CAS: 101199-38-6; Sodium 3-(10H-Phenothiazin-10-yl)Propane-1-Sulfonate

相似化合物

362-03-8 2803477-05-4 15375-48-1

上下游产品

CAS号1120-71-4 1,3-丙烷磺内酯 | CAS号92-84-2 吩噻嗪 | CAS号109-64-8 1,3-二溴丙烷

10-(3-溴丙基)吩噻嗪置于sodium Sulfite体系中,用 水,乙腈 用作溶剂,化学反应 12.0H,以51%的收率获得吩噻嗪-10-基-丙基磺酸钠盐
参考文献:库仑对吩噻嗪和紫精之间光诱导的电子转移反应的影响
标题:库仑对吩噻嗪和紫精之间光诱导的电子转移反应的影响
摘要:
Doi:10.1021/j100402A041

专利信息

专利号:US-7855287-B2
优先权日:2007-01-24
标题 :Preparation of high purity phenothiazine N-alkylsulfonates and their use in chemiluminescent assays for the measurement of peroxidase activity
发明人：DELLA CIANA LEOPOLDO
权利人:CYANAGEN SRL
摘要:A process is described for preparing, efficiently and with a high degree of purity N-alkylsulfonates of phenothiazine. The process consists in (a) the preparation of the phenothiazine anion, and (b) the reaction of said anion with cyclic alkyl sulfonates, such as 1,3-propane sultone and 1,4-butane sultone. This process is simpler, more direct, and more efficient than the procedures currently used for the synthesis of N-alkylsulfonates derivatives of phenothiazine. In addition, the products obtained with this process are far more pure than those obtained through current procedures and therefore ideal for bioanalytical applications that require high sensitivity, such as assays based on the measurement of peroxidase activity using chemiluminescence.