CAS: 106-92-3; Allyl Glycidyl Ether

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烯丙基醚置于双氧水,C15H18N9(3+)*3O5S(2-)*3H(1+)体系中,用98%的收率获得烯丙基缩水甘油醚
参考文献:在温和条件下使用催化 Taim[x] (X = Wo42-,Hso5-) 可回收离子液体,超声波促进无金属均相烯烃环氧化和烯烃直接转化为环状碳酸酯
标题:在温和条件下使用催化 Taim[x] (X = Wo42-,Hso5-) 可回收离子液体,超声波促进无金属均相烯烃环氧化和烯烃直接转化为环状碳酸酯
摘要:制备了taim[wo 4 ]和taim[hso 5 ]离子液体,作为高效溶剂和可回收催化剂,用于烯烃的温和环氧化以及超声辐射下烯烃多米诺制备环状碳酸酯.h 2 O 2为催化剂氧化剂.通过各种分析方法(包括 Ftir,Edx,粘度和密度测量)研究了离子液体的物理性质和结构.各种烯烃(无论是脂肪族还是芳香族类型)的环氧化物以及环状和末端烯烃在低co 2(G) 压力(~1 Atm.)下转化为环状碳酸酯均获得了高至优异的收率.中度co 2(G)发现在离子液体中的溶解度.此外,所有烯烃都获得了优异的环氧化物选择性.该方法的可扩展性证明了具有前景的克级烯烃环氧化的直接可扩展性,且效率损失最少.Taim[wo 4 ]和taim[hso 5 ]离子液体可以通过简单的溶剂-溶剂萃取从均质混合物中回收,并重复使用至少几次,活性损失微乎其微.
Doi:10.1016/j.Inoche.2023.110944

专利信息

专利号:US-7994359-B2
优先权日:2004-02-13
标题:Process for the synthesis of (7-methoxy-1-naphthyl) acetonitrile and its application in the synthesis of agomelatine
发明人：SOUVIE JEAN-CLAUDE; BLANCO ISAAC GONZALEZ
权利人:SERVIER LAB
摘要:A process for the industrial synthesis of the compound of formula (I) n nApplication in the synthesis of agomelatine.

专利号:US-7999129-B2
优先权日:2004-02-13
标 题:Process for the synthesis of (7-methoxy-1-naphthyl) acetonitrile and its application in the synthesis of agomelatine
发明人：SOUVIE JEAN-CLAUDE; BLANCO ISAAC GONZALEZ
权利人:SERVIER LAB
摘要:A process for the industrial synthesis of the compound of formula (I) n nApplication in the synthesis of agomelatine.

专利号:WO-2023152730-A1
优先权日:2022-02-14
标题 :Amine-borane adducts in the synthesis of polyester and its copolymers using cyclic esters and compositions thereof
发明人：FENG XIAOSHUANG; LIU JINGJING; GNANOU YVES
权利人:UNIV KING ABDULLAH SCI & TECH
摘要:Embodiments of the present disclosure provide for the process of synthesis of polyester and its copolymers through (co)polymerization of cyclic esters and with other oxygenated monomers using amine-borane adduct. Embodiments of the present disclosure further describe the controlled anionic ring-opening polymerization of the cyclic compounds. Embodiments of the present disclosure also describe the polymerization of cyclic compounds using the synergistic effect of amines and thioureas. Embodiments of the present disclosure also describe compositions of polymers formed by the said process.

专利号:US-5606077-A
优先权日:1995-02-21
标 题:Method for the synthesis of organopolysiloxanes containing carbonate groups
发明人：LERSCH PETER; WEITEMEYER CHRISTIAN
权利人:GOLDSCHMIDT AG TH
摘要:The invention relates to a method for the synthesis of organopoiysiloxanes of the general formula which contains cyclic carbonate groups. The inventive compounds have a high polarity, can be synthesized easily and, because of their compatibility with polar media, find use as additives for dispersion paints or lacquers and for coating the surfaces of pigments and fillers.

专利号:US-8541571-B2
优先权日:2008-03-03
标题:Homogeneous synthesis of cellulose ethers in ionic liquids
发明人：MOELLMANN EUGEN; HEINZE THOMAS; LIEBERT TIM; KOEHLER SARAH
权利人:MOELLMANN EUGEN; HEINZE THOMAS; LIEBERT TIM; KOEHLER SARAH; SE TYLOSE GMBH & CO KG
摘要:The invention is directed to a simple and new method for the homogeneous synthesis of cellulose ethers. Ionic liquids are not only used as solvent, but also as reaction media for the homogeneous etherification of cellulose. The dissolved cellulose is treated with the etherification agent in the absence of organic and/or inorganic bases and in the absence and/or in the presence of moderate amounts of water. The obtained cellulose ethers show new distributions of substitution on the polymer chain, resulting in new properties and applications.

专利号:US-11753503-B2
优先权日:2018-05-17
标 题:Supported onium salts as initiators for the synthesis of polycarbonates by copolymerization of CO2 with epoxides
发明人：FENG XIAOSHUANG; PATIL NAGANATHA; LUCIANI CAROLINE; GNANOU YVES; HADJICHRISTIDIS NIKOS
权利人:UNIV KING ABDULLAH SCI & TECH
摘要:Supported onium salts used as initiators for the synthesis of polycarbonates by copolymerization of carbon dioxide with epoxides are described. Embodiments of the present disclosure describe initiators comprising an insoluble portion including an onium cation attached to an insoluble support; and an anion, wherein the anion is a counter-ion to the onium cation. Embodiments further describe methods of making polycarbonates using the initiator, methods of making initiators, and the like.