2176-98-9 = 867-36-7 反应条件:1.1 Reagents: Thionyl Chloride 标题:Reactions Of Thionyl Chloride With Tetraorganotin(Iv) Compounds 作者:Narula,Suraj P.; Et Al 参考文献:Indian Journal Of Chemistry 日期:1983 卷标:(3) 页码:246-7]
2176-98-9 = 867-36-7 反应条件:1.1 Reagents: Tin Tetrachloride; 2 H,Rt -> 100 °C; 4 H,100 °C -> 220 °C 标题:Synthesis And Characterization Of Linear Poly(Dialkylstannane)S 作者:Choffat,Fabien; Et Al 参考文献:Macromolecules (Washington 日期:2007 卷标:40(22) 页码:7878-7889]
927-77-5 = 867-36-7 反应条件:1.1 Reagents: Tin Tetrachloride Solvents: Diethyl Ether,Hexane; 1 H,Cooled; 2 H,Reflux1.2 Solvents: Toluene; 1 H,90 °C1.3 Reagents: Hydrochloric Acid Solvents: Water; Cooled2.1 Reagents: Tin Tetrachloride; 2 H,Rt -> 100 °C; 4 H,100 °C -> 220 °C 标题:Synthesis And Characterization Of Linear Poly(Dialkylstannane)S 作者:Choffat,Fabien; Et Al 参考文献:Macromolecules (Washington 日期:2007 卷标:40(22) 页码:7878-7889
专利号:US-2024383928-A1 优先权日:2021-07-30 标 题:Production of diorganotin dihalides 发明人:VINCENT ROBERT; ZIMMERMANN JARROD C 权利人:MERCK PATENT GMBH 摘要:The disclosed and claimed subject matter relates to the safe and efficient synthesis of diorganotin dihalide compounds of the formula R2SnX2 that as-synthesized are free of tetraalkyltin (R4Sn), trialkyltin halide (R3SnX) and monoalkyltin trihalide (RSnX3) species and of methods for their synthesis and use.
专利号:US-8329923-B2 优先权日:2010-06-17 标 题:4, 4′ disubstituted 4H-cyclopentadithiophene and new methods for synthesizing the same 发明人:VANDERZANDE DIRK; LUTSEN LAURENCE; VAN MIERLOO SARAH 权利人:VANDERZANDE DIRK; LUTSEN LAURENCE; VAN MIERLOO SARAH; IMEC; UNIV HASSELT 摘要:The present preferred embodiments relate to a method for the synthesis of a compound having the following general formula: n nthe method comprising the step of reacting, in presence of a diprotic acid having a negative pKa, a compound having the general formula:n n nwherein R 1 and R 2 are organic groups and wherein X and Y are independently selected from the group consisting of hydrogen, chloro, bromo, iodo, boronic acid, boronate esters, borane, pseudohalogen and organotin. It further relates to compounds so obtained and to compounds resulting from the ring closure of compound (II).
摘要:Schafer, E. W., Jr., and W. A. Bowles Jr. 1985. Acute oral toxicity and repellency of 933 chemicals to house and deer mice. Archives of Environmental Contamination and Toxicology 14:111-129. https://www.aphis.usda.gov/ws/nwrc/chem-effects-db/S_schafer851.pdf