专利号:US-2023114534-A1 优先权日:2021-10-11 标题:High Temperature Chemical Process For The Preparation Of Cesium Tungstate 发明人:CARDARELLI FRANCOIS 权利人:CARDARELLI FRANCOIS 摘要:The present disclosure broadly relates to a high temperature chemical process for the synthesis of cesium tungstate in the solid state and the preparation of aqueous solutions or deuterated solutions of cesium tungstate. More specifically, but not exclusively, the present disclosure relates to a high temperature chemical process in which tungsten oxide compounds such as tungsten oxides, or natural or synthetic concentrates such as wolframite or scheelite, tungsten industrial by-products or there mixture thereof, are mixed with cesium compounds such as cesium carbonate, or cesium sulfate, or cesium hydroxide or their mixtures thereof and the mixture is roasted in air or oxygen at high temperature inside a kiln. After cooling, the solid sintered mass containing cesium tungstate is leached or dissolved with water or heavy water for producing dense aqueous solutions or deuterated solutions of cesium tungstate.
专利号:US-7833926-B2 优先权日:2005-07-01 标题 :Arylphenoxy catalyst system for producing ethylene homopolymer or copolymers of ethylene and α-olefins 发明人:WOO TAE WOO; OK MYUNG AHN; HAHN JONG SOK; LEE MAL-OU; KANG SANG OOK; KO SUNG-BO; KIM TAE-JIN; KIM SUNG-KWAN 权利人:SK ENERGY CO LTD 摘要:The present invention relates to an arylphenoxy catalyst system producing an ethylene homopolymer or copolymers of ethylene and α-olefins, and a method of producing an ethylene homopolymer or copolymers of ethylene and α-olefins having a high molecular weight under a high temperature solution polymerization condition using the same. The catalyst system includes a group IV arylphenoxy-based transition metal catalyst and an aluminoxane cocatalyst or a boron compound cocatalyst. In the transition metal catalyst, a cyclopentadiene derivative and arylphenoxide as fixed ligands are located around the group IV transition metal, arylphenoxide is substituted with at least one aryl derivative and is located at the ortho position thereof, and the ligands are not crosslinked to each other. The catalyst includes an environmentally-friendly raw material, synthesis of the catalyst is economical, and thermal stability of the catalyst is excellent. It is useful for producing an ethylene homopolymer or copolymers of ethylene and α-olefins having various physical properties in commercial polymerization processes.
专利号:US-4356308-A 优先权日:1980-04-05 标 题 :Process for the preparation of 2,2,6,6-tetramethylpiperidone-4 发明人:WIEZER HARTMUT; NOWY GUENTHER; HAEBERLEIN HARALD 权利人:HOECHST AG 摘要:In the synthesis of 2,2,6,6-tetramethylpiperidone-4 (triacetone-amine) from acetone and ammonia, a partially halogenated or perhalogenated aliphatic or cyclic hydrocarbon is used as catalyst in an amount of from 0.01 to 5 mol %, relative to acetone.
专利号:US-2025164360-A1 优先权日:2022-06-09 标 题:On-slide synthesis of a schiff reagent 发明人:BIRD JEAN MARIE; CANTORIA MARY JO CASTRO; DURRANT EDWARD E; HANNON ANDREW 权利人:VENTANA MED SYST INC 摘要:The present disclosure is directed to compositions, kits, and methods for synthesizing a Schiff's reagent in situ, i.e., directly on a substrate, such as within a puddle disposed on the surface of a substrate. In some embodiments, the kits comprise at least a dye composition and a sulfite composition. In some embodiments, the dye composition comprises a compound having a 4-Benzhydrylidene-2,5-cyclohexadien-1-imine core functionalized to include at least two substituted or unsubstituted amine groups, wherein the compound has a molecular weight ranging from between about 300 g/mol to about 600 g/mol. In some embodiments, the dye composition optionally includes an acid. In some embodiments, the sulfite composition comprises a sulfite or SO2 source.
专利号:US-6657068-B2 优先权日:2002-03-22 标题:Liquid phase oxidation of halogenated ortho-xylenes 发明人:COLBORN ROBERT EDGAR; HALL DAVID BRUCE; KOCH PETER; OECKEL GERALD 权利人:GEN ELECTRIC 摘要:A method for the manufacture of halophthalic acid by liquid phase oxidation of halo-ortho-xylene is disclosed. The halophthalic acid may be dehydrated to form halophthalic anhydride which is useful in the synthesis of polyetherimide.
专利号:US-6649773-B2 优先权日:2002-03-22 标题:Method for the manufacture of halophthalic acids and anhydrides 发明人:COLBORN ROBERT EDGAR; HALL DAVID BRUCE; KOCH PETER; OECKEL GERALD 权利人:GEN ELECTRIC 摘要:A method for the manufacture of halophthalic acid by liquid phase oxidation of halo-ortho-xylene is disclosed. The halophthalic acid may be dehydrated to form halophthalic anhydride which is useful in the synthesis of polyetherimide.
摘要:Chciuk, T. V.; Flowers, R. A.; Flowers, R. A., Science of Synthesis Knowledge Updates, (2016) 2, 184. 摘要:Flowers, R. A., II; Chciuk, T. V.; Bartulovich, C. O., Science of Synthesis, (2020) , 87. 摘要:AMA Archives of Industrial Hygiene and Occupational Medicine., 2(407), 1950 摘要:Toxicometric Parameters of Industrial Toxic Chemicals Under Single Exposure, Izmerov, N.F., et al., Moscow, Centre of International Projects, GKNT, 1982, -(107), 1982 摘要:Hamilton A, Hardy HL; Industrial Toxicology. 3rd ed. Acton, Mass: Pub Sci Group p. 295 (1974)