CAS: 13889-95-7; S-Tert-Butyl Chloromethanethioate

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CAS号75-44-5 光气 | CAS号75-66-1 叔丁基硫醇 | CAS号75-65-0 叔丁醇 | CAS号32315-10-9 三光气 | CAS号62603-67-2 S-tert-butyl N-...

📜S-Tert-Butyl O-Ethyl Carbonodithioate置于草酰氯体系中,用 乙腈 用作溶剂,化学反应 3.0H,以55%的收率获得s-叔丁基硫代氯甲酸酯
参考文献:来自黄原酸盐的 S-烷基氯硫代甲酸酯
标题:来自黄原酸盐的 S-烷基氯硫代甲酸酯
摘要:S-烷基 O-乙基黄原酸酯 (S-烷基 O-乙基二硫代碳酸酯) 与由 N-甲酰基吗啉 (Morpholine-4-Carbaldehyde) 原位生成的催化 Vilsmeier 试剂反应以非常好的收率获得 S-烷基氯硫代甲酸酯.
Doi:10.1055/s-2007-983756

专利信息

专利号:US-8202985-B2
优先权日:2005-10-31
标 题:Monomer compositions for the synthesis of polynucleotides, methods of synthesis, and methods of deprotection
发明人：DELLINGER DOUGLAS J; TIMAR ZOLTAN; SIERZCHALA AGNIESZKA; DELLINGER GERALDINO; CARUTHERS MARVIN H
权利人:DELLINGER DOUGLAS J; TIMAR ZOLTAN; SIERZCHALA AGNIESZKA; DELLINGER GERALDINO; CARUTHERS MARVIN H; AGILENT TECHNOLOGIES INC; UNIV COLORADO
摘要:Nucleotide monomers, polynucleotides, methods of making each, and methods of deprotecting each, are disclosed. An embodiment of the nucleotide monomer, among others, includes a nucleotide monomer having a heterobase protecting group selected from structures I through III as described herein. An embodiment of the polynucleotide, among others, includes a plurality of nucleotide moieties having a heterobase protecting group selected from one of structures I through III as described herein.

专利号:US-7759471-B2
优先权日:2005-10-31
标题 :Monomer compositions for the synthesis of RNA, methods of synthesis, and methods of deprotection
发明人：DELLINGER DOUGLAS J; TIMAR ZOLTAN; SIERZCHALA AGNIESZKA; DELLINGER GERALDINE; CARUTHERS MARVIN H
权利人:AGILENT TECHNOLOGIES INC; UNIV COLORADO
摘要:Nucleotide monomers, polynucleotides, methods of making each, methods of deprotecting each, and the like are disclosed herein.

专利号:US-2007100138-A1
优先权日:2005-10-31
标题:Monomer compositions for the synthesis of polynucleotides, methods of synthesis, and methods of deprotection

专利号:US-2007100136-A1
优先权日:2005-10-31
标题:Monomer compositions for the synthesis of RNA, methods of synthesis, and methods of deprotection

专利号:US-9067961-B2
优先权日:2007-05-10
标 题 :Thiocarbon-protecting groups for RNA synthesis
发明人：DELLINGER DOUGLAS J; SIERZCHALA AGNIESZKA B; TURNER JOHN; MYERSON JOEL; KUPIHAR ZOLTAN; FERREIRA FERNANDO; CARUTHERS MARVIN H; DELLINGER GERALDINE F
权利人:DELLINGER DOUGLAS J; SIERZCHALA AGNIESZKA B; TURNER JOHN; MYERSON JOEL; KUPIHAR ZOLTAN; FERREIRA FERNANDO; CARUTHERS MARVIN H; DELLINGER GERALDINE F; AGILENT TECHNOLOGIES INC; UNIV COLORADO DENVER
摘要:Aspects of the invention include 2′ protected nucleoside monomers that are protected at the 2′ site with thiocarbon protecting groups. Thiocarbon protecting groups of interest include thiocarbonate, thionocarbonate, dithiocarbonate groups, as well as thionocarbamate protecting groups. Aspects of the invention further include nucleic acids that include the protecting groups of the invention, as well as methods of synthesizing nucleic acids using the protecting groups of the invention.

专利号:EP-1792909-A1
优先权日:2005-10-31
标 题:Synthesis of polynucleotides