CAS: 96824-28-1; 2-[(4-Acetylphenyl)Methyl]Cyclopentan-1-One
- 英文名称2-[(4-Acetylphenyl)Methyl]Cyclopentan-1-One
- 中文名称洛索洛芬相关化合物3
- IUPAC名称2-(4-acetylbenzyl)cyclopentan-1-one
- 其它别名2-[(4-Acetylphenyl)Methyl]Cyclopentan-1-One; Loxoprofen Impurity D; Loxoprofen Related Compound 3 (2-[(4-Acetylphenyl)Methyl]Cyclopentan-1-One); Loxoprofen Impurity 6/2-[(4-Acetylphenyl)Methyl]Cyclopentan-1-One; Loxoprofen Related Compound 3; 2-[4-(2-Oxycyclopentylmethyl)-Phenyl]Methylketone; 2-(4-Acetylbenzyl)Cyclopentan-1-One
- CAS编号96824-28-1
- MFCD编号:MFCD22581680
- FDA UNII编号:M895P7AU5D
- 分子式:C14H16O2分子量:216.28
- 产品CID: 2018948
- 产品分类分析化学 → 标准品 → 药典标准品和杂质标准品
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2-benzylcyclopentanone acetyl chloride loxoprofen Phosphoric acid 1-cyano-2-[4-(cyano-methyl-methyl)-benzyl]-cyclopentyl ester diethyl ester合成工艺路线路线简述
- 68767-14-6 = 96824-28-1
反应条件:1.1 Reagents: 2,4,6-Trimethylpyridine,Tetrabutylammonium Perchlorate,Water Catalysts: Tempo Solvents: Dichloromethane; 10 Min,Rt; 10 H,Rt1.2 Reagents: Hydrochloric Acid Solvents: Water
标题:Electrochemical Decarboxylative Oxygenation Of Carboxylic Acids
作者:Meng,Xiangtai; Xu,Hehua; Zheng,Yu; Luo,Jinyue; Huang,Shenlin
参考文献:Acs Sustainable Chemistry & Engineering 日期:2022 卷标:10(15) 页码:5067-5071]
68767-14-6 = 96824-28-1
反应条件:1.1 Reagents: Oxygen Catalysts: Cupric Acetate,2,9-Dimethyl-1,10-Phenanthroline Solvents: Acetonitrile,Water; 24 H,30 °C
标题:Copper(Ii)-Photocatalyzed Decarboxylative Oxygenation Of Carboxylic Acids
作者:Reichle,Alexander; Sterzel,Hannes; Kreitmeier,Peter; Fayad,Remi; Castellano,Felix N.; Et Al
参考文献:Chemical Communications (Cambridge 日期:2022 卷标:58(28) 页码:4456-4459]
2867-63-2 = 96824-28-1
反应条件:1.1 Reagents: Aluminum Chloride
标题:New Methods And Reagents In Organic Synthesis. 45. A New Synthesis Of Some Nonsteroidal Antiinflammatory Agents Via Cyano Phosphates
作者:Harusawa,Shinya; Nakamura,Shuji; Yagi,Sayoko; Kurihara,Takushi; Hamada,Yasumasa; Et Al
参考文献:Synthetic Communications 日期:1984 卷标:14(14) 页码:1365-71]
68767-14-6 = 96824-28-1
反应条件:1.1 Reagents: Dabco Catalysts: Iron(Iii) Acetylacetonate Solvents: Acetonitrile; 24 H,35 °C
标题:Iron-Catalyzed Ring-Opening Of Cyclic Carboxylic Acids Enabled By Photoinduced Ligand-To-Metal Charge Transfer
作者:Tu,Jia-Lin; Gao,Han; Luo,Mengqi; Zhao,Lulu; Yang,Chao; Et Al
参考文献:Green Chemistry 日期:2022 卷标:24(14) 页码:5553-5558]
68767-14-6 = 96824-28-1
反应条件:1.1 Reagents: 2,6-Lutidine,Oxygen Catalysts: Cerium Trichloride Solvents: Acetonitrile; 15 H,Rt
标题:Chemoselective Decarboxylative Oxygenation Of Carboxylic Acids To Access Ketones,Aldehydes,And Peroxides
作者:Guan,Renpeng; Chen,Guanhong; Bennett,Elliot L.; Huang,Zhiliang; Xiao,Jianliang
参考文献:Organic Letters 日期:2023 卷标:25(14) 页码:2482-2486]
68767-14-6 = 96824-28-1
反应条件:1.1 Reagents: Oxygen Catalysts: Manganese,Bis[4,4′-Bis(1,1-Dimethylethyl)-2,2′-Bipyridine-Kn1,Kn1′]Bis(1,1,1-Tr... Solvents: Acetonitrile; 12 H,1 Atm,45 °C
标题:Decarboxylative Oxygenation Of Carboxylic Acids With O2Via A Non-Heme Manganese Catalyst
作者:Guan,Renpeng; Bennett,Elliot L.; Huang,Zhiliang; Xiao,Jianliang
参考文献:Green Chemistry 日期:2022 卷标:24(7) 页码:2946-2952
📜洛索洛芬置于三乙烯二胺,Iron(Iii) Acetylacetonate体系中,用 乙腈 作为反应溶剂,化学反应 24.0H,以92%的收率获得产物洛索洛芬相关化合物3
参考文献:通过光诱导配体到金属的电荷转移实现铁催化的环状羧酸开环
标题:通过光诱导配体到金属的电荷转移实现铁催化的环状羧酸开环
摘要:描述了通过铁催化光诱导配体到金属电荷转移 (Lmct)的环状叔羧酸的脱羧开环协议.该反应能够通过无应变碳环和杂环系统的均裂 C-C 键断裂来制备 1,N-二羰基化合物.该方法具有合成条件温和,操作简单,扩增方便等优点.机理研究支持通过氧捕获然后自由基碎裂产生过氧自由基物质.
DOI:10.1039/d2Gc01738E
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