581-42-0 + 65051-83-4 + 496-11-7 + 573-98-8 + 569-41-5 + 527-53-7 + 575-41-7 + 767-59-9 + 620-14-4 = 629-59-4 + 27133-93-3 + 3296-50-2 + 4175-53-5 + 493-02-7 + 5325-97-3 + 2039-89-6 反应条件:1.1 Reagents: Dodecane,Decane,Tridecane,Pentadecane,Hydrogen Catalysts: Ruthenium; 134.1 Bar; 3.25 H,157.6 Bar,Rt -> 305 °C 标题:An Improved Catalytic Pyrolysis Concept For Renewable Aromatics From Biomass Involving A Recycling Strategy For Co-Produced Polycyclic Aromatic Hydrocarbons 作者:Genuino,Homer C.; Muizebelt,Inouk; Heeres,Andre; Schenk,Niels J.; Winkelman,Jos G. M.; Et Al 参考文献:Green Chemistry 日期:2019 卷标:21(14) 页码:3802-3806]
104-54-1 = 629-59-4 反应条件:1.1 Solvents: Toluene; 5 Min,Rt1.2 Catalysts: (T-4)-[1,3-Bis(2,4,6-Trimethylphenyl)-2-Imidazolidinylidene]Dichloro[[2-(1-Methy... Solvents: Toluene; 2 H,80 °C; 80 °C -> 110 °C1.3 Catalysts: Potassium Hydroxide,Tricyclohexylphosphine; 110 °C2.1 Solvents: Toluene; 5 Min,30 °C2.2 Catalysts: (T-4)-[1,3-Bis(2,4,6-Trimethylphenyl)-2-Imidazolidinylidene]Dichloro[[2-(1-Methy... Solvents: Toluene; 1 H,30 °C2.3 Catalysts: Potassium Hydroxide,Tricyclohexylphosphine Solvents: Toluene; Rt -> 110 °C; 24 H,110 °C 标题:Dehydrogenative Alcohol Coupling And One-Pot Cross Metathesis/dehydrogenative Coupling Reactions Of Alcohols Using Hoveyda-Grubbs Catalysts 作者:Ozer,Halenur; Et Al 参考文献:New Journal Of Chemistry 日期:2021 卷标:45(13) 页码:5992-6000]
= 629-59-4 反应条件:1.1 Solvents: Toluene; 5 Min,30 °C1.2 Catalysts: (T-4)-[1,3-Bis(2,4,6-Trimethylphenyl)-2-Imidazolidinylidene]Dichloro[[2-(1-Methy... Solvents: Toluene; 1 H,30 °C1.3 Catalysts: Potassium Hydroxide,Tricyclohexylphosphine Solvents: Toluene; Rt -> 110 °C; 24 H,110 °C 标题:Dehydrogenative Alcohol Coupling And One-Pot Cross Metathesis/dehydrogenative Coupling Reactions Of Alcohols Using Hoveyda-Grubbs Catalysts 作者:Ozer,Halenur; Et Al 参考文献:New Journal Of Chemistry 日期:2021 卷标:45(13) 页码:5992-6000]
10374-74-0 = 629-59-4 反应条件:1.1 Catalysts: Potassium Hydroxide,Tricyclohexylphosphine Solvents: Toluene; Rt -> 110 °C; 24 H,110 °C 标题:Dehydrogenative Alcohol Coupling And One-Pot Cross Metathesis/dehydrogenative Coupling Reactions Of Alcohols Using Hoveyda-Grubbs Catalysts 作者:Ozer,Halenur; Et Al 参考文献:New Journal Of Chemistry 日期:2021 卷标:45(13) 页码:5992-6000]
= 629-59-4 + 629-62-9 + 496-11-7 + 575-37-1 + 620-14-4 + 112-40-3 反应条件:1.1 Catalysts: Iron,Calcium; 15 Min,500 °C 标题:Preparation Of Sodium Silicate/red Mud-Based Zsm-5 With Glucose As A Second Template For Catalytic Cracking Of Waste Plastics Into Useful Chemicals 作者:Wang,Xiaofeng; Et Al 参考文献:Rsc Advances 日期:2022 卷标:12(34) 页码:22161-22174
正十六烷置于nickel Kieselguhr,氢气体系中,250.0~310.0 °C,1.37 Mpa 条件下,反应生成 十四烷 参考文献:Selective Demethylation Of Saturated Hydrocarbons 标题:Selective Demethylation Of Saturated Hydrocarbons
专利号:US-2004249114-A1 优先权日:2001-02-06 标题 :Methods of synthesis of polysuccinimide or polyaspartate by end capping polymerization 发明人:SWIFT GRAHAM; REDLICH GEORGE H; WEHBY JOHN NOLAN 摘要:Disclosed are methods of synthesis of homopolymers or copolymers containing succinimide or aspartate moieties formed in the presence of an end capping initiator. Also disclosed are methods of isolating, compounding, stabilizing and processing the homopolymers and copolymers.
