
    标题:High-Throughput Experimentation Platform: Parallel Microwave Chemistry In Hplc/gc Vials
    作者:Damm,Markus; Kappe,C. Oliver
    参考文献:Journal Of Combinatorial Chemistry 日期:2009 卷标:11(3) 页码:460-468]

    112-85-6 = 929-77-1
    反应条件:1.1 Catalysts: Diiron Nonacarbonyl; 1 H,180 °C
    标题:Methylation Of Aliphatic And Aromatic Carboxylic Acids With Dimethyl Carbonate Under The Influence Of Manganese And Iron Carbonyls
    作者:Khusnutdinov,R. I.; Shchadneva,N. A.; Mayakova,Yu. Yu.
    参考文献:Russian Journal Of General Chemistry 日期:2018 卷标:88(1) 页码:15-19]

    112-85-6 = 929-77-1
    反应条件:1.1 Reagents: Hydrochloric Acid Solvents: Methanol,Water; 3 H,Reflux
    标题:Bioactive Polyester And Polyolefin Molding Compositions And Articles
    参考文献:Germany]

    112-85-6 = 929-77-1
    反应条件:1.1 Catalysts: Triethylamine; 5 H,160 °C
    标题:Methylation Of Mono- And Dicarboxylic Acids With Dimethyl Carbonate Catalyzed With Binder-Free Zeolite Nay
    作者:Khusnutdinov,R. I.; Shchadneva,N. A.; Mayakova,Yu. Yu.; Konovalova,Yu. S.; Khazipova,A. N.; Et Al
    参考文献:Russian Journal Of Organic Chemistry 日期:2017 卷标:53(2) 页码:163-168]

    112-85-6 = 929-77-1
    反应条件:1.1 Catalysts: Methanesulfonic Acid,Phosphinic Acid Solvents: Water; Rt -> 130 °C; 2 H,130 °C; 130 °C -> 80 °C1.2 Reagents: Potassium Hydroxide Solvents: Water; Neutralized,80 °C
    标题:Branched Polymeric Esterified Glycerylated Alkyl Glycosides Emulsifiers With Good Emulsification Effect
    参考文献:World Intellectual Property Organization]

    112-85-6 = 929-77-1 [标题:Reaction Conditions
    标题:Pitch Problems In Making Japanese Papers. Iii. Separation And Identification Of Acidic Components And Their Contribution To Speck Formation
    作者:Su,Yu Chang; Tachibana,Sanro; Sumimoto,Massashi
    参考文献:Journal Of The Faculty Of Agriculture 日期:1992 卷标:37(1) 页码:93-104]

    112-85-6 = 929-77-1 [标题:Reaction Conditions
    标题:Analysis For Anthropogenic And Biogenic Lipids In The Aerosol Of A Coastal Area In East Mediterranean Sea
    作者:Stephanou,Euripides G.
    参考文献:Fresenius' Journal Of Analytical Chemistry 日期:1991 卷标:339(10) 页码:780-4]

    112-85-6 = 929-77-1 [标题:Reaction Conditions
    标题:Gc/ftir Analysis Of Fatty Acid Methyl Esters
    作者:Doumenq,P.; Guiliano,M.; Bertrand,J. C.; Mille,G.
    参考文献:Applied Spectroscopy 日期:1990 卷标:44(8) 页码:1355-9]

    112-85-6 = 929-77-1 [标题:Reaction Conditions
    标题:Measurement Of The Metabolic Interconversion Of Deuterium-Labeled Fatty Acids By Gas Chromatography/mass Spectrometry
    作者:Rohwedder,William K.; Duval,Sandra M.; Wolf,Darhal J.; Emken,Edward A.
    参考文献:Lipids 日期:1990 卷标:25(7) 页码:401-5]

    112-85-6 = 929-77-1 [标题:Reaction Conditions
    标题:Gas Chromatographic Analysis And Gas Chromatographic-Mass Spectrometric Identification Of Components In The Cyclohexane-Extractable Fraction From Contaminated Sediment Samples
    作者:Remberger,Mikael; Hynning,Aake; Neilson,Alasdair H.
    参考文献:Journal Of Chromatography 日期:1990 卷标:508(1) 页码:159-78
📜次磷酸置于氢氧化钾,甲烷磺酸体系中,用 甲醇,水 作为反应溶剂,化学反应生成 山嵛酸甲酯
参考文献:Branched Polymeric Emulsifiers
标题:Branched Polymeric Emulsifiers
摘要:本发明涉及酯化的甘油化烷基葡糖苷以及制备该化合物的方法.所述的酯化的甘油化烷基葡糖苷具有一个或多个聚甘油基团和一个或多个酰基团,其中所有的一个或多个酰基团通过酯键位于一个或多个聚甘油基团上.已发现这些化合物在制备适用于个人护理,家庭护理,工业和机构,以及医疗保健应用的相稳定乳化剂和共乳化剂方面具有实用性.

