CAS: 6222-35-1; Cyclohexyl Propionate

上下游产品

CAS号123-62-6 丙酸酐 | CAS号108-93-0 环己醇 | CAS号105-37-3 丙酸乙酯 | CAS号637-27-4 丙酸苯酯 | CAS号54509-73-8 ethene | CAS号79-03-8 丙酰氯 | CAS号110-83-8 环己烯 | CAS号107-12-0 丙腈

📜丙酸酐,环己醇置于cl(1-)*c5H14No(1+)*3Zncl2体系中,用 Neat (No Solvent) 作为反应溶剂,化学反应 0.75H,以92%的收率获得产物丙酸环己酯
参考文献:一种以深共熔溶剂为催化剂酰化仲醇,酚和萘的高效,绿色方法
标题:一种以深共熔溶剂为催化剂酰化仲醇,酚和萘的高效,绿色方法
摘要:由氯化胆碱和氯化锌容易制备的典型深共熔溶剂[cholinecl] [zncl2] 3是绿色的,可用于用酸酐对仲醇,酚和萘进行酰化反应.
DOI:10.1039/c6Ra22757K

专利信息

专利号:US-8604219-B2
优先权日:2009-08-24
标题 :Method for synthesis of N-alkyl carbazole and derivatives thereof
发明人：GHARDA KEKI HORMUSJI
权利人:GHARDA KEKI HORMUSJI
摘要:Disclosed is a process for the preparation of N-alkyl carbazole. Said process comprises: a) chlorinating cyclohexanone to form 2-chlorocyclohexanone; b) reacting 2-chlorocyclohexanone with N-ethyl aniline to form 2-(N-ethyl anilino)cyclohexanone; c) cyclizing 2-(N-ethyl anilino) cyclohexanone by refluxing with simultaneous water removal to obtain 9-ethyltetrahydrocarbazole; d) treating 9-ethyl-tetrahydrocarbazole with concentrated hydrochloric acid followed by water wash for removing N-ethyl aniline; e) dehydrogenating 9-ethyltetrahydrocarbazole by heating 9-ethyltetrahydrocarbazole in a solvent, in presence of a catalyst to obtain N-alkyl carbazole.

专利号:US-5175146-A
优先权日:1989-12-05
标题 :Synthetic calcitonin peptides
发明人：BASAVA CHANNA; HOSTETLER KARL Y
权利人:VICAL INC
摘要:Synthetic hypocalcemic peptides which are similar in biological properties to native calcitonins as clinically useful agents. The peptides comprise analogues of native calcitonins having amino acid substitutions and deletions which act to improve potency, prolong duration of the hormonal effect, enhance receptor binding, and increase oral or nasal bioavailability. The calcitonin peptide analogues are less expensive and more easily synthesized than native calcitonins, and have improved resistance to inactivation or degradation. Methods are provided for the synthesis of these peptides. Also, disclosed are novel cyclic peptides, including calcitonin, having increased stability with respect to proteolysis. Methods for the synthesis of these peptides are provided, comprising converting disulfide cyclic peptides and proteins to enzymatically and chemically stable cyclic peptide structures by the replacement of cysteine residues with dicarboxylic acids and diamino acids. The method is applicable to various naturally occurring peptides, their synthetic analogues or derivatives, and proteins.

专利号:US-2012149915-A1
优先权日:2009-08-24
标题:Method for synthesis of n-alkyl carbazole and deriratives thereof

专利号:US-6878184-B1
优先权日:2002-08-09
标题 :Nanoparticle synthesis and the formation of inks therefrom
发明人：ROCKENBERGER JOERG; ZURCHER FABIO; HAUBRICH SCOTT; SLEIMAN NASSRIN
权利人:KOVIO INC
摘要:Methods for making metal-based nanoparticles and inks are disclosed. In accordance with the method of the present invention, molecular metal precursors are reduced in the presence of a reaction medium to form the nanoparticles. The molecular metal precursors are preferably reduced by heating the metal precursor in the medium, by adding a reducing agent, such an aldehyde or a combination thereof. Metal precursor are preferably metal oxides, transition metal complexes or combination thereof. The method of the present invention is used to make high yield nanoparticles with a range of particle size distributions. Nanoparticle formed by the present invention include mixtures of nanoparticle, alloy nanoparticles, metal core shell nanoparticles or nanoparticle comprising a single metal species.

专利号:WO-2011024186-A1
优先权日:2009-08-24
标题:Method for synthesis of n-alkyl carbazole and derivatives thereof

专利号:CN-85102572-A
优先权日:1985-04-01
标题 :Synthesis of Pineapple Ester Using 4-Vinylcyclohexene