专利号:US-2006211843-A1 优先权日:2001-02-06 标题:Methods of synthesis of poly(succinimide-aspartate) polysuccinimide or polyaspartate by end capping polymerization 发明人:SWIFT GRAHAM; REDLICH GEORGE H 权利人:SWIFT GRAHAM; REDLICH GEORGE H 摘要:Disclosed are methods of synthesis of homopolymers or copolymers containing succinimide or aspartate moieties formed in the presence of an end capping initiator. Also disclosed are methods of isolating, compounding, stabilizing and processing the homopolymers and copolymers.
专利号:US-9862745-B2 优先权日:2004-03-30 标题 :Synthesis of boronic ester and acid compounds 发明人:AMMOSCATO VINCE; BISHOP JOHN E; CHIU FANG-TING; GEISER ACHIM; GOMEZ JEAN-MARC; HETT ROBERT; KOELLNER CHRISTOPH; KULKARNI VITHALANAND R; LO YOUNG; MUNK STEPHEN; PICKERSGILL I FRASER 权利人:MILLENNIUM PHARM INC; MILLENNIUM PHARM INC 摘要:The invention relates to the synthesis of boronic ester and acid compounds. More particularly, the invention provides improved synthetic processes for the large-scale production of boronic ester and acid compounds, including the peptide boronic acid proteasome inhibitor bortezomib.
专利号:US-2004249115-A1 优先权日:2001-02-06 标题 :Methods of synthesis of poly(succinimide-aspartate) copolymer by end-capping polymerization 发明人:SWIFT GRAHAM; REDLICH GEORGE H 摘要:Disclosed are methods of synthesis of copoly(succinimide-aspartate), copolymers and derivatives thereof, prepared in a thermal or supercritical fluid method in the presence of an end capping initiator. Also disclosed are methods of isolating, compounding, stabilizing and processing the copoly(succinimide-aspartate), and its derivatives.
专利号:US-8642792-B2 优先权日:2007-02-15 标题 :Method for the synthesis of omega-amino-alkanoic acids 发明人:DUBOIS JEAN-LUC 权利人:DUBOIS JEAN-LUC; ARKEMA FRANCE 摘要:The invention relates to a method for the synthesis of amino acids/esters of general formula NH 2 —(CH 2 ) n —COOR in which n is an integer between 5 and 14, and R is either H or an alkyl radical including from 1 to 4 carbon atoms, from natural long-chain mono-unsaturated fatty acids or esters including at least 10 adjacent carbon atoms per molecule, said method comprising: first converting, if necessary, said natural long-chain fatty acid or ester into a monounsaturated fatty acid/ester of general formula R 1 —(CH 2 ) m —CHâ•?CH—(CH 2 ) p —COOR in which R 1 is H, CH 3 or a COOR radical, m is an integer between 0 and 14 and p is an integer between 2 and 11, then submitting the latter to a crossed catalytic metathesis reaction with a compound of formula R 2 —CHâ•?CH—R 3 in which R 2 is either H or CN and R 3 is CN or CH 2 NH 2 , provided that if R 2 is CN, R 3 can be only CN, and finally converting the resulting product of the general formula R 3 —CHâ•?CH—(CH 2 ) p —COOR into an amino-acid, either by hydrogenation, or by hydrogenation of the trple terminal bond, or by amination of the double terminal bond.
