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3-羟基吡啶置于溴,Sodium Hydroxide体系中,用 水 作为反应溶剂,化学反应 24.0H,以66%的收率获得产物2-溴-3-羟基吡啶
参考文献:作为螺旋肽模拟物的苯基吡啶支架的合成
标题:作为螺旋肽模拟物的苯基吡啶支架的合成
摘要:基于苯基吡啶和苯基联吡啶的支架已被设计和合成为新型螺旋肽模拟物.该合成需要优化和选择性烷基化来生产 2,6-官能化 3-羟基吡啶衍生物,以实现收敛方案.吡啶类似物通过一系列 Suzuki/stille 型交叉偶联反应进行偶联.产生了一系列联芳基和三芳基取代的杂环.该合成方法简洁且产率高,允许在所需的侧链连接点上存在较大的可变性.合成了许多化合物以显示该策略的多功能性.
DOI:10.1002/chem.201000315

专利信息

专利号:US-7999090-B2
优先权日:2000-07-07
标 题:Fungal cell wall synthesis gene
发明人：TSUKAHARA KAPPEI; HATA KATSURA; SAGANE KOJI; NAKAMOTO KAZUTAKA; TSUCHIYA MAMIKO; WATANABE NAOAKI; OHBA FUMINORI; TSUKADA ITARU; UEDA NORIHIRO; TANAKA KEIGO; KAI JUNKO
权利人:EISAI R&D MAN CO LTD
摘要:The present invention provides isolated DNA encoding a GWT1 protein having activity to confer resistance of a fungus against a compound of formula Ia, and wherein a defect of a function of the GWT1 protein leads to a decrease in the amount of a glycosylphosphatidylinositol (GPI)-anchored protein in the cell wall of a fungus.

专利号:US-11229713-B2
优先权日:2014-11-25
标题:Methods and compositions for 18F-radiolabeling of biologics
发明人：DONNELLY DAVID
权利人:BRISTOL MYERS SQUIBB CO
摘要:The invention relates to water soluble 18 F-prosthetic groups and the synthesis and use of 18 F-labeled biological molecules containing the 18 F-prosthetic groups for imaging various processes within the body, for detecting the location of molecules associated with disease pathology, and for monitoring disease progression are disclosed.

专利号:EP-2644618-A1
优先权日:2007-02-09
标题:tether intermediates for the synthesis of macrocyclic ghrelin receptor modulators

专利号:US-9738661-B2
优先权日:2006-10-27
标题:HCV NS3 protease inhibitors
发明人：LIVERTON NIGEL J; SUMMA VINCENZO; HARPER STEVEN; MCCAULEY JOHN A; ROMANO JOSEPH J; RUDD MICHAEL T
权利人:MERCK SHARP & DOHME; MSD ITALIA SRL
摘要:The present invention relates to macrocyclic compounds of formula (I) that are useful as inhibitors of the hepatitis C virus (HCV) NS3 protease, their synthesis, and their use for treating or preventing HCV infections.

专利号:US-11806409-B2
优先权日:2016-06-01
标题 :Imaging methods using 18F-radiolabeled biologics
发明人：DONNELLY DAVID; LEUNG DAVID K
权利人:BRISTOL MYERS SQUIBB CO
摘要:The invention relates to water soluble 18 F-prosthetic groups and the synthesis and use of 18 F-labeled biological molecules containing the 18 F-prosthetic groups for imaging various processes within the body, for detecting the location of molecules associated with disease pathology, and for monitoring disease progression are disclosed.

专利号:CN-116854632-A
优先权日:2023-07-07
标题:Synthesis method and application of large-steric-hindrance heteroatom compound