Trimethoxy-[3-(2,2,5,5-Tetramethyl-1,2,5-Azadisilolidin-1-yl)Phenyl]Silane置于甲醇体系中,用 四氢呋喃 作为反应溶剂,以96%的收率获得产物间-氨基苯基三甲氧基硅烷 参考文献: Preparation Of An Aminoaryl-Containing Organosilicon Compound And Methods Of Preparaing Intermediates Used In Its Preparatrion[fr] Procede De Fabrication D'Un Compose D'Organosilicium Contenant Un Aminoaryle Et Procede De Fabrication D'Un Produit Intermediaire Dudit Compose 标题: Preparation Of An Aminoaryl-Containing Organosilicon Compound And Methods Of Preparaing Intermediates Used In Its Preparatrion[fr] Procede De Fabrication D'Un Compose D'Organosilicium Contenant Un Aminoaryle Et Procede De Fabrication D'Un Produit Intermediaire Dudit Compose
专利号:WO-03068806-A1 优先权日:2002-02-14 标 题 :Solid phase peptide synthesis on silica 发明人:GROARKE MICHELLE 权利人:JOHNSON MATTHEY PLC; GROARKE MICHELLE 摘要:A method for peptide synthesis is described, comprising steps of forming an organofunctional silica by reaction of an alkyl silicate, an organofunctional silane and water, optionally in the presence of a template compound; removing the template compound if present; reacting said organofunctional silica with a first protected amino acid to produce a tethered protected amino acid; deprotecting the tethered protected amino acid; reacting at least one further protected amino acid with said tethered deprotected amino acid to form a tethered peptide, and removing the peptide from the organofunctional silica. Preferably, prior to reaction of the first protected amino acid, the organofunctional silica is reacted with at least one linking compound to form a linker-modified organofunctional silica with which the first protected amino acid is reacted. A method for preparing an organfunctional silica by the co-hydrolysis of an alkyl silicate and an organofunctional silane is depicted below. The wavy line represents the silicon atom on or within the resulting silica material formula (I). A reaction of a protected amino acid with an organofunctional silica to provide a tethered protected amino acid is depicted below formula (II).
专利号:CN-106179503-A 优先权日:2016-07-08 标题:Catalyst for Synthesis of Cyclohexanol/Cyclohexanone by Highly Selective Catalytic Oxidation of Cyclohexane
专利号:US-2008069887-A1 优先权日:2006-09-15 标 题 :Method for nanoparticle surface modification 发明人:BARAN JIMMIE R; FANSLER DUANE D 权利人:3M INNOVATIVE PROPERTIES CO 摘要:The present disclosure discloses a method for making surface-modified nanoparticles. The surface of a nanoparticle is modified with an aminorganosilane and an alkylating agent in a one-pot synthesis to provide alkylamine surface-modified nanoparticles.
专利号:US-10173898-B2 优先权日:2014-05-09 标题 :Functionalized graphene 发明人:BLANFORD CHRISTOPHER; WEHNER MIRJA; FLITSCH SABINE 权利人:UNIV MANCHESTER 摘要:Graphene is chemically modified by a process resulting in the introduction of functional groups located only at an edge of the graphene plane. The functionalized graphene finds uses in numerous applications and further chemical synthesis, including a process for coupling an organic or inorganic moiety to the graphene plane via the edge-located functional group. The disclosed products and processes provide highly flexible platforms for the integration of graphene into a variety of applications.
专利号:JP-5382400-B2 优先权日:2008-02-05 标题:Synthesis method of organic-inorganic composite
专利号:CN-114573811-A 优先权日:2021-12-29 标题 :A kind of imide slurry, its synthesis method and the composition containing this imide slurry
参考文献:10.1007/s00894-020-04489-z 摘要:Joseph E, Swaminathan N, Kannan K. Material identification for improving the strength of silica/SBR interface using MD simulations. Journal of Molecular Modeling. 2020 Aug 17;26(9):234. doi: 10.1007/s00894-020-04489-z.