专利号:US-6214847-B1 优先权日:1997-08-14 标题 :Crystalline 10,10-Bis((2-fluoro-4-pyridinyl)methyl)-9(10H)-Anthracenone and an improved process for preparing the same 发明人:PESTI JAAN A; FORTUNAK JOSEPH M; HUHN GEORGE F; MAURIN MICHAEL; YIN JIANGUO 权利人:DU PONT PHARM CO 摘要:The present invention relates to processes for the synthesis of a crystalline polymorph of 10,10-Bis((2-fluoro-4-pyridinyl)methyl)-9(10H)-Anthracenone in high purity. The product is useful in the synthesis of pharmaceutical compounds for the reduction of cholinergic system dysfunction.
专利号:US-7696386-B2 优先权日:2006-09-29 标 题:Method of producing diol, polydiol, secondary alcohol or diketone compound 发明人:HOSONO HIDEO; BUCHAMMAGARI HARITHA; TODA YOSHITAKE; HIRANO MASAHIRO; OSAKADA KOHTARO; TAKEUCHI DAISUKE 权利人:JAPAN SCIENCE & TECH AGENCY 摘要:The invention is a process of using, as a reducing agent, a 12CaO.7Al 2 O 3 electride containing electrons in a number of 10 19 or more and 2.3×10 21 cm −3 or less in its cages to subject a carbonyl compound to reductive coupling in a solvent, thereby synthesizing a diol or polydiol. The invention is also a process of reducing a ketone compound in a solvent, thereby synthesizing a secondary alcohol or diketone compound. According to the process of the invention, it is possible to synthesize a diol or polydiol, or a secondary alcohol or diketone compound through simple operations in a short period without using an expensive and harmful metal hydride or metal salt nor limiting the atmosphere for the synthesis to an inert gas atmosphere as in conventional processes.
专利号:CN-111253235-A 优先权日:2020-03-30 标题:Synthesis method and synthesis device of high-purity hypericin
专利号:CN-106966891-A 优先权日:2017-02-07 标题:A kind of total synthesis process of rhein
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合成参考文献
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