📜亚氨基二乙酸置于phosphorus(III) Oxide,三氟甲磺酸体系中,化学反应 4.0H,以97.8%的收率获得亚氨基二(甲基磷酸) 参考文献: Method For The Synthesis Of Alpha-Aminoalkylenephosphonic Acid[fr] Procédé De Synthèse D'Acide Alpha-Aminoalkylènephosphonique 标题: Method For The Synthesis Of Alpha-Aminoalkylenephosphonic Acid[fr] Procédé De Synthèse D'Acide Alpha-Aminoalkylènephosphonique 摘要:本发明涉及一种合成α-氨基烯基膦酸或其膦酸酯的新方法,包括以下步骤:通过混合含有一个p原子在氧化态(+111)和另一个p原子在氧化态(+111)或(+v)的p-O-P酸酐基团的化合物,氨基烷基羧酸和酸催化剂来形成反应混合物,其中所述反应混合物中α-氨基烯基羧酸与p-O-P酸酐基团的当量比至少为0.2,并从反应混合物中回收所得的α-氨基烯基膦酸化合物或其酯.
专利号:US-8614312-B2 优先权日:2008-02-21 标 题 :Method for preparing nucleotides and related analogues by synthesis on soluble substrate, and biological tools thus prepared 发明人:PEYROTTES SUZANNE; PERIGAUD CHRISTIAN; CRAUSTE CELINE 权利人:PEYROTTES SUZANNE; PERIGAUD CHRISTIAN; CRAUSTE CELINE; CENTRE NAT RECH SCIENT; UNIV MONTPELLIER II 摘要:The invention concerns a method for preparing monomer nucleotides or nucleotide analogues comprising the steps of: (1) coupling a soluble polyethylene glycol support provided with at least one diacid or ether-acid linker and a monomer nucleoside or nucleoside analogue to an amine group or hydroxyl group of the nucleoside with the aid of a coupling agent; (2) at least one step for phosphorylation of said nucleoside or nucleoside analogue coupled to said support with a phosphorylation agent; (3) cleavage of said support and recovery of at least one monomer nucleotide or nucleotide analogue. The nucleotides prepared are biological tools.
专利号:AU-2005306708-A1 优先权日:2004-11-12 标 题:Recovery of noble metals from aqueous process streams in the synthesis of glyphosate using adsorption media such as ion exchange resins
专利号:US-2008050747-A1 优先权日:2006-03-30 标题:Articles having localized molecules disposed thereon and methods of producing and using same 发明人:KORLACH JONAS; TURNER STEPHEN 权利人:PACIFIC BIOSCIENCES CALIFORNIA 摘要:Sequencing methods and compositions, substrates, devices and systems are provided. Methods include synthesizing a nascent nucleic acid sequence that is greater than 100 bases in length and sequencing the nucleic acids by detecting synthesis. Compositions and substrates that include polymerization complexes for the methods are included.
专利号:CA-2587384-A1 优先权日:2004-11-12 标 题:Recovery of noble metals from aqueous process streams in the synthesis of glyphosate using adsorption media such as ion exchange resins
专利号:WO-2006055441-A1 优先权日:2004-11-12 标题:Recovery of noble metals from aqueous process streams in the synthesis of glyphosate using adsorption media such as ion exchange resins
专利号:EP-1809642-A1 优先权日:2004-11-12 标 题 :Recovery of noble metals from aqueous process streams in the synthesis of glyphosate using adsorption media such as ion exchange resins
参考标题:Hydro-Ionothermal Syntheses, Crystal Structures, And Properties Of Five New Divalent Metal Iminophosphonates 作者:Kevin J. Gagnon,Andrey V. Prosvirin,Kim R. Dunbar,Simon J. Teat,Abraham Clearfield 摘要:Hydrophobic Ionic Liquid 1-Butyl-2,3-Dimethylimidazolium Tetrafluoroborate ([bdmim][bf4]) With Water As A Cosolvent, While 2 Has Been Synthesized From Identical Conditions In The Absence Of The [bdmim][bf4]. We Also Report The Microwave Assisted Hydro-Ionothermal Synthesis Of The Known Polymorph Of 2, Co(H2O)2(Ho3Pch2Nh2Ch2Po3H)2, (6), Synthesized In Two Hours Providing High Quality Crystals In Good Yield
合成参考文献
参考文献:10.1016/j.bmc.2009.03.039 摘要:Kasser J, Nazarov AA, Hartinger CG, Wdziekonski B, Dani C, Kuznetsov ML, Arion VB, Keppler BK. A one step/one pot synthesis of N,N-bis(phosphonomethyl)amino acids and their effects on adipogenic and osteogenic differentiation of human mesenchymal stem cells. Bioorg Med Chem. 2009 May 01;17(9):3388–93. doi: 10.1016/j.bmc.2009.03.039.