CAS: 328090-25-1; 1-Ethyl-3-Methyl-1H-Imidazol-3-Ium 4-Methylbenzenesulfonate

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410522-18-8 150999-33-0 783321-71-1

📜对甲苯磺酰氯置于potassium Carbonate体系中,用 Neat (No Solvent) 用作溶剂,化学反应 0.58H,反应生成1-乙基-3-甲基咪唑嗡甲苯磺酰酯
参考文献:A Dicationic,Podand-Like,Ionic Liquid Water System Accelerated Copper-Catalyzed Azide-Alkyne Click Reaction
标题:A Dicationic,Podand-Like,Ionic Liquid Water System Accelerated Copper-Catalyzed Azide-Alkyne Click Reaction
摘要:In This Work,An Effective,Task Specific,Dicationic,Podand-Like Ionic Liquid Was Synthesized And Applied To Improve The Capability Features Of Click Reaction. Moreover,To Broaden The Scope And Decreasing The Serious Limitations Of Preparation Methods Of Organic Azides,A Simple Green Procedure For The Preparation Of Alkyl Azides,The Fundamental Starting Materials In Click Reactions,From Alcohols Under Solvent-Free Conditions And Microwave Irradiation Has Been Reported,For The First Time. (C) 2014 Mohammad Javaherian. Published By Elsevier B.V. On Behalf Of Chinese Chemical Society. All Rights Reserved.
Doi:10.1016/j.Cclet.2014.09.005

专利信息

专利号:US-2010191010-A1
优先权日:2007-07-02
标题 :Process for the synthesis of carbamates using co2
发明人：BOSMAN JORIS KAREL PETER; CARR ROBERT HENRY
权利人:HUNTSMAN INT LLC
摘要:Process for the synthesis of non cyclic carbamate derivatives from amine compounds, alcohols and CO 2 in the presence of ionic liquids and optionally in the presence of a base.

专利号:US-9267213-B1
优先权日:2005-03-25
标题:Electrochemical deblocking solution for electrochemical oligomer synthesis on an electrode array
发明人：MAURER KARL; COOPER JOHN J
权利人:CUSTOMARRAY INC
摘要:There is disclosed an electrochemical deblocking solution for use on an electrode microarray. There is further disclosed a method for electrochemical synthesis on an electrode array using the electrochemical deblocking solution. The solution and method are for removing acid-labile protecting groups for synthesis of oligonucleotides, peptides, small molecules, or polymers on a microarray of electrodes while substantially improving isolation of deblocking to active electrodes. The method comprises applying a voltage or a current to at least one electrode of an array of electrodes. The array of electrodes is covered by the electrochemical deblocking solution.

专利号:US-10407676-B2
优先权日:2014-12-09
标题 :High efficiency, small volume nucleic acid synthesis
发明人：POEHMERER THOMAS; KUHN PHILLIP; NOTKA FRANK; ZEIDLER ANDREAS; HEIL KORBINIAN; TREFZER AXEL; FONNUM GEIR; KATZEN FEDERICO; ANDERSSON KRISTIAN
权利人:LIFE TECHNOLOGIES CORP; THERMO FISHER SCIENT GENEART GMBH; LIFE TECH AS
摘要:The disclosure generally relates to compositions and methods for the production of nucleic acid molecules. In some aspects, the invention allows for the microscale generation of nucleic acid molecules, optionally followed by assembly of these nucleic acid molecules into larger molecules. In some aspects, the invention allows for efficient production of nucleic acid molecules (e.g., large nucleic acid molecules such as genomes).

专利号:EP-2173705-A1
优先权日:2007-07-02
标 题:Process for the synthesis of carbamates using co2

专利号:EP-2011782-A1
优先权日:2007-07-02
标题:Process for the synthesis of carbamates using co2

专利号:WO-2009013062-A1
优先权日:2007-07-02
标 题:Process for the synthesis of carbamates using co2