CAS: 589-09-3; N-Allylaniline

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CAS号106-95-6 烯丙基溴 | CAS号583-55-1 2-溴碘苯 | CAS号107-11-9 丙烯胺 | CAS号14465-74-8 N-(2-丙炔基)苯胺 | CAS号107-18-6 烯丙醇 | CAS号591-87-7 乙酸烯丙酯 | CAS号98-80-6 苯硼酸 | CAS号591-50-4 碘苯 | CAS号111-34-2 乙烯基正丁醚 | CAS号111457-18-2 N-(2-prop-2-eny... | CAS号5388-42-1 2-苯基-1-氧代二氢氮杂茚 | CAS号4096-21-3 1-苯基吡咯烷 | CAS号622-80-0 N-丙基苯胺 | CAS号139944-54-0 3-anilino-2-met... | CAS号31121-11-6 3-苯氨基-1-丙醇 | CAS号345305-22-8 (2S)-1-N-Phenyl... | CAS号345305-21-7 (2R)-1-N-Phenyl... | CAS号4641-57-0 1-苯基-2-吡咯烷酮 | CAS号1745-81-9 2-烯丙基酚

📜1,2-二苯肼置于正丁基锂,Titanium(Iii) Chloride,水体系中,用 四氢呋喃,正己烷 作为反应溶剂,化学反应 4.25H,反应生成 N-烯丙基苯胺
参考文献:三氯化 钛(iii)的水溶液将肼还原为胺†
标题:三氯化 钛(iii)的水溶液将肼还原为胺†
摘要:肼中n-n键的裂解被广泛用于胺的制备中,因此在有机合成中占有重要地位.在本文中,我们报告了一种新的方法,该方法可通过市售廉价的水溶液还原肼中的n-n键三氯化钛.反应可在从酸性到中性和碱性的宽ph范围内顺利进行,从而以非常好的收率得到胺.此方法与包含官能团的底物兼容,例如,Cc双键,苄基-氮键,苄氧基和酰基.
DOI:10.1039/c1Ob05328K

专利信息

专利号:US-2023174477-A1
优先权日:2021-12-03
标题:Methods for synthesis of the tricyclic prostaglandin d2 metabolite methyl ester
发明人：DAI MINGJI; SIMS HUNTER
权利人:PURDUE RESEARCH FOUNDATION
摘要:Methods for the synthesis of a tricyclic-prostaglandin D 2 metabolite methyl ester or a pharmaceutically acceptable salt thereof.

专利号:US-6472228-B2
优先权日:2000-12-04
标题:Composition and methods for synthesis of novel tracers for detecting amphetamine and methamphetamine in samples
发明人：WANG GUOHONG; FOLEY THOMAS
权利人:LIFEPOINT INC
摘要:This invention relates to novel tracers and their synthesis and use in an immunoassay for the detection of controlled drugs such as amphetamine (APM), methamphetamine (MAPM) and their derivatives, in a biological or aqueous sample. In particular, this invention provides methods for synthesizing novel tracers in which a non-controlled substance is both the starting material in tracer synthesis and the binding site on the resulting novel tracer for the antibody, thereby eliminating the necessity of using controlled substances as starting materials. In addition, the novel tracers of the present invention can be used as an analyte analog in an immunoassay, such as a continuous flow displacement immunoassay. It was unexpectedly discovered that the novel tracers of the present invention substantially improve the performance of the continuous flow displacement immunoassay as compared with conventionally designed tracers.

专利号:US-7034040-B2
优先权日:2002-03-01
标题:Fluorinated heterocyclic compounds and methods of synthesis
发明人：KWIATKOWSKI STEFAN; GOLINSKI MIROSLAW
权利人:R T ALAMO VENTURES I
摘要:Compositions of the present invention comprise fluorinated heterocyclic compounds, including monofluoroflosequinan and difluoroflosequinan. The methods of the present invention comprise the synthesis of monofluoroflosequinan and difluoroflosequinan.

专利号:US-3888844-A
优先权日:1971-09-10
标 题:Halogenated esters of phosphorus-containing acids (ii)
发明人：D ALELIO GAETANO F
权利人:ALELIO GAETANO F D
摘要:This invention deals with new phosphorus containing polymeric esters having pendent groups therein of the formula OBTAINED BY THE REACTION OF A POLYMER HAVING AT LEAST 2 AND PREFERABLY AT LEAST 4 HYDROXY GROUPS THEREIN WITH A PHOSPHORUSHALOGEN COMPOUND OF THE FORMULA XP(O) (ORCX CXR'')2 wherein: R represents a divalent hydrocarbon radical containing 1-20 carbon atoms; R'' represents X, hydrogen or R''''; R'''' represents a monovalent hydrocarbon radical containing 1-20 carbon atoms; and X represents chlorine or bromine. Somewhat related polymers are also disclosed as derived by the reaction of WHEREIN Q'' is an organic moiety, n'' has a value of at least one, n'''' is one or two, R'''''' represents hydrogen or a monovalent hydrocarbon group of 1-20 carbon atoms, and the other symbols have the same meaning as defined above. Also disclosed are the reaction products of the phosphite compound HOP(ORCX CXR'')2 with an aldehyde and an organic nitrogen compound having one or two hydrogen atoms on the nitrogen, or with a compound having an ethylenic group therein. These new ester polymers and compounds are useful particularly as fire retardants, agricultural chemicals, fuel additives, plasticizers, monomers and intermediates for the synthesis of other useful derivatives.

专利号:US-3962273-A
优先权日:1972-09-01
标题:Novel method for the synthesis of 4-thio and 4-seleno ethers of 2-pyrazolin-5-ones
发明人：MACHIELE DELWYN E
权利人:EASTMAN KODAK CO
摘要:Method for synthesizing 4-substituted thiol and 4-substituted seleno-2-pyrazolin-5-ones by reaction of an appropriate thiol or selenol compound with a 4,4-dihalo-2-pyrazolin-5-one.

专利号:US-6384216-B1
优先权日:2000-08-09
标 题 :Purification of alkenyl compounds
发明人：LORENZ RUDOLF ERICH; BOETTCHER ARND; PINKOS ROLF
权利人:BASF AG
摘要:A process for purifying alkenyl compounds having a divalent or trivalent heteroatom in the alpha-position relative to the double bond by distillation comprises carrying out at least two distillations in which the purified alkenyl compounds are obtained from the gas phase by condensation, where the time between the first distillation after the synthesis of the alkenyl compounds and at least one further distillation is at least one day and the purified alkenyl compounds have an APHA color number of <30.