CAS: 100-00-5; 4-Chlorobenzonitrile

上下游产品

styrene N-nitrosamide of N-(4-nitrophenyl)acetamide 4-nitro-phenol ethanol 1-(4-nitro-phenyl)-pyrrolidine 1-(4-nitrophenyl)piperidine 1-morpholino-4-nitrobenzene 1-(4-Nitrophenyl)piperazine

对氯苯胺置于双氧水,Sodium Carbonate体系中,用 甲醇,水,乙腈 用作溶剂,化学反应 23.0H,以53%的收率获得对硝基氯苯
参考文献:"过碳酸钠" (Spc) 作为有机合成的过氧化氢来源
标题:"过碳酸钠" (Spc) 作为有机合成的过氧化氢来源
摘要:"过碳酸钠"(spc)是一种廉价,稳定,安全且可商购的材料,可用作有机合成的过氧化氢来源.环氧化,胺和硫化物氧化反应用固体试剂简单地进行,产率中等至极好.
Doi:10.1246/cl.1986.665

专利信息

专利号:US-4267070-A
优先权日:1979-10-30
标题:Catalyst for the synthesis of aromatic monoisocyanates
发明人：NEFEDOV BORIS K; MANOV-JUVENSKY VLADIMIR I; DERGUNOV JURY I; RYSIKHIN ANATOLY I; CHIMISHKIAN ALEXANDR L
权利人:NEFEDOV BORIS K; MANOV JUVENSKY VLADIMIR I; DERGUNOV JURY I; RYSIKHIN ANATOLY I; CHIMISHKIAN ALEXANDR L
摘要:A catalyst for the synthesis of aromatic monoisocyanates comprising 1.64 to 16.6% by weight of palladium chloride, 0.16 to 47.6% by weight of an oxide of a metal of Group VB of the periodic system, 1.5 to 81.8% by weight of an oxide of a metal of Group VI B of the periodic system, 1.64 to 89.8% by weight of pyridine or an alkylsubstituted pyridine. n The use of the catalyst according to the invention in the synthesis of aromatic monoisocyanates makes it possible to obtain a high degree of conversion of the starting compound of up to 100%, a high yield of the desired product of up to 97%, and increased productivity of the catalyst of up to 40 g of the desired product per g of PdCl 2 per hour.

专利号:US-9845289-B2
优先权日:2014-08-01
标题 :Process for the synthesis of Dapsone and its intermediates
发明人：BARATELLA MARCO; CASTALDI GRAZIANO; CASTALDI MARTA; GABOARDI MAURO; PALLANZA GIUSEPPE
权利人:SEEGPHARM SA
摘要:A process for the synthesis of Dapsone and intermediates thereof are described.

专利号:US-7531694-B2
优先权日:2004-07-07
标题:Process for synthesis of 4-4′-diamino-diphenyl-sulfone
发明人：VILLA MARCO; DE FAVERI CARLA; ZANOTTI RICCARDO; CIARDELLA FRANCESCO; BORIN FABRIZIO
权利人:LUNDBECK PHARMACEUTICALS ITALY
摘要:A new process for the preparation and purification of 4-4′-diamino-diphenyl-sulfone (dapsone) is described. The process described is a three step process comprising a condensation reaction with the synthesis of a thioether intermediate and then steps of oxidation and reduction in suitable conditions in order to obtain a product with good yield and purity.

专利号:US-5354439-A
优先权日:1990-07-16
标 题 :Process for the synthesis of fluorinated derivatives
发明人：FORAT GERARD; GILBERT LAURENT; LANGLOIS BERNARD
权利人:RHONE POULENC CHIMIE
摘要:A process for the synthesis of fluorinated organic compounds and a reagent suitable for use in the process. The process is carried out by exchange with fluorides, while preferably agitating the reaction medium with ultrasonic sound.

专利号:US-2004044225-A1
优先权日:2001-06-01
标 题:Chiral and achiral synthesis of 2-acyl substituted chromanes and their derivatives
发明人：KANTER JAMES; MARLOWE CHARLES; PANDEY ANJALI; MULLINS JOHN J G; SCARBOROUGH ROBERT; BUTKE GREG; JACOBSON BARRY; WALKER DEREK
摘要:Disclosed are processes for producing a (2S) or (2R) 4-oxo-chroman-2-yl acyl compounds and chroman-2-yl acyl compounds, esters or amides thereof as well as derivatives thereof. Such processes may involve chiral synthesis or achiral synthesis, preferably coupled with a resolution procedure. Such compounds, particularly (2S) or (2R) acetic acid esters, are useful intermedates for producing platelet aggregation inhibitors and/or are themselves potent platelet aggregation inhibitors. Further disclosed are processes for making derivatives of such substantially pure, or enhanced compositions of single (2R) or (2S) enantiomer intermediates or processes for producing final products or salts from such desired enantiomers.

专利号:US-4683332-A
优先权日:1985-05-20
标 题 :Para-nitrodiphenylamine synthesis
发明人：STURM BUDD H
权利人:GOODYEAR TIRE & RUBBER
摘要:There is disclosed a process for the synthesis of para-nitrodiphenylamines via the Formanilide Process wherein the improvement is characterized in that a specific catalyst is utilized. More specifically, a zinc (II) compound (zinc in the plus two oxidation or valence state), is used as a catalyst in the preparation of para-nitrodiphenylamines via the formanilide process.