CAS: 5324-13-0; 2,6-Dibromo-4-Chlorophenol

该化合物是一种卤代酚化合物,在有机合成中和作为特殊化学品生产的中间体中应用,其结构以溴和氯替代成分为特点,增强了其反应活动性,在电动芳香替代反应中提高了其效用,该化合物因其作为农用化学和制药制造的前体的稳定性和有效性而备受珍视,其高纯度和一贯性使其适合于需要精确溴化或氯化步骤的研究和工业过程.适当处理由于其潜在的毒性和环境影响而至关重要.建议在惰性条件下储存以稳定性.

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CAS号106-48-9 对氯苯酚 | CAS号1679-18-1 4-氯苯硼酸 | CAS号106-47-8 对氯苯胺 | CAS号7726-95-6 溴素 | CAS号64-19-7 冰醋酸 | CAS号10035-10-6 氢溴酸 | CAS号64-17-5 乙醇 | CAS号7782-99-2 亚硫酸 | CAS号695-96-5 2-溴-4-氯苯酚 | CAS号15969-10-5 2-溴-4-氯-6-硝基苯酚 | CAS号1570-64-5 4-氯-2-甲基苯酚 | CAS号1123-63-3 4-氯-2,6-二甲基苯酚 | CAS号76800-28-7 5,5'-dichloro-2... | CAS号76800-29-8 3-bromo-5,5'-di... | CAS号19643-45-9 2,6-二溴對苯醌

合成工艺路线路线简述

    📜对氯苯酚置于potassium Bromide体系中,化学反应生成 2,6-二溴对氯苯酚
    参考文献:准二元体系 Lamno3-srmno3 和 Lamno3-camno3 中的相图研究
    标题:准二元体系 Lamno3-srmno3 和 Lamno3-camno3 中的相图研究
    摘要:研究了准二元体系lamno 3-Srmno 3 和lamno 3-Camno 3 .两种系统在空气中低于约 1400 oc 的中间 La:Sr 和 La:Ca 比率下均显示出混溶间隙.这种现象导致单相(La,Sr)Mno 3− X 和(La,Ca)Mno 3− X 固溶体分解为富la Srmno 3− X + 富sr Lamno 3− X 和富la Camno 3− X + 富钙 Lamno 3− X 分别在较低温度下.在 1400 oc 的 Lamno 3-srmno 3 体系中,没有观测到 (La,Sr)Mno 3 随着 Sr 含量的增加从斜方晶向菱面体的结构转变,La 0.7 Sr 0.3 Mno 3 的结构被确定为斜方晶系,A = 0.54927 +/-0.0009 Nm,B = 0.54582 +/-0.0009 Nm,C 4 0.76772 +/-0.0034 Nm.
    DOI:10.1557/jmr.2000.0164

    海关参考信息

    专利信息


    专利号:US-11440989-B2
    优先权日:2018-09-17
    标题:Application of Mannich base in flame-retardant polyurethane material
    发明人:GUAN YONGJIAN; LI PING; LI ZHIJUN; WANG FENG; LI YUBO
    权利人:JIAHUA SCIENCE & TECH DEVELOPMENT SHANGHAI LTD; JIAHUA CHEMICALS INC
    摘要:Application of a Mannich base in a flame-retardant polyurethane material is provided. The Mannich base has a structure represented by a formula (I). In the Mannich base, flame-retardant groups, i.e., halogens are introduced at the second, fourth and sixth positions of a phenyl group, and flame-retardant elements, i.e., halogens and nitrogen are introduced into synthesized polyether polyol, giving the synthesized polyether polyol good flame retardance. The amount of active hydrogen in the Mannich base is small so that occurrence of side reactions during the synthesis of the polyether polyol is reduced, and the viscosity of the flame-retardant polyether polyol is lowered. Due to autocatalytic performance of tertiary amido in the flame-retardant polyether polyol, use of a catalyst can be reduced and even avoided during the synthesis. A preparation method of the Mannich base is also provided.

    专利号:US-11401375-B2
    优先权日:2018-09-17
    标题:Flame-retardant polyether polyol as well as preparation method and application thereof
    发明人:GUAN YONGJIAN; LI PING; LI ZHIJUN; WANG FENG; LI YUBO
    权利人:JIAHUA SCIENCE & TECH DEVELOPMENT SHANGHAI LTD; JIAHUA CHEMICALS INC
    摘要:A flame-retardant polyether polyol is provided, including a Mannich base and an epoxide. The epoxide is selected from ethylene oxide, propylene oxide and butylene oxide. The Mannich base has a structure represented by a formula (I). In the Mannich base, flame-retardant groups, i.e., halogens are introduced at the second, fourth and sixth positions of a phenyl group, and flame-retardant elements, i.e., halogens and nitrogen are introduced into synthesized polyether polyol. The amount of active hydrogen in the Mannich base is small so that side reactions during synthesis of the polyether polyol are reduced, and the viscosity of the polyether polyol is lowered. A flame-retardant polyurethane material is also provided, synthesized from raw materials comprising the above-mentioned flame-retardant polyether polyol and an isocyanate. Due to autocatalytic performance of tertiary amido in the flame-retardant polyether polyol, use of a catalyst can be reduced and even avoided during the synthesis.

    专利号:CN-117886760-A
    优先权日:2023-12-18
    标题 :Synthesis method of 3-(5-fluoropyrimidin-2-yl)-2-methoxyaniline

    专利号:CN-110143852-A
    优先权日:2019-06-28
    标 题:A method of photocatalytic synthesis is at more bromophenol compounds in water phase

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    品牌试剂参考报价(招募中)

    📌 第三方产品分析报告

    ✅ COA系统入驻 | 共享模式

    合成参考文献


    参考文献:10.1007/s11696-024-03579-z
    摘要:Rita BH, Uemi M, Raminelli C. Selenium species-catalyzed biomimetic halogenations of aromatic and heteroaromatic compounds. Chem. Pap. 2024 Jun 22;78(12):6971–7. doi: 10.1007/s11696-024-03579-z.
    参考文献:10.1007/bf01623498
    摘要:Ventura F, Rivera J. Potential formation of bromophenols in Barcelona's tap water due to daily salt mine discharges and occasional phenol spills. Bulletin of Environmental Contamination and Toxicology. 1986 Dec;36(1):219–25. doi: 10.1007/bf01623498.
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