五氯化铌置于mg,Al体系中,用 Neat (No Solvent) 用作溶剂,化学反应生成碳化铌 参考文献:Gmelin Handbuch Der Anorganischen Chemie,Gmelin Handbook: Nb: Mvol.B1,88,Page 188-190 标题:Gmelin Handbuch Der Anorganischen Chemie,Gmelin Handbook: Nb: Mvol.B1,88,Page 188-190
专利信息
专利号:US-12275713-B1 优先权日:2023-10-30 标题:Method for preparing 5-hydroxymethylfurfural 发明人:XU HAI; XU QIANG; YU SANXI; LI XINGLONG 权利人:HEFEI LEAF BIOTECH CO LTD 摘要:The application discloses a method for preparing 5-hydroxymethylfurfural and belongs to the technical field of synthesis of 5-hydroxymethylfurfural, mainly using biomass sugar as raw material and catalyzing the sugar to prepare 5-hydroxymethylfurfural in a tubular reactor filled with catalyst particles. In the application, the preparation of the humin-supported Sn catalyst is simple and has mild reaction conditions; the catalyst, as a high value-added product of humin, has good catalytic efficiency; the preparation of 5-hydroxymethylfurfural using the catalyst has the advantages of high yield, low cost and the like; the tubular reactor adopted can reduce backmixing, greatly shorten the reaction time and reduce the generation of humin and can also be equipped with inline monitoring equipment to monitor the preparation of HMF in a timely manner. Therefore, the application has the advantages of simple process, low energy consumption, high yield, cost saving, and the like.