4-octene置于吡啶,Dihydrogen Hexachloroplatinate,三氯硅烷体系中,用 四氢呋喃,苯 作为反应溶剂,110.0 °C,9.81 Mpa 条件下,反应 6.0H,反应生成 辛基三甲氧基硅烷 参考文献:Pinazzi,Ch.P. Et Al.,Bulletin De La Societe Chimique De France,1974,P. 2166-2170 标题:Pinazzi,Ch.P. Et Al.,Bulletin De La Societe Chimique De France,1974,P. 2166-2170
专利号:US-2024010511-A1 优先权日:2019-05-02 标 题 :Methods and compositions for synthesis of phosphor and its incorporation in a polymer matrix for light conversion 发明人:SAHI SUNIL 权利人:SOLGO INC; SOLGRO INC 摘要:The invention relates to methods and compositions for synthesizing a phosphor and preparing a surface-modified phosphor comprising a phosphor, a silica, and a silane, and articles comprising same. The invention also relates to a method of dispersion of the disclosed surface-modified phosphor with a blue emitting agent in a polymer matrix and uses thereof.
专利号:US-11033507-B2 优先权日:2013-12-19 标 题 :Method of synthesis of silica vesicles and use thereof 发明人:YU CHENGZHONG; MITTER NEENA; ZHANG JUN 权利人:UNIV QUEENSLAND 摘要:The invention relates, in part, to a method of producing silica vesicles including under controlled conditions to thereby heavily influence the morphology and characteristics of the vesicles. The vesicles are shown to be effective as delivery agents for chemical and biological agents. They are also shown to be useful in methods of treatment and as components of an immunogenic composition.
专利号:US-9828454-B2 优先权日:2013-01-28 标题 :Synthesis of functional polyisobutylene-containing oligomers and polymers 发明人:BURDZY MATTHEW; FENG DINGSONG; ZHANG TIANZHI 权利人:Henkel IP & Holding GmbH 摘要:Disclosed are single step and multi-step methods of making functional polyisobutylene (PIB)-containing oligomers and polymers and the materials made thereby. In the single step method a functional group containing PIB oligomer or polymer is made under cationic polymerization conditions in a direct, one step reaction. In the multi-step method a functional group containing PIB oligomer or polymer is made in a two-step process. The first step is performed under cationic polymerization conditions. The second step is performed under non-cationic polymerization conditions.
专利号:US-11052374-B2 优先权日:2018-12-20 标题:Surfactant-templated synthesis of nanostructured xerogel adsorbent platforms 发明人:DE LEON PATRICIA IGNACIO; LAIBLE PHILIP D; MEYER MACKENZIE ELIZABETH; POVINELLI CHRISTOPHER R; TRACEY KILLIAN L; ARENAS DANIEL YOAV 权利人:UCHICAGO ARGONNE LLC 摘要:A process for separations and recovery from mixtures via specific adsorption using high-surface area, flexible silica-based nanostructured gel adsorbents and articles of manufacture relating to same.
专利号:WO-03068806-A1 优先权日:2002-02-14 标 题 :Solid phase peptide synthesis on silica 发明人:GROARKE MICHELLE 权利人:JOHNSON MATTHEY PLC; GROARKE MICHELLE 摘要:A method for peptide synthesis is described, comprising steps of forming an organofunctional silica by reaction of an alkyl silicate, an organofunctional silane and water, optionally in the presence of a template compound; removing the template compound if present; reacting said organofunctional silica with a first protected amino acid to produce a tethered protected amino acid; deprotecting the tethered protected amino acid; reacting at least one further protected amino acid with said tethered deprotected amino acid to form a tethered peptide, and removing the peptide from the organofunctional silica. Preferably, prior to reaction of the first protected amino acid, the organofunctional silica is reacted with at least one linking compound to form a linker-modified organofunctional silica with which the first protected amino acid is reacted. A method for preparing an organfunctional silica by the co-hydrolysis of an alkyl silicate and an organofunctional silane is depicted below. The wavy line represents the silicon atom on or within the resulting silica material formula (I). A reaction of a protected amino acid with an organofunctional silica to provide a tethered protected amino acid is depicted below formula (II).
专利号:US-7432031-B2 优先权日:2005-03-22 标 题:Toner for electrostatic charge developing, production method thereof, developer for electrostatic charge developing using the same, and image forming method 发明人:MIZUTANI NORIYUKI; MAEHATA HIDEO; HAMANO HIROKAZU; TANAKA HIROYUKI; KITAGAWA SOICHIRO; IGUCHI MOEGI 权利人:FUJI XEROX CO LTD 摘要:A toner for electrostatic charge developing prepared by a production method including aggregating one or more kind of particles in a raw material dispersion including the particles to form aggregated particles, and coalescing the aggregated particles by heating. At least one kind of the particles is resin particles including an amorphous polyester resin synthesized by copolymerizing one or more polyvalent carboxylic acids and two or more polyhydric alcohols; at least one of the polyvalent carboxylic acids is polyvalent carboxylic acid having a sulfonic acid group; two of the polyhydric alcohols are an ethylene oxide adduct of bisphenol A and a propylene oxide adduct of bisphenol A; and the following equation is satisfied:n n10/90≦ BPA ( EO )/ BPA ( PO )≦90/10.n n In the equation, BPA(EO) represents a total mole amount of the ethylene oxide adduct of bisphenol A used in synthesis of the amorphous polyester resin, and BPA(PO) represents a total mole amount of the propylene oxide adduct of bisphenol A used in synthesis of the amorphous polyester resin.
[参考文献]: Brandy J Johnson, Et Al. Porphyrin-Embedded Silicate Materials For Detection Of Hydrocarbon Solvents. Sensors (Basel). 2011;11(1):886-904. [参考文献]: Jiqian Wang, Et Al. Immobilization Of Lipases On Alkyl Silane Modified Magnetic Nanoparticles: Effect Of Alkyl Chain Length On Enzyme Activity. Plos One. 2012;7(8):E43478. [参考文献]: Ruixia Gao, Et Al. Preparation Of Cu(2+)-Mediated Magnetic Imprinted Polymers For The Selective Sorption Of Bovine Hemoglobin. Talanta. 2016 Apr 1:150:46-53.
合成参考文献
摘要:S13 | EUCOSMETICS | Combined Inventory of Ingredients Employed in Cosmetic Products (2000) and Revised Inventory (2006) | DOI:10.5281/zenodo.2624118 摘要:Final Report 12/2016 Available from CIR