海关参考信息

专利信息


专利号:WO-0009528-A1
优先权日:1998-08-13
标题:Lower alkyl ester recycling synthesis
发明人：KENNEALLY COREY JAMES; TROUT JAMES EARL; SARAMA ROBERT JOSEPH; HOWIE JOHN KEENEY
权利人:PROCTER & GAMBLE; KENNEALLY COREY JAMES; TROUT JAMES EARL; SARAMA ROBERT JOSEPH; HOWIE JOHN KEENEY
摘要:Process for synthesizing and purifying polyol fatty acids polyesters or other nondigestible fats selected from the group of esterified linked alkoxylated polyols and esterified epoxide extended polyols, in which unreacted lower alkyl ester is recovered from a reaction mixture and recycled for use in the synthesis of the nondigestible fat. The process includes the steps of reacting an excess of lower alkyl ester with polyol to esterify hydroxyl groups thereof and form polyol fatty acid polyester, separating at least a portion of the unreacted lower alkyl ester from the polyol fatty acid polyester, and recycling the separated unreacted lower alkyl ester for further reaction with polyol or partially esterified polyol. The recycled lower alkyl ester is substantially free of lower alkyl ester degradation reaction products, such as carbonyls and free fatty acids.

专利号:WO-2017105352-A1
优先权日:2015-12-18
标 题 :Synthesis of inorganic sio2 microcapsules containing phase change materials and applications therein
发明人：YANG JINGLEI; AN JINLIANG; YANG EN-HUA
权利人:UNIV NANYANG TECH
摘要:Disclosed herein are microcapsules that encapsulate a phase change material, where the microcapsules have a dual-core structure with a first shell being made of an organic polymeric material, in particular polyurea surrounded by a second inorganic material shell, in particular silica. Also disclosed herein is a process to manufacture said microcapsules and applications thereof.

专利号:WO-2008044544-A1
优先权日:2006-10-04
标题 :Fine particle of hydroxide and/or oxide and process for producing the same
发明人：HORIGUCHI SHINICHI; ARIZONO JYUNICHI; OOSHIMA YASUHIRO
权利人:NISSHIN SPINNING; HORIGUCHI SHINICHI; ARIZONO JYUNICHI; OOSHIMA YASUHIRO
摘要:Fine particles of a hydroxide and/or oxide which are produced by electrodialysis; and a process for producing the fine particles. A conductive liquid which is a poor solvent for the hydroxide and/or oxide to be generated in a synthesis chamber is used as a synthesis-chamber liquid. The synthesis chamber is used in combination with a desalting chamber separated from the synthesis chamber by a cation-exchange membrane, the desalting chamber being filled with an aqueous electrolyte solution containing metal ions as a raw material for the hydroxide and/or oxide. A voltage not lower than the theoretical water electrolysis voltage is applied to the chambers. The fine hydroxide and/or oxide particles, which are produced through electrodialysis, are reduced in equipment cost and production cost.

专利号:CN-104910009-A
优先权日:2015-06-25
标题 :A kind of method of ionic liquid catalyzed synthesis of pletil alcohol ester

专利号:EP-1047659-B1
优先权日:1997-11-10
标题:A process for making high purity fatty acid lower alkyl esters
发明人：KENNEALLY COREY JAMES; BUSCH GARY ALLEN; GANSMULLER ERICH WILLIAM
权利人:PROCTER & GAMBLE
摘要:Processes for the synthesis of high purity fatty acid lower alkyl esters comprise the steps of: (a) converting a fatty acid source to a product mixture comprising lower alkyl esters and by-products; (b) water-washing the product mixture at elevated temperature and elevated pressure to remove by-products; and (c) fractionally distilling the water-washed product mixture to obtain high purity fatty acid lower alkyl esters. At least a portion of the fatty acids have from about 20 to about 24 carbon atoms. The high purity lower alkyl esters have an acid value no greater than about 1.0.

专利号:CN-105218369-B
优先权日:2014-05-29
标 题 :A new method for the synthesis of a class of brominated unsaturated fatty acid esters

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合成参考文献


摘要:S13 | EUCOSMETICS | Combined Inventory of Ingredients Employed in Cosmetic Products (2000) and Revised Inventory (2006) | DOI:10.5281/zenodo.2624118
参考文献:10.1016/j.phytochem.2005.10.012
摘要:Szafranek BM, Synak EE. Cuticular waxes from potato (Solanum tuberosum) leaves. Phytochemistry. 2006 Jan;67(1):80–90. doi: 10.1016/j.phytochem.2005.10.012.
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