CAS: 121-62-0; 4-Acetamidobenzenesulfonic Acid

该化合物是一种全氟辛烷磺酸芳香化合物,广泛用作有机合成和制药制造的中间体,其主要优点包括:在电子代用反应中具有高度的回活动性,使其对染料,药品和特殊化学品产生价值;全氟辛烷磺酸组增强了水溶剂和极地溶剂的溶性,便利了下游加工;乙胺基甲酸碱提供了稳定性,并指导了进一步的功能化,使化学精确的化学改造得以进行;该化合物还用于分析化学,因其明确特性而成为试剂;其一贯的纯度和可靠性能使它在需要受控消毒反应的工业和研究应用中成为首选.

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    CAS号103-84-4 N-乙酰苯胺 | CAS号121-57-3 对氨基苯磺酸 | CAS号103-88-8 4'-溴乙酰苯胺 | CAS号539-03-7 N-(4-氯苯基)乙酰胺 | CAS号248584-41-0 N-(4-((((3S,3aR... | CAS号463-51-4 乙烯酮 | CAS号515-74-2 对氨基苯磺酸钠 | CAS号108-24-7 乙酸酐 | CAS号121-60-8 对乙酰氨基苯磺酰氯 | CAS号69564-58-5 hexyl 4-acetami... | CAS号121-60-8 对乙酰氨基苯磺酰氯 | CAS号2158-14-7 4-乙酰氨基苯磺酰叠氮 | CAS号3989-50-2 N-[4-(hydrazine...

    合成工艺路线路线简述

      📜对氨基苯磺酸置于硫酸,乙酸酐体系中,用 N-甲基乙酰胺,水 用作溶剂,化学反应生成4-乙酰氨基苯磺酸
      参考文献:Process For The Preparation Of N-Acetylaminoarylsulfonic Acids In
      标题:Process For The Preparation Of N-Acetylaminoarylsulfonic Acids In
      摘要:这项发明涉及无盐n-乙酰氨基芳基磺酸,其通过用乙酸酐或乙酰氯,硫酸对乙酸酐或乙酰氯进行乙酰化制备,硫酸可以含有少量水和/或二甲基甲酰胺和/或n-甲基吡咯烷酮,作用作溶剂,并且利用n-乙酰氨基芳基磺酸制备它们的酸氯化物.

      海关参考信息

      专利信息


      专利号:US-4207261-A
      优先权日:1977-08-12
      标题 :Process for preparing o-phenylenediamine
      发明人:CSIKOS REZSO
      权利人:MAGYAR ASVANYOLAJ ES FOELDGAZ
      摘要:The invention relates to a process for preparing o-phenylenediamine. According to the invention 1,4-dichlorobenzene is nitrated to give 2,5-dichloro-nitrobenzene which is then reacted with an aqueous ammonium hydroxide solution and the 4-chloro-2-nitraniline obtained is subjected to catalytic hydrogenation to afford the end product which can thereafter be separated. n The process according to the invention can be accomplished with a total yield of about 90% related to the 1,4-dichlorobenzene starting compound. n o-Phenylenediamine is a valuable intermediate for instance in the synthesis of plant protecting agents and heat-resistant polymers.

      专利号:CN-111392697-B
      优先权日:2020-03-18
      标题:A kind of treatment method of organic waste acid in the synthesis of para-acetamidobenzenesulfonyl chloride

      专利号:CN-113952827-A
      优先权日:2021-11-24
      标题:A kind of treatment method of organic waste gas in the synthesis of p-acetamidobenzenesulfonyl chloride

      专利号:US-7038043-B1
      优先权日:1995-08-11
      标 题:Glycosylated indolocarbazole synthesis
      发明人:WOOD JOHN L; STOLTZ BRIAN M; DIETRICH HANS-JURGEN; PFLUM DEREK A
      权利人:UNIV YALE
      摘要:Indolocarbazoles are furanosylated (e.g., 7 ) with acetals (e.g., 8 ) or their open chain congeners (e.g., 9 ) under conditions known to promote acetal exchange or formation, such as protic or Lewis acids. Furanosylated indolocarbazoles (e.g., 10 ) are also prepared via ring contraction of pyranosylated indolocarbazoles (e.g., 11 ) under conditions know to effect oxidation and benzylic acid type rearrangements, and pyranosylated indolocarbazoles (e.g., 11 ) are prepared via ring expansion of the furanosylated congeners (e.g., 10 )

      专利号:CN-111392697-A
      优先权日:2020-03-18
      标题 :Method for treating organic waste acid in synthesis of p-acetamido-benzenesulfonyl chloride

      专利号:CN-216259951-U
      优先权日:2021-11-24
      标题:Processing apparatus of organic waste gas in synthesis of p-acetamido benzene sulfonyl chloride

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      ✅ COA系统入驻 | 共享模式

      合成参考文献


      参考文献:10.5281/zenodo.3827487
      摘要:USEPA/Office of Pesticides and Toxic Substances; Simazine: Revised Preliminary HED Chapter of the Reregistration Eligibility Decision Document (RED), Document ID: EPA-HQ-OPP-2005-0151-0023 p.17-18 (May 31, 2005). Available from, as of June 6, 2007:
      参考文献:10.1055/s-0028-1083600
      摘要:Jang D, Kim J. Convenient One-Pot Synthesis of Sulfonyl Azides from Sulfonic Acids. Synlett. 2008 Oct 23;2008(18):2885–7. doi: 10.1055/s-0028-1083600.
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