CAS: 3572-44-9; 3-Anot

该化合物是有机化合物,其特点是存在氨基氨基化合物(-NH2)和与富氨基甲酰胺结构相连的硝基甲基苯基化合物,该化合物一般是固体的,由于氨基甲基混合物的存在,在极地溶剂中可以溶解.该化合物可以使用氢结合;该硝基氮组有助于其反应,成为各种化学反应(包括核生殖替代和减少)的潜在候选物;氨基和硝基氨的功能表明它可能表现出生物活动,有可能在合成药物或农用化学品过程中充当中间体;此外,该复合物的结构表明它具有特定的电子特性,影响其在化学反应和与其他物质相互作用中的行为;应当参考安全数据,因为硝基化合物有时可能具有危险性,实验室环境应当遵循适当的处理程序.

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CAS号148-01-6 二硝托胺

合成工艺路线路线简述

    📜二硝托胺置于palladium On Activated Charcoal,环己烯体系中,用 乙醇 用作溶剂,化学反应生成5-氨基-2-甲基-3-硝基苯甲酰胺,3-氨基-2-甲基-5-硝基苯甲酰胺
    参考文献:Chemical Reduction Of Zoalene To Anot For Use In Zoalene Residue Studies
    标题:Chemical Reduction Of Zoalene To Anot For Use In Zoalene Residue Studies
    摘要:A Novel Chemical Synthesis And Purification Scheme To Produce Anot (3-Amino-5-Nitro-O-Toluamide) Was Developed To Yield An Analytical Standard Grade Material For Zoalene Residue Investigations. An Original Conversion Of Zoalene (3,5-Dinitro-O-Toluamide) To Anot Was Developed. Several Literature References Were Available For The Partial Reduction Of Dinitro Aryl Compounds,But None Detailed The Conversion Of Zoalene To Anot. A Chemical Synthesis Was Chosen Over A Biological Synthesis Due To The Latter'S Complex Reaction Matrix,Difficult Recovery,And Low Batch Yields. Using General Partial Reduction Of Dinitro Aryl Schemes,It Was Found That 10% Palladium On Carbon Coupled To A Cyclohexene Reducing Agent Provided An Optimum Anot Yield. Chromatographic Techniques Were Utilized To Isolate Anot From The Product Mixture And To Purify It To A Standard Grade Material (>99% Pure). The Chemically Synthesized Anot Product Was Characterized Using Colorimetric,Tlc,Ftir,NMR,And Lc/ms Techniques.
    Doi:10.1021/jf9802068

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    专利信息


    专利号:WO-2022213975-A1
    优先权日:2021-04-08
    标题:Compounds targeting y220c mutant of p53
    发明人：LI SUJING; LI AMIN; ZHENG QIAN; Dang Chaojie; FAN XINRUI; LONG WEI; WANG YANPING
    权利人:JACOBIO PHARMACEUTICALS CO LTD
    摘要:Provided are compounds of formula (I) which can bind to p53 mutant and restore its ability to bind DNA and activate downstream effects involved in tumor suppression. Also provided are the synthesis processes and use of the compounds.

    专利号:EP-0785786-A1
    优先权日:1994-10-25
    标题:Microbial synthesis of hiv protease inhibitors

    专利号:EP-0785989-A4
    优先权日:1994-10-25
    标题 :MICROBIAL SYNTHESIS OF INHIBITORS OF THE HIV PROTEASE

    专利号:WO-9612492-A1
    优先权日:1994-10-25
    标 题 :Microbial synthesis of hiv protease inhibitors

    专利号:WO-9612790-A1
    优先权日:1994-10-25
    标题:Microbial synthesis of hiv protease inhibitors

    专利号:EP-0785786-A4
    优先权日:1994-10-25
    标 题 :MICROBIAL SYNTHESIS OF HIV PROTEASE INHIBITORS

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    合成参考文献


    摘要:Pesticide Chemicals Official Compendium, Association of the American Pesticide Control Officials, Inc., 1966., -(51), 1966
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