专利号:US-10059599-B2 优先权日:2014-02-03 标 题 :Synthesis of borane compounds 发明人:SAFRONOV ALEXANDER VALENTINOVICH; JALISATGI SATISH SUBRAY; HAWTHORNE MARION FREDERICK 权利人:SAFRONOV ALEXANDER VALENTINOVICH; JALISATGI SATISH SUBRAY; HAWTHORNE MARION FREDERICK; UNIV MISSOURI 摘要:The present invention is directed to a process for the synthesis of alkali metal tetrahydroborates- 10 B and amine borane- 10 B precursors, such as sodium tetrahydroborate- 10 B and triethylamine borane- 10 B.
[参考文献]: He Bo, Et Al. Tetradecane And Hexadecane Binary Mixtures As Phase Change Materials (Pcms) For Cool Storage In District Cooling Systems.Energy.Volume 24, Issue 12, January 1999, Pages 1015-1028. [参考文献]: Brian D Fitz, Et Al. Evaluation Of Injection Methods For Fast, High Peak Capacity Separations With Low Thermal Mass Gas Chromatography. J Chromatogr A. 2015 May 1:1392:82-90. [参考文献]: Enrico Colombo, Et Al. Role Of Counterions In Controlling The Properties Of Ultrasonically Generated Chitosan-Stabilized Oil-In-Water Emulsions. Acs Appl Mater Interfaces. 2015 Jun 17;7(23):12972-80. [参考文献]: F Aladar Bencsath, Et Al. Screening For Petrochemical Contamination In Seafood By Headspace Solid-Phase Microextraction Gas Chromatography-Mass Spectrometry. Anal Bioanal Chem. 2015 May;407(14):4079-90. [参考文献]: Georg Reiter, Et Al. In Vitro And In Vivo Toxicological Studies Of V Nerve Agents: Molecular And Stereoselective Aspects. Toxicol Lett. 2015 Jan 22;232(2):438-48.
合成参考文献
参考文献:10.1016/j.ijpharm.2011.06.046 摘要:Plajnšek KT, Pajk S, Govedarica B, Pečar S, Srčič S, Kristl J. A novel fluorescent probe for more effective monitoring of nanosized drug delivery systems within the cells. International Journal of Pharmaceutics. 2011 Sep;416(1):384–93. doi: 10.1016/j.ijpharm.2011.06.046. 参考文献:10.1136/thx.2010.156695 摘要:Ibrahim B, Basanta M, Cadden P, Singh D, Douce D, Woodcock A, Fowler SJ. Non-invasive phenotyping using exhaled volatile organic compounds in asthma. Thorax. 2011 Sep;66(9):804–9. doi: 10.1136/thx.2010.156695. 参考文献:10.1107/s1600536811013663 摘要:Dardouri R, Rodi YK, Ladeira S, Essassi EM, Ng SW. 3-Hexadecyl-1,5-dimethyl-1H-1,5-benzodiazepine-2,4(3H,5H)-dione. Acta Crystallogr E Struct Rep Online. 2011 Apr 16;67(5):o1155. doi: 10.1107/s1600536811013663. 参考文献:10.1155/2011/120462 摘要:Hasan GM, Garg N, Dogra E, Surolia R, Ghosh PC. Inhibition of the Growth ofPlasmodium falciparumin Culture by Stearylamine-Phosphatidylcholine Liposomes. Journal of Parasitology Research. 2011;2011():1–9. doi: 10.1155/2011/120462.