专利号:US-5852179-A 优先权日:1998-05-27 标 题 :Preparation of disperse azo dyestuffs in the presence of alkoxylated acetylenic diols 发明人:DADO GREGORY PAUL 权利人:AIR PROD & CHEM 摘要:The use of alkoxylated acetylenic diol surfactants in the aqueous synthesis of disperse azo dyes provides a simple process for improving filtration properties of dyestuff. The surfactants may be added prior to the coupling step of the synthesis or prior to heat treatment of the dye slurry. Advantages that are realized by incorporation of the surfactants into the synthesis include decreased filtration time, increased solid content in filter cake, improved washing properties of filter cake, and increased dye yield. In addition, for azo dyes that are synthesized as non-heat-stable crystal modifications, the presence of alkoxylated acetylenic diol surfactants in the dye slurry is effective in promoting the conversion of the dye to the desired thermally stable crystal modification.
专利号:US-9145304-B2 优先权日:2012-09-07 标 题 :Synthesis of nanosized sodium titanates 发明人:HOBBS DAVID T; TAYLOR-PASHOW KATHRYN M L; ELVINGTON MARK C 权利人:SAVANNAH RIVER NUCLEAR SOLUTIONS LLC 摘要:Methods directed to the synthesis and peroxide-modification of nanosized monosodium titanate are described. Methods include combination of reactants at a low concentration to a solution including a nonionic surfactant. The nanosized monosodium titanate can exhibit high selectivity for sorbing various metallic ions.
专利号:US-2024383831-A1 优先权日:2021-10-07 标 题 :Alkoxylation of cannabidiol and other cannabinoids 发明人:LAHASKY SAMUEL; SHARP KIP DOUGLAS; SLIKTA ALBERTO; PRESTRIDGE BRITNEY HEBERT; BARKER EMILY MATTHEWS; RICHARDSON RYAN 权利人:INDORAMA VENTURES OXIDES LLC 摘要:The present disclosure generally relates to the synthesis of an alkoxylated cannabinoid using a double metal cyanide (DMC) catalyst. This procedure affords a novel process for preparing water-dispersible and water-soluble versions of cannabidiol (CBD) and other cannabinoids in high yields through mild reaction conditions.
专利号:US-5457233-A 优先权日:1992-09-11 标 题 :Process for the preparation of amines 发明人:OUZIEL PHILIPPE 权利人:CIBA GEIGY CORP 摘要:A process for the preparation of amines of formula (1) wherein the variables are defined as in the claims, which comprises reacting 1 molar equivalent of an amine of formula (2) with 0.8 to 1.5 molar equivalents of an aldehyde of formula R-CHO(3) and 0.8 to 2 molar equivalents of formic acid, in aqueous medium, and adjusting the pH by addition of a mineral acid such that, at the conclusion of the reaction, the pH is in the range from 3 to 7. The compounds obtainable by the process are useful intermediates for the synthesis of dyeing assistants.
专利号:US-4076842-A 优先权日:1975-06-10 标 题:Crystalline zeolite ZSM-23 and synthesis thereof 发明人:PLANK CHARLES J; ROSINSKI EDWARD J; RUBIN MAE K 权利人:MOBIL OIL CORP 摘要:A new crystalline zeolite, designated ZSM-23, a method of making same and the use thereof in catalytic conversion of organic compounds is the subject of this application. The new zeolite has a composition, in the anhydrous state, expressed in terms of mole ratios of oxides, as follows; n n (0.58-3.4)M.sub.2/n O : Al.sub.2 O.sub.3 : (40-250)SiO.sub.2 n n wherein M is at least one cation having a valence n, and is characterized by a specified X-ray powder diffraction pattern.
专利号:ES-2939559-B2 优先权日:2021-10-22 标题 :Synthesis of trans 2,4,7,9-tetramethyldecen-4,7-diol by catalytic semi-hydrogenation with molecular hydrogen
[参考文献]: Betsy T Kren, Et Al. Preclinical Evaluation Of Cyclin Dependent Kinase 11 And Casein Kinase 2 Survival Kinases As Rna Interference Targets For Triple Negative Breast Cancer Therapy. Breast Cancer Res. 2015:17:19.
合成参考文献
摘要:S13 | EUCOSMETICS | Combined Inventory of Ingredients Employed in Cosmetic Products (2000) and Revised Inventory (2006) | DOI:10.5281/zenodo.2624118