📜对氨基苯磺酸置于硫酸,乙酸酐体系中,用 N-甲基乙酰胺,水 用作溶剂,化学反应生成4-乙酰氨基苯磺酸 参考文献:Process For The Preparation Of N-Acetylaminoarylsulfonic Acids In 标题:Process For The Preparation Of N-Acetylaminoarylsulfonic Acids In 摘要:这项发明涉及无盐n-乙酰氨基芳基磺酸,其通过用乙酸酐或乙酰氯,硫酸对乙酸酐或乙酰氯进行乙酰化制备,硫酸可以含有少量水和/或二甲基甲酰胺和/或n-甲基吡咯烷酮,作用作溶剂,并且利用n-乙酰氨基芳基磺酸制备它们的酸氯化物.
专利号:US-4207261-A 优先权日:1977-08-12 标题 :Process for preparing o-phenylenediamine 发明人:CSIKOS REZSO 权利人:MAGYAR ASVANYOLAJ ES FOELDGAZ 摘要:The invention relates to a process for preparing o-phenylenediamine. According to the invention 1,4-dichlorobenzene is nitrated to give 2,5-dichloro-nitrobenzene which is then reacted with an aqueous ammonium hydroxide solution and the 4-chloro-2-nitraniline obtained is subjected to catalytic hydrogenation to afford the end product which can thereafter be separated. n The process according to the invention can be accomplished with a total yield of about 90% related to the 1,4-dichlorobenzene starting compound. n o-Phenylenediamine is a valuable intermediate for instance in the synthesis of plant protecting agents and heat-resistant polymers.
专利号:CN-111392697-B 优先权日:2020-03-18 标题:A kind of treatment method of organic waste acid in the synthesis of para-acetamidobenzenesulfonyl chloride
专利号:CN-113952827-A 优先权日:2021-11-24 标题:A kind of treatment method of organic waste gas in the synthesis of p-acetamidobenzenesulfonyl chloride
专利号:US-7038043-B1 优先权日:1995-08-11 标 题:Glycosylated indolocarbazole synthesis 发明人:WOOD JOHN L; STOLTZ BRIAN M; DIETRICH HANS-JURGEN; PFLUM DEREK A 权利人:UNIV YALE 摘要:Indolocarbazoles are furanosylated (e.g., 7 ) with acetals (e.g., 8 ) or their open chain congeners (e.g., 9 ) under conditions known to promote acetal exchange or formation, such as protic or Lewis acids. Furanosylated indolocarbazoles (e.g., 10 ) are also prepared via ring contraction of pyranosylated indolocarbazoles (e.g., 11 ) under conditions know to effect oxidation and benzylic acid type rearrangements, and pyranosylated indolocarbazoles (e.g., 11 ) are prepared via ring expansion of the furanosylated congeners (e.g., 10 )
专利号:CN-111392697-A 优先权日:2020-03-18 标题 :Method for treating organic waste acid in synthesis of p-acetamido-benzenesulfonyl chloride
专利号:CN-216259951-U 优先权日:2021-11-24 标题:Processing apparatus of organic waste gas in synthesis of p-acetamido benzene sulfonyl chloride
参考文献:10.5281/zenodo.3827487 摘要:USEPA/Office of Pesticides and Toxic Substances; Simazine: Revised Preliminary HED Chapter of the Reregistration Eligibility Decision Document (RED), Document ID: EPA-HQ-OPP-2005-0151-0023 p.17-18 (May 31, 2005). Available from, as of June 6, 2007: 参考文献:10.1055/s-0028-1083600 摘要:Jang D, Kim J. Convenient One-Pot Synthesis of Sulfonyl Azides from Sulfonic Acids. Synlett. 2008 Oct 23;2008(18):2885–7. doi: 10.1055/s-0028-1083600.