专利号:US-9422259-B2 优先权日:2011-01-18 标题:Synthetic transtaganolide and basiliolide products, derivatives thereof, and synthesis methods thereof 发明人:NELSON HOSEA; MURAKAMI KEI; VIRGIL SCOTT C; STOLTZ BRIAN M; GORDON JONATHAN R 权利人:CALIFORNIA INST OF TECHN 摘要:Compounds represented by Formula I are provided that include synthetic transtaganolide and basiliolide products. Derivatives of these compounds and methods of synthesis are also provided.
专利号:US-4107210-A 优先权日:1976-09-07 标 题 :Synthesis of alpha-diketones 发明人:FREITER EDWARD R 权利人:DOW CHEMICAL CO 摘要:Alpha-diketones, such as 1-phenyl-1,2-propanedione and 1-propyl-1,2-butanedione, are prepared by reacting an acylmethyl ester of a carboxylic acid (e.g., benzoylmethyl acetate or butanoylmethyl propionate) with an aldehyde, such as formaldehyde or acetaldehyde, in the presence of an acid catalyst and water. Such alpha-diketones are also obtained by first refluxing a mixture of an alpha-haloketone and a carboxyl anion source and then reacting the mixture with an aldehyde in the presence of an acid catalyst and water.
专利号:JP-3919930-B2 优先权日:1998-03-25 标 题:Synthesis of β-diketone-based alkaline earth metal complexes
专利号:US-4511515-A 优先权日:1983-06-28 标题:Method for making a volatile cerium diketonate compound 发明人:THOMPSON DAVID A 权利人:CORNING GLASS WORKS 摘要:A method for the synthesis of tetrakis-(6,6,7,7,8,8,8,-heptafluoro-2,2-dimethyl-3,5-octanedione) cerium (IV), [Ce(fod) 4 ] wherein the product is directly formed by reacting the deprotonated beta-diketonate ligand with a cerium (IV) salt, is disclosed.
专利号:CN-1962619-A 优先权日:2005-11-10 标 题:Method for synthesis of 2,3-octadione monoxime
专利号:CN-113999099-B 优先权日:2021-02-05 标题 :A kind of synthesis method of 2,3-octanedione
参考文献:10.1007/s10529-006-9062-2 摘要:Hu J, Xu Y. Anti-prelog reduction of prochiral carbonyl compounds by Oenococcus oeni in a biphasic system. Biotechnol Lett. 2006 Jul;28(14):1115–9. doi: 10.1007/s10529-006-9062-2. 摘要:The Good Scents Company Information System 摘要:von Angerer, S., Science of Synthesis, (2005) 26, 83. 摘要:Landais, Y.; Vincent, J. M., Science of Synthesis, (2005) 26, 677.