📜全氟辛基碘烷 以62%的收率获得产物全氟辛烷磺酰氯 参考文献:Process For The Preparation Of Perhaloalkanesulfinic And-Sulfonic 标题:Process For The Preparation Of Perhaloalkanesulfinic And-Sulfonic 摘要:制备全卤代烷基磺酸和其衍生物的过程.通过将金属羟甲磺酸盐(最好是钠,锌或铜羟甲磺酸盐)与全卤代烷基卤化物基团在极性溶剂中接触,制备全卤代烷基磺酸盐.可选地,然后将全卤代烷基磺酸盐转化为全卤代烷基磺酸或磺酸或这些酸中任一的衍生物.
专利号:US-4912269-A 优先权日:1987-07-10 标题 :Synthesis of perfluoroalkyl bromides 发明人:DRIVON GILLES; DURUAL PIERRE; GURTNER BERNARD; LANTZ ANDRE 权利人:ATOCHEM 摘要:The invention relates to the preparation of perfluoroalkyl bromides or bromoperfluoroalkanes, CnF 2n+1 -Br (n=1 to 20). n Gaseous hydrogen bromide is reacted with a perfluoroalkanesulphonyl chloride, C n F 2n+1 -SO 2 Cl, in the presence of a catalyst consisting of a tertiary amine or phosphine or a quaternary ammonium or phosphonium salt, at a temperature ranging from 80° to 200° C.
专利号:US-5057633-A 优先权日:1989-11-24 标题 :Synthesis of perfluoroalkyl bromides 发明人:DRIVON GILLES; DURUAL PIERRE; GHENASSIA ELIE 权利人:ATOCHEM 摘要:The invention relates to the preparation of perfluoroalkyl bromides or bromoperfluoroalkanes C n F 2n+1 -Br (n=1 to 20). n A perfluoroalkanesulphonyl chloride C n F 2n+1 -SO 2 Cl is reacted with a compound of formula: ##STR1## in which X represents a nitrogen or phosphorus atom and R 1 , R 2 , R 3 and R 4 , which may be identical or different, each represent an optionally substituted hydrocarbon radical, it also being possible for one of these symbols to be a hydrogen atom.
专利号:EP-3717521-A1 优先权日:2017-11-27 标 题:Process for the synthesis of a cyclodextrin derivative
专利号:ES-2948930-T3 优先权日:2017-11-27 标题 :Process for the synthesis of a cyclodextrin derivative
专利号:WO-2019102009-A1 优先权日:2017-11-27 标 题:Process for the synthesis of a cyclodextrin derivative
专利号:FR-2617836-A1 优先权日:1987-07-10 标 题:SYNTHESIS OF PERFLUOROALKYL BROMIDES
参考标题:Protease Inhibitors: Synthesis Of Potent Bacterial Collagenase And Matrix Metalloproteinase Inhibitors Incorporating N-4-Nitrobenzylsulfonylglycine Hydroxamate Moieties 作者:Andrea Scozzafava,Claudiu T. Supuran |发布日期:2000.5.1 摘要:A Series Of Compounds Was Prepared By Reaction Of Alkyl/arylsulfonyl Halides With N-4-Nitrobenzylglycine, Followed By Conversion Of The Cooh To The Conhoh Group, With Hydroxylamine In The Presence Of Carbodiimides. Other Structurally Related Compounds Were Obtained By Reaction Of N-4-Nitrobenzylglycine With Aryl Isocyanates, Arylsulfonyl Isocyanates, Or Benzoyl Isothiocyanate, Followed By The Similar
合成参考文献
摘要:S25 | OECDPFAS | List of PFAS from the OECD | DOI:10.5281/zenodo.2648775