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Befuraline hydrochloride, DIV-154

苯呋拉林Chemical Name: N-Benzyl-coumarilic acid piperazide hydrochloride; N-Benzo[b]furan-2-ylcarbonyl-N'-benzylpiperazine hydrochloride; 1-(2-Benzofuranylcarbonyl)-4-(phenylmethyl)piperazine hydrochloride
CAS No. 41717-30-0 (free base)
项目整合开发状态: Biological Testing
项目研究机构: Aventis Pharma (Originator)
合成路线:Coumarilic acid is reacted with N-benzylpiperazine (II) by two different ways:a) The acid chloride (I) is treated with (II) in the presence of a further base to give (III) or without a base in boiling dimethylformamide.b) The coumarilic acid salt of N-benzylpiperazine (IV) is converted to (III) by heating up to 170-250 C.
📌 参考资料/链接:
参考文献标题:Cyclic diamine derivatives
文献作者:Soeder,A.; et al.(Aventis Pharma AG)
参考来源:DE 2157424; DE 2240665; ES 408565; FR 2160611; GB 1407854; US 4374990

📄 详细内容


合成路线:Coumarilic acid is reacted with N-benzylpiperazine (II) by two different ways:a) The acid chloride (I) is treated with (II) in the presence of a further base to give (III) or without a base in boiling dimethylformamide.b) The coumarilic acid salt of N-benzylpiperazine (IV) is converted to (III) by heating up to 170-250 C.

参考文献标题:Befuraline Hydrochloride
文献作者:Unterhalt,B.
参考来源:Drugs Fut 1978,3(6),426


合成路线:Coumarilic acid is reacted with N-benzylpiperazine (II) by two different ways:a) The acid chloride (I) is treated with (II) in the presence of a further base to give (III) or without a base in boiling dimethylformamide.b) The coumarilic acid salt of N-benzylpiperazine (IV) is converted to (III) by heating up to 170-250 C.
参考文献标题:Synthesis and pharmacological activity of befuralline,a new antidepressnt compound
文献作者:Boksay,I.J.E.; et al.
参考来源:Arzneim-Forsch Drug Res 1978,28(19,Suppl.2),


产品链接: CAS No. 41717-30-0››