CAS: 500011-88-1; Ethyl 2-(3-Chloropyridin-2-yl)-5-Oxopyrazolidine-3-Carboxylate

相似化合物

774600-50-9 7426-59-7 500011-91-6

上下游产品

3-溴-1-(3-氯吡啶-2-基)-4,5-二氢-1H-吡唑-5-甲酸乙酯 Ethyl 3-Bromo-1-(3-Chloropyridin-2-yl)-4,5-Dihydro-1H-Pyrazole-5-Carboxylate 500011-91-6

📜2,3-二氯吡啶置于sodium Ethanolate,一水合肼,溶剂黄146体系中,用 乙醇 作为反应溶剂,化学反应生成 乙基2-(3-氯-2-吡啶基)-5-氧代-3-吡唑烷羧酸酯
参考文献:Sub亚结构邻氨基苯甲酰胺的合成及杀虫活性
标题:Sub亚结构邻氨基苯甲酰胺的合成及杀虫活性
摘要:合成了一系列具有sub亚结构的邻氨基苯甲酰胺,并使用1 HNMR,13 C NMR,Ir和元素分析对其进行了表征.测试了所有化合物对小菜蛾的体外杀虫活性.结果表明合成的化合物具有非常好的杀虫活性.的lc 50个的化合物的值viig,Viil,Viim,Viin表现出优异的杀虫活性,与lc 50,得到7.92毫克的l-1,12.01毫克的l-1,0.62毫克的l-1和10.71毫克的l-1,分别.这些可能被证明可用作潜在的杀虫剂.
DOI:10.1515/chempap-2015-0100

专利信息

专利号:US-2022298136-A1
优先权日:2019-08-21
标题 :Process for synthesis of pyrazolidinone compounds
发明人：MATHUR SUCHET SARAN; JAIN NANDKUMAR JANARDAN; MORE MAHENDRA MAHIPAT
权利人:GHARDA CHEMICALS LTD
摘要:A process for the synthesis of pyrazolidinone, particularly alkyl 2-(3-chloropyridin-2-yl)-5-oxo-pyrazolidine-3-carboxylate (pyrazolidinone) compound, is provided. The process is simple, economical, and produces alkyl 2-(3-chloropyridin-2-yl)-5-oxo-pyrazolidine-3-carboxylate with a comparatively high yields.

专利号:WO-2021033165-A1
优先权日:2019-08-21
标 题:Process for synthesis of pyrazolidinone compounds
发明人：MATHUR SUCHET SARAN; MHATRE HRIDAYNATH VISHWANATH; PEDHAVI VISHAL PARSHURAM
权利人:GHARDA CHEMICALS LTD
摘要:The present disclosure relates to a process for the synthesis of pyrazolidinone, particularly alkyl 2-(3-chloropyridin-2-yl)-5-oxo-pyrazolidine-3-carboxylate (pyrazolidinone) compound. The process of the present disclosure is simple, economical, and produces alkyl 2-(3-5 chloropyridin-2-yl)-5-oxo-pyrazolidine-3-carboxylate with a comparatively high yields.

专利号:WO-2021033172-A1
优先权日:2019-08-20
标题:Process for the preparation of chlorantraniliprole
发明人：V ASHWIN; PRADHAN ASHOK KUMAR; PALIMKAR SANJAY SAMBHAJIRAO; MANE AVINASH SHESHRAO; KUNHIMON SYAM KUMAR UNNIARAN
权利人:EUROFINS ADVINUS LTD
摘要:The present invention relates to two novel, efficient and one-pot methods for synthesizing chlorantraniliprole. In the first scheme, Chlorantraniliprole is prepared by a novel telescopic process starting from 3-Bromo-1-(3-chloropyridin-2-yl)-1H-pyrazole-5-carboxylic acid a key raw material-A (Key RM-A). In the second scheme, starting from Key RM-A, the process steps use of a novel variant of anthranilic acid (Methyl 2-amino-5-chloro-3-methylbenzoate), to get Chlorantraniliprole. Furthermore, the present invention also relates to the synthesis of key starting material for the synthesizing chlorantraniliprole in-situ. All the in-situ steps of the disclosed synthesis methods obtain good yield, without using any expensive reagent or base or harsh reaction conditions, which makes the process simple, environment friendly and more cost effective. With this process the production cost of chlorantraniliprole and its intermediates is substantially reduced; fewer by-products are formed during its synthesis and since it's a one-pot reaction, isolation and purification are easy to achieve.

专利号:WO-2021033166-A1
优先权日:2019-08-21
标 题 :Process for synthesis of pyrazolidinone compounds

专利号:EP-4003962-A1
优先权日:2019-08-21
标题 :Process for synthesis of pyrazolidinone compounds

专利号:CN-108084152-B
优先权日:2017-11-02
标题:A kind of bisamide compound and its synthesis method and application