合成路线:The methylation of 4,5-dimethoxy-2-methylthiophenol (I) with dimethyl sulfate by means of sodium ethoxide in refluxing ethanol gives 4,5-dimethoxy-2-methylphenyl methyl sulfide (II),which is then oxidized with H2O2 in glacial acetic acid.
参考文献标题:
文献作者:Bentley,J.M.; Rushworth,W.I.
参考来源:CA 960697; DE 2160148; FR 2116579; GB 1337575; US 3804904; US 3886285; ZA 7107860
合成路线:The methylation of 4,5-dimethoxy-2-methylthiophenol (I) with dimethyl sulfate by means of sodium ethoxide in refluxing ethanol gives 4,5-dimethoxy-2-methylphenyl methyl sulfide (II),which is then oxidized with H2O2 in glacial acetic acid.
参考文献标题:Tolmesoxide
文献作者:Castar,J.; Hillier,K.
参考来源:Drugs Fut 1978,3(9),691
产品链接: CAS No. 38452-29-8››