CAS: 628-96-6; 2-Nitrooxyethyl Nitrate

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CAS号75-21-8 环氧乙烷 | CAS号107-21-1 乙二醇 | CAS号54509-73-8 ethene | CAS号66329-10-0 1-nitritoethan-... | CAS号7697-37-2 硝酸 | CAS号137-40-6 丙酸钠 | CAS号624-76-0 2-碘-1-乙醇 | CAS号80-62-6 甲基丙烯酸甲酯 | CAS号67-64-1 丙酮 | CAS号3710-84-7 N,N-二乙基羟胺(DEHA) | CAS号119-61-9 二苯甲酮 | CAS号91-01-0 二苯甲醇 | CAS号632-50-8 對稱四苯乙烷 | CAS号100-52-7 苯甲醛

📜环氧乙烷置于dinitrogen Tetraoxide,臭氧体系中,化学反应生成 乙二醇二硝酸酯
参考文献:氮氧化物硝化,第1部分:应变环氧杂环与五氧化二氮的反应制备硝酸酯
标题:氮氧化物硝化,第1部分:应变环氧杂环与五氧化二氮的反应制备硝酸酯
摘要:环氧化物和氧杂环丁烷与五氧化二氮反应反应生成高或接近定量收率的相应二硝酸盐.简要讨论了该方法的范围和局限性.
DOI:10.1016/0040-4039(88)85272-9

专利信息

专利号:US-11001553-B1
优先权日:2020-10-22
标题:Process for the synthesis of 2-nitratoethyl acrylate (2NEA)
发明人：VACCARELLO DAVID N
权利人:US NAVY
摘要:An elegant process for the synthesis of 2-nitratoethyl acrylate is a single reactive step. A 2-hydroxyethyl acrylate having only one hydroxyl group is nitrated in a 1:1 volumetric mixture of nitric acid and sulfuric acid therein forming 2-nitratoethyl acrylate. The 2-nitratoethyl acrylate is minimally soluble in a quenched cold acid water mixture, which enables relatively easy isolation of about 96% purity 2-nitratoethyl acrylate at a yield of about 85%.

专利号:US-2003089435-A1
优先权日:2000-03-23
标题:Method of synthesizing diglycerol tetranitrate, and solid rocket motor propellant containing the same
发明人：SANDERSON ANDREW J; MARTINS LAURA J
摘要:Diglyercol tetranitrate is an energetic nitrate ester plasticizer having no freezing point, making the nitrate ester plasticizer especially suited for use in solid rocket motor propellants that are subjected to low temperature storage and operational environments, which can reach as low as −54° C. in temperature. In order to avoid problems associated with fume-off that characterize the conventional synthesis method of making diglycerol tetranitrate, synthesis is performed in a medium including a mixed acid phase and an inert organic phase. The mixed acid phase contains, as ingredients, at least one nitronium ion source and at least one acid having sufficient strength to generate nitronium ions from the nitronium ion source. The nitronium ions in the mixed acid nitrate diglycerol to form diglycerol tetranitrate, which is then received into the organic liquid. The organic liquid, which preferably is a chlorocarbon such as dichloromethane, is insoluble with diglycerol but soluble with diglycerol tetranitrate. The inert organic phase is then treated to neutralize any acid contained in the inert organic phase, and the diglycerol tetranitrate is separated from the inert organic phase.

专利号:WO-2006097348-A1
优先权日:2005-03-15
标 题:Use of agents such as nonpolymeric nitric oxide donors for making the lips full again and/or colouring the lips
发明人：CALS-GRIERSON MARIE-MADELEINE
权利人:OREAL; CALS-GRIERSON MARIE-MADELEINE
摘要:The invention relates in particular to the cosmetic use (i) of at least one agent for promoting the production of NO in and/or on the lips, chosen from nitric oxide NO donors or precursors; nonpolymeric NO releasers; and NO synthase synthesis and/or activity stimulators; or (ii) of other agents for promoting microcirculation in the skin, chosen from potassium channel openers; calcium channel blockers; phosphodiesterase inhibitors; flavonoids; vasodilator peptides that are not NO donors; temperature modulators; agents for promoting the stimulation and/or maintenance of angiogenesis; agents for promoting the stimulation of endothelial cell proliferation; agents for promoting endothelial cell migration; and mixtures thereof, in a makeup and/or care composition for the lips, as an agent for naturally making the lips full again and/or naturally coloring the lips. It also relates to specific care and/or makeup compositions for the lips containing said agent, and also to a cosmetic process aimed at making the lips naturally full and/or colored, using said compositions .

专利号:EP-4103640-B1
优先权日:2020-02-11
标 题 :New method of synthesis of chitosan derivatives and uses thereof
发明人：KARGAPOLOV YURIY; FOMENKO VLADISLAV
权利人:NOVOCHIZOL SA

专利号:US-2012108838-A1
优先权日:2009-09-24
标 题 :Synthesis of an energetic nitrate ester

专利号:US-2023096466-A1
优先权日:2020-02-11
标 题 :New method of synthesis of chitosan derivatives and uses thereof