合成路线:By reacting 1,3-dihydro-7-nitro-5-phenyl-2H-1,4-benzodiazepin-2-one (I) with sodium methoxide (A) and chloromethylmethylether in dimethylformamide (1); by treating the 4,5-dihydro-4-p-tolylsulfonyl derivative (II) with sodium methoxide in dimethyl formamide (2) or by heating the 4-hydroxy derivative (III) in toluene containing dicyclohexylcarbodiimide (3).
参考文献标题:
文献作者:Hellerbach,J.; Walser,A.
参考来源:CH 574442
合成路线:By reacting 1,3-dihydro-7-nitro-5-phenyl-2H-1,4-benzodiazepin-2-one (I) with sodium methoxide (A) and chloromethylmethylether in dimethylformamide (1); by treating the 4,5-dihydro-4-p-tolylsulfonyl derivative (II) with sodium methoxide in dimethyl formamide (2) or by heating the 4-hydroxy derivative (III) in toluene containing dicyclohexylcarbodiimide (3).
参考文献标题:
文献作者:Hellerbach,J.; Walser,A.
参考来源:CH 574420
合成路线:By reacting 1,3-dihydro-7-nitro-5-phenyl-2H-1,4-benzodiazepin-2-one (I) with sodium methoxide (A) and chloromethylmethylether in dimethylformamide (1); by treating the 4,5-dihydro-4-p-tolylsulfonyl derivative (II) with sodium methoxide in dimethyl formamide (2) or by heating the 4-hydroxy derivative (III) in toluene containing dicyclohexylcarbodiimide (3).
参考文献标题:Motrazepam
文献作者:Unterhalt,B.
参考来源:Drugs Fut 1978,3(10),758
产品链接: CAS No. 29442-58-8››