CAS: 54041-17-7; N-(4-Fluorophenyl)-2-Hydroxy-N-Isopropylacetamide

相似化合物

201668-31-7 121431-17-2 66602-64-0

上下游产品

2-chloro-N-(4-fluorophenyl)-N-(1-methylethyl)acetamide 4-fluoro-N-isopropyl-aniline 4-Fluoronitrobenzene 4-fluoroaniline

2-Chloro-N-(4-Fluorophenyl)-N-(1-Methylethyl)Acetamide置于甲醇,Potassium Acetate体系中,化学反应生成 N-(4-氟苯胺)-2-羟基--N-异丙基乙酰胺
参考文献:Synthesis And Herbicidal Activity Of N-Aryl-2-Heteroaryloxy-N-Isopropyl Acetamide
标题:Synthesis And Herbicidal Activity Of N-Aryl-2-Heteroaryloxy-N-Isopropyl Acetamide
摘要:一系列新型n-芳基-2-杂芳基氧-N-异丙基乙酰胺衍生物通过多步反应合成.其结构通过1H NMR,质谱和元素分析进行了表征.目标化合物的除草活性对抗狗尾草(echinochloa Crusgalli),血草(digitaria Sanguinalis Scop.),白花芙蓉(abutilon Theophrasti),虎尾草(setaria Viridis),百日草(zinnia Elegans)和南风毛菊(acalypha Australis)进行了评估.结果表明,一些标题化合物表现出了优异的除草活性.
DOI:10.14233/ajchem.2013.15239

专利信息

专利号:US-5808152-A
优先权日:1997-12-12
标 题:Synthesis of N-(4-fluorophenyl)-2-hydroxy-N-(1-methylethyl)acetamide using sodium formate
发明人：PRASAD VIDYANATHA A; APPLEGATE JACQUELINE M; ERDMAN DAVID T; NEWALLIS PETER E
权利人:BAYER AG
摘要:The present invention relates to a process for making N-(4-fluorophenyl)-2-hydroxy-N-(1-methylethyl)acetamide. The process includes the steps of (a) reacting 2-chloro-N-(4-fluorophenyl)-N-(1-methylethyl)acetamide with sodium formate to form a reaction mixture that contains N-(4-fluorophenyl)-2-hydroxy-N-(1-methylethyl)acetamideformate; (b) adding an aprotic, aromatic solvent to the reaction mixture; (c) hydrolyzing the N-(4-fluorophenyl)-2-hydroxy-N-(1-methylethyl)acetamideformate in the reaction mixture and (d) recovering N-(4-fluorophenyl)-2-hydroxy-N-(1-methylethyl)acetamide from the organic phase.

专利号:CA-2254608-A1
优先权日:1997-12-12
标 题 :Synthesis of n-(r-fluorophenyl)-2-hydroxy-n-(1-methylethyl)acetamide using sodium formate

专利号:EP-2947075-A1
优先权日:2013-02-05
标题:Synthesis method of thiadiazolylamide derivative

专利号:EP-2947075-B1
优先权日:2013-02-05
标 题:Synthesis method of thiadiazolylamide derivative

专利号:CN-103113322-B
优先权日:2013-02-05
标题:Synthesis method of thiadiazolylamide derivative