CAS: 4292-19-7; 1-Iodododecane

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📜十二烷醇置于咪唑,碘,三苯基膦体系中,用 二氯甲烷 作为反应溶剂,化学反应生成 1-碘十二烷
参考文献:卤代烷通过卤素原子转移进行光氧化还原多氟芳基化
标题:卤代烷通过卤素原子转移进行光氧化还原多氟芳基化
摘要:多氟芳烃部分在药物化学,农用化学品和材料科学中引起人们的兴趣.在此,我们首次通过卤素原子转移过程对未活化的卤代烷进行多氟芳基化.该方法在酰胺,氨基甲酸酯,酯,芳族和磺酰胺部分(包括复杂生物活性分子的衍生物)存在下,以非常好的产率将伯,仲和叔烷基卤转化为相应的多氟芳基化合物.机理工作表明,这种转变是通过卤素原子转移后产生的烷基进行的.
DOI:10.1021/acs.Orglett.1C04267

专利信息

专利号:US-5098602-A
优先权日:1988-05-11
标题 :Novel halogen-containing ester compounds, and their intermediates, and method of producing the same as well as liquid crystal compositions containing the same and light switching elements
发明人：HIRAI TOSHIHIRO; YOSHIZAWA ATSUSHI; NISHIYAMA ISA; FUKUMASA MITSUO; SHIRATORI NOBUYUKI; YOKOYAMA AKIHISA
权利人:NIPPON MINING CO
摘要:This invention provides a novel halogen-containing ester compound represented by the following general formula (I): ##STR1## (wherein R is an alkyl group, A is selected from a single bond, --O--, --COO-- and --CO--, both of X and Y are halogen atoms or either one of X and Y is a halogen atom and the other is a hydrogen atom, each of m and n is 0 or 1, m+n=0 or 1, each of k and l is an integer of 1 or more, provide k
专利号:US-8168671-B2
优先权日:2008-06-26
标题 :Synthesis of thieno[3,4-b]thiophene, thieno[3,4-b]furan, related compounds and their derivatives and use thereof
发明人：SOTZING GREGORY A
权利人:SOTZING GREGORY A; UNIV CONNECTICUT
摘要:Inexpensive and facile methods of preparing fused heterocycles such as thieno[3,4-b]thiophene, thieno[3,4-b]furan, related compounds, and their derivatives are disclosed. Also disclosed are regioregular polymers prepared from the fused heterocycles.

专利号:EP-4065643-B1
优先权日:2019-11-28
标题 :Fluorescent acridinium salts, synthesis thereof and use for detection of cardiolipin
发明人：ARSENJANS PAVELS; DIMITRIJEVS PAVELS
权利人:LATVIAN INST ORGANIC SYNTHESIS

专利号:WO-2020181929-A1
优先权日:2019-03-08
标题 :Preparation method for heptamethylbenzylindole cyanine dye and application thereof
发明人：WU AIGUO; LI JUAN; JIANG ZHENQI; YUAN BO
权利人:CIXI INSTITUTE OF BIOMEDICAL ENGINEERING NINGBO INSTITUTE OF INDUSTRIAL TECH CHINESE ACADEMY OF SCIE; NINGBO INSTITUTE OF MATERIALS TECH & ENGINEERING CHINESE ACADEMY OF SCIENCES
摘要:The present application relates to the fields of polymethylbenzylindole cyanine dyes and the preparation thereof, and disclosed thereby are a preparation method for a heptamethylbenzylindole cyanine dye and an application thereof. The method comprises the following steps: 1) reacting raw materials comprising a 2,3,3-trimethyl-4,5-benzoindole derivative and a nucleophilic substitution compound under vacuum conditions at an increased temperature to obtain an organic ammonium salt; 2) reacting the organic ammonium salt obtained in step 1) with a solution of a cycloolefin derivative at an increased temperature under closed conditions. The structural formula of the heptamethylbenzindole cyanine dye is as shown in formula (I). The dye has near-infrared light absorption and fluorographic properties, and can be used as a probe auxiliary. The method has the advantages of having a short synthesis route, having a friendly solvent environment, having a simple process, preventing noble metal catalysis, having high yield, having high purity, and so on, has high applicability, and can be used to synthesize products of various structure types.

专利号:US-2006159608-A1
优先权日:2004-12-03
标题 :Method for the use of [11C] carbon monoxide in labeling synthesis of 11C-labelled acids by photo-induced free radical carbonylation

专利号:US-2006165590-A1
优先权日:2004-12-17
标 题 :Method for the use of [11C] carbon monoxide in labeling synthesis of 11C-labelled esters by photo-induced free radical carbonylation