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α-picoline dipropionyl peroxide ethyl iodide propionic acid pyridine-2,4-dicarboxylic acid 2-(4-Bromo-phenyl)-7-ethyl-indolizine 7-Ethyl-2-phenyl-°Ctahydro-indolizine 📜碳酸甲丙酯置于乙酸酐,锌体系中,化学反应生成 4-乙基-2-甲基吡啶
参考文献:De390333
标题:De390333
专利信息
专利号:US-8703952-B2
优先权日:2008-12-12
标题:Synthesis of 9-(arylalkyl)-1,2,3,4-tetrahydro-γ-carboline and analogues and intermediates
发明人:WILLIAMSON CRAIG; STOREY JOHN MERVYN DAVID
权利人:WILLIAMSON CRAIG; STOREY JOHN MERVYN DAVID; WISTA LAB LTD
摘要:The present invention pertains generally to methods of preparing certain 9-(arylalkyl)-1,2,3,4-tetrahydro-γ-carboline compounds and their analogues, and especially to methods of preparing dimebon. The present invention also pertains to methods of preparing certain intermediate compounds which find use in the synthesis of the 9-(arylalkyl)-1,2,3,4-tetrahydro-γ-carboline compounds.
专利号:EP-0150883-B1
优先权日:1984-02-02
标题 :Process for preparing n-(dibenzyloxyphosphoryl)-cyanamide and processes using said compounds as intermediate for the synthesis of phosphagen substances
摘要:The invention relates to a process for preparing compounds of general formula: wherein R = Hydrogen, halogen, alkyl, nitro-group; said compounds, which are indicated hereinunder with the general term <> are useful as intermediates in the synthesis of phosphagen compounds such as phosphocreatine, phosphocreatinine and similar compounds. Such process is characterized in that dibenzyloxyphosphoryl chloride is reacted with cyanamide, N-(dibenzyloxyphosphoryl)-cyanamide being produced; this latter can react with substances provided with a primary or secondary amine function, to give the corresponding guanidinoderivatives; e.g., with a sarcosine derivative to give N-(dibenzyloxyphosphoryl)-creatine or N-(dibenzyloxyphosphoryl)-creatinine.
专利号:US-6251350-B1
优先权日:1999-06-21
标 题 :Process for the manufacture of thiophosphoryl chloride
发明人:APPLEGATE JACQUELINE M; NEWALLIS PETER E; PRASAD VIDYANATHA A
权利人:BAYER AG
摘要:The present invention relates to an improved process for the preparation of thiophosphoryl chloride which is useful as an intermediate for the synthesis of insecticidally active compounds. The improvement comprises the presence in the reaction mixture of a catalytic amount of a nitroxide free radical of the following general formula: n wherein R 1 , R 2 , R 3 and R 4 represent an alkyl group.
专利号:US-3655835-A
优先权日:1968-05-20
标 题 :Process for the preparation of dimethyl-thiophosphite or of organothiophosphonous acid o-monomethyl ester
发明人:SCHLIEBS REINHARD
权利人:BAYER AG
摘要:REACTING TRIMETHYLPOSPHITE OR ORGANO-PHOSPHONOUS ACID O,O-DIMETHYL ESTER WITH HYDROGEN SULFIDE IN THE PRESENCE OF A WEAK ORGANIC BASE (THE PKA OF WHICH IN AQUEOUS SOLUTION IS ABOT 0.5-8) AT A TEMPERATURE OF SUBSTANTIALLY BETWEEN ABOUT 0-70*C. AND A STARTING PRESSURE OF SUBSTANTIALLY BETWEEN ABOUT 1-65 ATMOSPHERES ABSOLUTE, TO FORM IN HIGH YIELD AND PURITY THE CORRESPONDING KNOWN DIMETHYL-THIOPHOSPHITE OR ORGANO-THIOPHOSPHONOUS ACIDO-MONO METHYL ESTER, WHICH ARE KNOWN INTERMEDIATES USEABLE FOR THE SYNTHESIS OF KNOWN BIOCIDAL, ESPECIALLY INSECTICIDAL, PHOSPHORIC ACID ESTERS.
专利号:US-6432294-B1
优先权日:2000-12-14
标题 :Electrochemical activation of organic disulfides for electrophilic substitution
发明人:GLASS RICHARD S; JOUIKOV VIATCHESLAV V; BOJKOVA NINA V
权利人:UNIV ARIZONA
摘要:Electrochemical oxidation of organic disulfides is conducted in an electrolytic solution containing an arene (e.g., anthracene, acenaphthylene, phenanthrene), and depending on the arene used and/or the product desired, an organic base (e.g., pyridine) to effect the synthesis of organothiated products in good yields.
专利号:US-2009256111-A1
优先权日:2006-11-09
标题:Dialkylborane amine complexes
发明人:BURKHARDT ELIZABETH
权利人:BASF SE PATENTS TRADEMARKS AND
摘要:The present invention relates to new dialkylborane amine complexes, a process for the synthesis of new dialkylborane amine complexes, solutions comprising new dialkylborane amine complexes and a method of using new dialkylborane amine complexes for organic reactions.