CAS: 29046-78-4; Dichloronickel,1,2-Dimethoxyethane

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CAS号1033772-47-2 双[(2-二甲氨基)苯基]胺氯...

📜乙二醇二甲醚,Nickel(II) Chloride Hexahydrate置于原甲酸三乙酯体系中,化学反应 2.5H,以74%的收率获得氯化镍二甲氧基乙烷
参考文献:Nickel(II) Complexes With Imino-Imidazole Chelating Ligands Bearing Pendant Donor Groups (Sr,Or,Nr2,Pr2) As Precatalysts In Ethylene Oligomerization
标题:Nickel(II) Complexes With Imino-Imidazole Chelating Ligands Bearing Pendant Donor Groups (Sr,Or,Nr2,Pr2) As Precatalysts In Ethylene Oligomerization
摘要:New Imino-Imidazole Ligands Bearing A Pendant Donor Function L Were Synthesized In Excellent Yields. The Corresponding Nickel(II) Complexes [nicl2(Imino-Imidazole-L)](N) (L-(Ch2)(2)Sme (2A),(Ch2)(2)Ome (2B),(Ch2)(2)Net2 (2C),(Ch2)(2)Pph2 (2D),(C6H4)-P-Ome (2E),(Ch2)(3)Ome (2F),(Ch2)(3)Ch3 (2G); N = 1,2) Were Prepared And Characterized By Ft-Ir Spectroscopy And Elemental Analysis. Furthermore,The Coordination Geometry Around The Metal Center In The Dinuclear Complex 2A And The Mononuclear Complexes 2C And 2E Was Unambiguously Established By Single Crystal X-Ray Diffraction. All Complexes Have Been Evaluated For The Oligomerization Of Ethylene In The Presence Of Etalcl2 Or Mao (Methylaluminoxane) As Cocatalyst,And Mostly Dimers And Trimers Were Produced. Better Activities Were Observed With Etalcl2 As Cocatalyst Than With Mao. (C) 2012 Elsevier B. V. All Rights Reserved.
Doi:10.1016/j.Jorganchem.2012.07.044

专利信息

专利号:WO-2024076306-A1
优先权日:2022-10-05
标题:Micro-flow synthesis of compounds and systems thereof
发明人：WU JIE; LIU CHENGUANG; WANG MU
权利人:NAT UNIV SINGAPORE
摘要:The present disclosure concerns a micro-flow system for synthesis of a compound, comprising a tubing reactor configured to flow a reactant within its lumen thereof, an actuator for regulating the flow of the reactant in the lumen and a heterogeneous catalyst in fluid communication with the lumen. The present disclosure also concerns a method of micro-flow synthesising a compound using the micro-flow system.

专利号:US-2023174477-A1
优先权日:2021-12-03
标题:Methods for synthesis of the tricyclic prostaglandin d2 metabolite methyl ester
发明人：DAI MINGJI; SIMS HUNTER
权利人:PURDUE RESEARCH FOUNDATION
摘要:Methods for the synthesis of a tricyclic-prostaglandin D 2 metabolite methyl ester or a pharmaceutically acceptable salt thereof.

专利号:WO-2020194337-A4
优先权日:2019-03-28
标题:A process for the asymmetric synthesis of sitagliptin intermediate
发明人：PUNJI BENUDHAR; SENTHILKUMAR BEERAN; VENKATA RAMANA CHEPURI
权利人:COUNCIL SCIENT IND RES
摘要:The present invention relates to a process for the asymmetric synthesis of compound of Formula 2. wherein, R1 is selected from the group consisting of C(O)R or C(O)OR; R is selected from the group consisting of CH3, ethyl, isopropyl and tert-butyl R2 is selected from the group consisting of straight or branched, substituted or unsubstituted C1-C10 alkyl, substituted or unsubstituted aryl groups. More particularly, the present invention relates to an asymmetric hydrogenation of compound of Formula 2 by using new catalyst system, which provides desired product formation in a very cost effective way.

专利号:US-2025115551-A1
优先权日:2023-10-03
标 题:Synthesis of ras inhibitors
发明人：LI YI; MENDOZA BENJAMIN; NAGANATHAN SRIRAM; WANG ROSS; YI YI; BALLMER STEVEN G; DAVIDSON JAMES; HUANG XIAOJUN
权利人:REVOLUTION MEDICINES INC
摘要:The present invention relates to Ras inhibitors, intermediates in the synthesis thereto, and methods for preparing the Ras inhibitors and the intermediates.

专利号:US-2022274930-A1
优先权日:2019-06-14
标题:Processes and compounds for the decarboxylative amination of redox-active esters with diazirines
发明人：LOPCHUK JUSTIN M; CHANDRACHUD PREETI P
权利人:H LEE MOFFITT CANCER CT & RES
摘要:The invention described herein relates generally to processes for the synthesis of amine-containing organic compounds. More specifically, described herein relates to processes for the decarboxylative amination of redox-active esters with diazirines and the products formed thereof. Compounds for use in the above processes are also described.

专利号:US-2025163076-A1
优先权日:2022-02-18
标 题 :Synthesis of bruton's tyrosine kinase inhibitors
发明人：TRAN NGOC DUC; XIOURAS CHRISTOS; CLEATOR EDWARD; MATON WILLIAM MARC; RAMMELOO THOMAS JOACHIM LANDEWALD; FERNANDES PHILIPPE; BONGARTZ JEAN-PIERRE A; CAO DUY CHI TRUNG; HORWITZ MATTHEW ALLAN; JUSSEAU XAVIER JEAN-MARIE; LEMAIRE SÉBASTIEN FRANCOIS-EMMANUEL; SCHWEITZER-CHAPUT BERTRAND
权利人:JANSSEN PHARMACEUTICA NV
摘要:The present disclosure is directed to methods of synthesizing a compound of Formula (I), where the R groups are defined herein, and to methods of synthesizing a compound of Formula (II). Some aspects of the present disclosure is directed to converting the compound of Formula (II) into its P form.