📜2-乙酰胺基噻唑置于硝酸,乙酸酐体系中,化学反应生成醋胺硝唑 参考文献:The Nitration Of 2-Nitraminothiazoles And 2-Acetamidothiazoles 标题:The Nitration Of 2-Nitraminothiazoles And 2-Acetamidothiazoles 摘要:通过使用99-100%硝酸和乙酸酐的混合物进行硝化反应,已经证明2-硝基氨基噻唑,例如2-硝基氨基-5-硝基噻唑和4-甲基-2-硝基氨基-5-硝基噻唑,可以以互变异构的硝基亚胺形式反应.硝化反应发生在噻唑环的三位.在噻唑环的二位具有乙酰胺基团的化合物,例如2-乙酰胺基-5-溴-2-噻唑和2-乙酰胺基-5-甲基噻唑,也可以在三位硝化,表明从乙酰胺基团到乙酰亚胺基团的互变异构. Doi:10.1139/v53-118
专利号:US-11958866-B1 优先权日:2023-04-07 标题:Synthesis of thiazole derivatives 发明人:NOOR AWAL; KHAN EZZAT; KHAN UMAR ALI 权利人:UNIV KING FAISAL 摘要:A synthetic protocol to use a thiourea or urea compound and auric chloride as starting materials to obtain thiazole and benzothiazole derivatives. The synthesis can be conducted at room temperature and the final compound can result from cyclization of the thiourea or urea compound in the presence of an Au salt from the auric chloride.
专利号:US-2024286909-A1 优先权日:2023-02-24 标 题 :Production of hexachlorodisiloxane 发明人:CHITTURI VENKATESWARA RAO; KOROLEV ANDREY 权利人:WONIK MAT NORTH AMERICA LLC 摘要:A method for the synthesis of perchlorodisiloxanes, and particularly hexachlorodisiloxane (Si2OCl6, HCDSO), using an amount of tetrachlorosilane (SiCl4) with an amount of molybdenum trioxide (MoO3). The method, in its broadest form, can be used to synthesize perchlorosiloxanes of the general formulae SixOx−1Cl2x+2. A catalytic amount of anhydrous HCl may be used to speed the reaction.
专利号:US-11814399-B1 优先权日:2023-04-07 标 题 :Synthesis of thiazole derivatives
专利号:CN-107722288-A 优先权日:2017-10-18 标题 :Synthesis of a Eu‑MOFs material and its application in antibiotic identification
专利号:US-2022370984-A1 优先权日:2021-05-21 标 题:Polymeric sorbent fiber compositions incorporating metal organic frameworks 发明人:WESTON SIMON C; KOROS WILLIAM J; Quan Wenying; LIVELY RYAN P; ZHANG FENGYI; ABNEY CARTER W; DEWITT STEPHEN J A; REALFF MATTHEW J; HOLMES HANNAH E; KAMATH MANJESHWAR G 权利人:EXXONMOBIL TECHNOLOGY & ENGINEERING COMPANY; GEORGIA TECH RES INST 摘要:Fiber compositions are provided that incorporate metal organic framework (MOF) materials into the polymeric matrix of the fiber. The metal organic framework materials can be incorporated by including MOF particles into a “dopeâ€? or synthesis solution used to form the fiber. The dope solution can then be used to form fibers that include 5.0 wt % or more of MOF in the resulting polymeric structural material of the fiber, relative to a weight of the fibers. In some aspects, the metal organic framework material can correspond to a MOF with selectivity for adsorption of CO 2 .
专利号:CN-109400895-A 优先权日:2018-10-19 标 题 :A kind of rare earth terbium-based metal organic framework material, synthesis method and its application in antibiotic identification
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合成参考文献
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