CAS: 86595-27-9; Diisopropyl Methylboronate

该化合物是一种有机体化合物,其独特结构包括两个异丙氧基组和一个甲基组,其特点是其独特的结构,包括两个异丙氧组和一个与一个天文原子捆绑在一起.该化合物一般没有色素,是黄色的,以反应作用为名,特别是在有机合成中,作为以黄色为基的试剂.该化合物经常用于水合反应中,它可以在藻类中添加双环,从而便利形成可进一步转化为酒精或其他功能组的有机体.二异丙基甲基丙烷还因其与某些子质有选择地反应的能力而受到重视,使其成为合成有机化学的有用工具.在处理该化合物时,安全考虑十分重要,因为它可能易燃,并且会在接触皮肤或眼睛时引起刺激.在一个冷却,干燥的地方,远离不相容的材料,对保持化学反应的稳定性和有效性至关重要.

结构式图片

相似化合物

62260-99-5 137297-49-5 121021-24-7

物理性质

MSDS等安全信息

欧盟法规

C&L通报

上下游产品

Triisopropyl borate Trimethylboroxine methyllithium (E)-1-hexenyldiisopropoxyborane(4-chlorophenyl)-methyl-borinic acid isopropyl alcohol trimethylborane 2]Li[MeB(5-Ms-pz)H2]

合成工艺路线路线简述

  • 合成目标产物 Diisopropoxymethylborane 主要起始原料 Triisopropyl Borate And Trimethylboroxine
  • 917-54-4 = 86595-27-9
    反应条件:1.1 -78 °C
    标题:Fluorodimethoxyborane Diethyl Etherate
    作者:Marron,Thomas G.
    参考文献:E-Eros Encyclopedia Of Reagents For Organic Synthesis 日期:2001 卷标:1 页码:1-2]

    917-54-4 = 86595-27-9 [标题:Reaction Conditions
    标题:Chlorodimethoxyborane
    作者:Michaelides,Michael R.
    参考文献:E-Eros Encyclopedia Of Reagents For Organic Synthesis 日期:2001 卷标:1 页码:1-2]

    917-54-4 = 86595-27-9
    反应条件:1.1 Reagents: Hydrochloric Acid
    标题:Organoboranes. 31. A Simple Preparation Of Boronic Esters From Organolithium Reagents And Selected Trialkoxyboranes
    作者:Brown,Herbert C.; Et Al
    参考文献:Organometallics 日期:1983 卷标:2(10) 页码:1316-19]

    = 86595-27-9 [标题:Reaction Conditions
    标题:Organoboranes. 48. Improved Procedures For The Preparation Of Boronic And Borinic Esters
    作者:Brown,Herbert C.; Et Al
    参考文献:Organometallics 日期:1986 卷标:5(11) 页码:2300-3]

    = 86595-27-9 + 95407-90-2
    反应条件:1.1 Reagents: Magnesium Solvents: Diethyl Ether
    标题:Organoboranes. 39. Convenient Procedures For The Preparation Of Methylboronic Acid And Trimethylboroxin
    作者:Brown,Herbert C.; Et Al
    参考文献:Organometallics 日期:1985 卷标:4(5) 页码:816-21
📜硼酸三异丙酯,甲基锂 反应生成 二异丙氧基甲基硼烷
参考文献:路易斯酸催化合成聚吡唑基硼酸酯配体
标题:路易斯酸催化合成聚吡唑基硼酸酯配体
摘要:路易斯酸在温和的条件下催化li [mebh 3]和na [bh 4]与吡唑的反应,反应生成聚吡唑基硼酸酯.li [mebh 3]与2当量的3-甲磺酰基吡唑(hpz Ms)在23oc(2天)下反应,得到li [meb(3-Mesityl-Pz)2 H](li [mebp Ms])和li [meb(3-Mesityl-Pz)(5-Mesityl-Pz)h](li [mebp Ms *])在存在meb(o I Pr)2的情况下产率为88%(异构体比例为3:1)(5摩尔%对hpz Ms),但没有这种添加剂仅收率28%.在li的产量相似的增强[mebp-[r]的产品的li [mebh的反应观测到3用3-T Bu-吡唑,3,5-Me 2-吡唑(hpz *)和3,5-T Bu 2-吡唑.li [mebh 3]与3当量的hpz Ms(thf,60°C,2天)在3 Mol%meb(o I
DOI:10.1021/om100590X

海关参考信息

专利信息


专利号:US-7973171-B2
优先权日:2005-06-13
标题:Process for synthesis of dialkoxyorganoboranes
发明人：BURKHARDT ELIZABETH; ATKINS WILLIAM
权利人:BURKHARDT ELIZABETH; ATKINS WILLIAM
摘要:The invention relates to a process for the synthesis of dialkoxyorganoboranes, in particular to a process for the synthesis of dialkoxyorganoboranes by an ester exchange reaction. Moreover, the invention relates to a process for the synthesis of organo-oxazaborolidine catalysts (organo-CBS) and of trialkylboroxins. Furthermore, the invention relates to methods of using dialkoxyorganoboranes for the preparation of organo-CBS catalysts and in Suzuki-type coupling reactions.

专利号:US-2024229131-A1
优先权日:2022-12-22
标 题 :Transition-metal catalyst compositions and methods for sequencing by synthesis
发明人：MARIANI ANGELICA; BEECH TIMOTHY; FRANCAIS ANTOINE; PANIGRAHI ADYASHA; HATTINGH KATHRYN; CRESSINA ELENA
权利人:ILLUMINA INC
摘要:The present application relates to compositions and methods for sequencing by synthesis. A blocking group of a nucleotide may be removed by a transition metal catalyst, the transition metal catalyst activated by a non-reducing ligand and a reducing agent.

专利号:US-2024218443-A1
优先权日:2021-05-20
标 题:Methods of sequencing using 3' blocked nucleotides
发明人：MARIANI ANGELICA; FRANCAIS ANTOINE; TOPPING FREDERICK JAMES; WINNARD CHRISTOPHER; BALDING PHILIP; YUN CHOL STEVEN; IAVICOLI PATRIZIA; HATTINGH KATHRYN; WU XIAOLIN; LIU XIAOHAI
权利人:ILLUMINA INC
摘要:The present application relates to palladium compositions, methods for sequencing by synthesis using nucleotides with 3′ blocking groups, and sequencing kits, where one or more palladium scavengers were used to improve sequencing metrics such phasing and prephasing values.

专利号:US-2008200728-A1
优先权日:2005-06-13
标 题 :Process for Synthesis of Dialkoxyorganoboranes

专利号:ES-2357375-T3
优先权日:2005-06-13
标 题:PROCEDURE FOR THE SYNTHESIS OF ORGAN-OXAZABOROLIDINS.

专利号:CA-2610969-C
优先权日:2005-06-13
标题:Process for synthesis of dialkoxyorganoboranes

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合成参考文献


摘要:Kaufmann, D. E.; cal, N., Science of Synthesis, (2005) 6, 640.
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